Document otsegocountymi_gov_doc_2c226f7145

BID 2020-05 for OTSEGO COUNTY ROYAL CREST MOTEL DEMOLITION Date Issued: July 31, 2020 Date Due: Friday, August 21, 2020, by 1:00 pm local time ---PAGE BREAK--- 000110 - 1 OTSEGO COUNTY ROYAL CREST MOTEL DEMOLITION OTSEGO COUNTY, MICHIGAN TABLE OF CONTENTS Advertisement For Bids AD1 Instructions to Bidders IB1-6 Bid Form BF1-4 Attachment A NCA1 Attachment B BI1 Engineer Table of Contents, Specifications, and Drawings 1-27 Appendices A, B, C, D 1-131 Otsego County Administrative Policy Manual 1-9 ---PAGE BREAK--- AD-1 ADVERTISEMENT FOR BIDS OTSEGO COUNTY ROYAL CREST MOTEL DEMOLITION Gaylord, Michigan BID 2020-05 1. Sealed Bids for the Otsego County Royal Crest Motel Demolition will be received by Otsego County Administration, 225 West Main Suite 203, Gaylord, Michigan 49735, until 1:00 pm local time, on Friday, August 21, 2020. Bids will be opened and publicly read aloud in Room 100 at that time. 2. The full bid package will be available on-line at http://www.otsegocountymi.gov/general-information/bids- and-proposals/ beginning Friday, July 31, 2020. Hard copies of the Bid Documents are available upon request, starting July 31, 2020, at the Otsego County Administration Office, 225 West Main, Suite 203, Gaylord, Michigan 49735. Phone: [PHONE REDACTED]. 3. A mandatory pre-bid/site walk-through will be held at 10:00 am, Monday, August 17, 2020, at the Project Site. 4. Any questions must be received by the end of business day on Wednesday, August 19, 2020. All questions related to the Demolition and Disposal of the former Royal Crest Motel are to be directed to Chris Churches at [EMAIL REDACTED] or (989) 731-7515. 5. The principal items of work consist of the following: Demolish and dispose of the former Royal Crest Motel buildings complete at 803 South Otsego Avenue, Gaylord, Michigan 49735. 6. The intent of Otsego County is to award one Contract for the entire project. 7. Bids shall remain firm and shall not be withdrawn for a period of ninety (90) calendar days after bid opening. 8. The County of Otsego reserves the right to accept, reject or negotiate any or all bids to waive or not waive informalities or irregularities in the bids or bidding procedures and to accept any bid determined by the County to be in the best interest of the County, regardless of price. Vendors located in Otsego County receive a 5% cost variance for low bid determination. ---PAGE BREAK--- IB1 INSTRUCTIONS TO BIDDERS ARTICLE 1 - DEFINED TERMS 1.01 Terms used in these Instructions to Bidders will have the meanings indicated in the General Conditions and Supplementary Conditions. Additional terms used in these Instructions to Bidders have the meanings indicated below which are applicable to both the singular and plural thereof: A. Bidder-The individual or entity who submits a Bid directly to OWNER. B. OWNER-The owner of this project is Otsego County. C. ENGINEER-The engineer is C2AE, 123 W. Main Street, Suite 200, Gaylord, Michigan 49735. Attention: Kevin Makarewicz. D. Issuing Office-The office from which the Bidding Documents are to be issued and where the bidding procedures are to be administered. The issuing office is Otsego County Administration, 225 W. Main Street, Suite 203, Gaylord, Michigan 49735. E. Successful Bidder-The lowest responsible Bidder submitting a responsive Bid to whom OWNER (on the basis of OWNER’S evaluation as hereinafter provided) makes an award. ARTICLE 2 - COPIES OF BIDDING DOCUMENTS 2.01 Complete hard copy sets of the Bidding Documents may be obtained from the Issuing Office upon request. The Complete set of Bidding Documents is available online at http://www.otsegocountymi.gov/general-information/bids-and-proposals/ 2.02 Complete sets of Bidding Documents must be used in preparing Bids; neither OWNER nor ENGINEER assumes any responsibility for errors or misinterpretations resulting from the use of incomplete sets of Bidding Documents. 2.03 OWNER in making copies of Bidding Documents available on the above terms does so only for the purpose of obtaining Bids for the Work and do not confer a license or grant for any other use. ARTICLE 3 - QUALIFICATIONS OF BIDDERS 3.01 To demonstrate Bidder’s qualifications to perform the Work, within five days of OWNER’S request Bidder shall submit written evidence such as financial data, previous experience, present commitments, and such other data as may be called for by the OWNER. 3.02 Bidders will be required to execute a Noncollusion Affidavit of Prime Bidder Statement (page NCA-1) and include the affidavit with this Bid. ARTICLE 4 - EXAMINATION OF BIDDING DOCUMENTS, OTHER RELATED DATA, AND SITE 4.01 On request, OWNER will provide Bidder access to the Site to conduct such examinations, investigations, explorations, tests, and studies as Bidder deems necessary for submission of a Bid. Bidder shall fill all holes and clean up and restore the Site to its former condition upon completion of such explorations, investigations, tests, and studies. 4.02 It is the responsibility of each Bidder before submitting a Bid to: ---PAGE BREAK--- A. Examine and carefully study the Bidding Documents, including any Addenda and the other related data identified in the Bidding Documents; B. Visit the Site and become familiar with and satisfy Bidder as to the general, local, and Site conditions that may affect cost, progress, and performance of the Work; Site visits shall be coordinated through Chris Churches, [EMAIL REDACTED] or (989) 731-7515 and shall take place during the week of Monday, August 17, 2020. C. Become familiar with and satisfy Bidder as to all federal, state, and local Laws and Regulations that may affect cost, progress, or performance of the Work; D. Agree at the time of submitting its Bid that no further examination, investigations, explorations, tests, studies, or data are necessary for the determination of its Bid for performance of the Work at the price bid and within the times and in accordance with the other terms and conditions of the Bidding Documents; E. Correlate the information known to Bidder, information and observations obtained from visits to the Site, reports and drawings identified in the Bidding Documents, and all additional examinations, investigations, explorations, tests, studies, and data with the Bidding Documents; F. give ENGINEER written notice of all conflicts, errors, ambiguities, or discrepancies that Bidder discovers in the Bidding Documents and confirm that the written resolution thereof by ENGINEER is acceptable to Bidder; and G. Determine that the Bidding Documents are generally sufficient to indicate and convey understanding of all terms and conditions for the performance of the Work. 4.03 The submission of a Bid will constitute an incontrovertible representation by Bidder that Bidder has complied with every requirement of this Article 4, that without exception the Bid is premised upon performing and furnishing the Work required by the Bidding Documents and applying any specific means, methods, techniques, sequences, and procedures of construction that may be shown or indicated or expressly required by the Bidding Documents, that Bidder has given ENGINEER written notice of all conflicts, errors, ambiguities, and discrepancies that Bidder has discovered in the Bidding Documents and the written resolutions thereof by ENGINEER are acceptable to Bidder, and that the Bidding Documents are generally sufficient to indicate and convey understanding of all terms and conditions for performing and furnishing the Work. ARTICLE 5 - PRE-BID CONFERENCE ARTICLE 6 - SITE AND OTHER AREAS 6.01 The Site is identified in the Bidding Documents. All additional lands and access thereto required or temporary construction facilities, construction equipment, or storage of materials and equipment to be incorporated in the Work are to be obtained and paid for by CONTRACTOR. Easements for permanent structures or permanent changes in existing facilities are to be obtained and paid for by OWNER unless otherwise provided in the Bidding Documents. ARTICLE 7 - INTERPRETATIONS AND ADDENDA 7.01 All questions about the meaning or intent of the Bidding Documents are to be submitted to ENGINEER in writing. Interpretations or clarifications considered necessary by ENGINEER in response to such IB2 5.01 A mandatory pre-bid conference will be held beginning at 10 a.m., Monday, August 17, 2020 at the Project Site. ---PAGE BREAK--- IB3 7.02 Addenda may be issued to clarify, correct, or change the Bidding Documents as deemed advisable by OWNER and ENGINEER. ARTICLE 8 - BID SECURITY 8.01 A Bid security is required in the amount of 10% of the bid amount. ARTICLE 9 - CONTRACT TIMES 9.01 The number of days within which, or the dates by which, the Work is to be Substantially Completed and also completed and ready for final payment are set forth in the Agreement. ARTICLE 10 - LIQUIDATED DAMAGES 10.01 Provisions for liquidated damages, if any, are set forth in the Bid Form. ARTICLE 11 - SUBSTITUTE AND “OR-EQUAL” ITEMS 11.01 The Contract, if awarded, will be on the basis of materials and equipment specified or described in the Bidding Documents without consideration of possible substitute or “or-equal” items. Whenever it is specified or described in the Bidding Documents that a substitute or “or-equal” item of material or equipment may be furnished or used by CONTRACTOR if acceptable to ENGINEER, application for such acceptance will not be considered by ENGINEER until after the Effective Date of the Agreement. The procedure for submission of any such application by CONTRACTOR and consideration by ENGINEER is set forth in the General Conditions. ARTICLE 12 - SUBCONTRACTORS, SUPPLIERS, AND OTHERS 12.01 The identity of certain Subcontractors, Suppliers, individuals, or entities are required to be submitted to OWNER within twenty-four (24) hours after the bid opening time and date. If OWNER or ENGINEER, after due investigation, has reasonable objection to any proposed Subcontractor, Supplier, individual, or entity, OWNER may, before the Notice of Award is given, request apparent Successful Bidder to submit a substitute, in which case apparent Successful Bidder shall submit an acceptable substitute, Bidder’s Bid price will be increased (or decreased) by the difference in cost occasioned by such substitution, and OWNER may consider such price adjustment in evaluating Bids and making the contract award. 12.02 If apparent Successful Bidder declines to make any such substitution, OWNER may award the Contract to the next lowest Bidder that proposes to use acceptable Subcontractors, Suppliers, individuals, or entities. Declining to make requested substitutions will not constitute grounds for forfeiture of the Bid security of any Bidder. Any Subcontractor, Supplier, individual, or entity so listed and against which OWNER or ENGINEER makes no written objection prior to the giving of the Notice of Award will be deemed acceptable to OWNER and ENGINEER subject to revocation of such acceptable after the Effective Date of the Agreement as provided in paragraph 6.06 of the General Conditions. questions will be issued by Addenda mailed or delivered to all parties recorded by ENGINEER as having received the Bidding Documents, as well as posted online with the Complete Bidding Document. Questions must be received by the end of business day, Wednesday, August 19, 2020, in order to be answered. Only questions answered by Addenda will be binding. Oral and other interpretations or clarifications will be without legal effect. ---PAGE BREAK--- IB4 12.03 CONTRACTOR shall not be required to employ any Subcontractor, Supplier, individual, or entity against whom CONTRACTOR has reasonable objection. ARTICLE 13 - PREPARATION OF BID 13.01 The Bid form is included with the Bidding Documents. Additional copies may be obtained from the OWNER. 13.02 All blanks on the Bid form shall be completed by printing in ink or by typewriter and the Bid signed. A Bid price shall be indicated for each Bid item and alternative listed therein. 13.03 A Bid by a corporation shall be executed in the corporate name by the president or a vice-president or other corporate officer accompanied by evidence of authority to sign. The corporate seal shall be affixed and attested by the secretary or an assistant secretary. The corporate address and state of incorporation shall be shown below the signature. 13.04 A Bid by a partnership shall be executed in the partnership name and signed by a partner (whose title must appear under the signature), accompanied by evidence of authority to sign. The official address of the partnership shall be shown below the signature. 13.05 A Bid by a limited liability company shall be executed in the name of the firm by a member and accompanied by evidence of authority to sign. The state of formation of the firm and the official address of the firm must be shown below the signature. 13.06 A Bid by an individual shall show the Bidder’s name and official address. 13.07 A Bid by a joint venture shall be executed by each joint venturer in the manner indicated on the Bid form. The official address of the joint venture must be shown below the signature. 13.08 All names shall be typed or printed in ink below the signatures. 13.09 The Bid shall contain an acknowledgment of receipt of all Addenda, the numbers of which shall be filled in on the Bid form. 13.10 The address and telephone number for communications regarding the Bid shall be shown. 13.11 The Bid shall contain evidence of Bidder’s authority and qualification to do business in the state where the Project is located or covenant to obtain such qualification prior to award of the Contract. Bidder’s state contractor license number for the state of the Project, if any, shall also be shown on the Bid form. ARTICLE 14 - BASIS OF BID; EVALUATION OF BIDS 14.01 Lump Sum A. Bidders shall submit a Bid on a lump sum basis for the base Bid and include a separate price for each option described in the Bidding Documents as provided for in the Bid form. The price for each option will be the amount added or deleted from the base Bid if OWNER selects the alternate. In the evaluation of Bids, options will be applied in any order or combination as determined by the Owner. ARTICLE 15 - SUBMITTAL OF BID ---PAGE BREAK--- IB5 15.01 Each prospective Bidder is furnished one copy of the Bidding Documents with one separate unbound copy each of the Bid form. The unbound copy of the Bid form is to be completed and submitted with the Bid security and the following data: A. Attachment A Noncollusion Affidavit of Prime Bidder B. Attachment B Bidder Information 15.02 Attachment C Subcontractor Information shall be submitted within twenty-four (24) hours after the Bid opening date and time as indicated in Article 12 of these Instructions to Bidders. 15.03 A Bid shall be submitted no later than the date and time prescribed and at the place indicated in the advertisement or invitation to Bid and shall be enclosed in an opaque sealed envelope plainly marked with the Project title (and, if applicable, the designated portion of the Project for which the Bid is submitted), the name and address of Bidder, and shall be accompanied by the Bid security and other required documents. If a Bid is sent by mail or other delivery system, the sealed envelope containing the Bid shall be enclosed in a separate envelope plainly marked on the outside with the notation “BID ENCLOSED.” A mailed Bid shall be addressed to: OTSEGO COUNTY ADMINISTRATION 225 West Main, Suite 203 Gaylord, Michigan 49735 ARTICLE 16 - MODIFICATION AND WITHDRAWAL OF BID 16.01 A Bid may be modified or withdrawn by an appropriate document duly executed in the manner that a Bid must be executed and delivered to the place where Bids are to be submitted prior to the date and time for the opening of Bids. 16.02 If within 24 hours after Bids are opened any Bidder files a duly signed written notice with OWNER and thereafter demonstrates to the reasonable satisfaction of OWNER that there was a material and substantial mistake in the preparation of its Bid, that Bidder may withdraw its Bid, and the Bid security will be returned. Thereafter, if the Work is rebid, that Bidder will be disqualified from further bidding on the Work. ARTICLE 17 - OPENING OF BIDS 17.01 Bids will be opened at the time and place indicated in the advertisement or invitation to Bid and, unless obviously non-responsive, read aloud publicly. An abstract of the amounts of the base Bids and options, if any, will be made available to Bidders after the opening of Bids. ARTICLE 18 - BIDS TO REMAIN SUBJECT TO ACCEPTANCE 18.01 All Bids will remain subject to acceptance for the period of time stated in the Bid form, but OWNER may, in its sole discretion, release any Bid and return the Bid security prior to the end of this period. ARTICLE 19 - AWARD OF CONTRACT ---PAGE BREAK--- IB6 19.01 OWNER reserves the right to reject any or all Bids, including without limitation, nonconforming, nonresponsive, unbalanced, or conditional Bids. OWNER further reserves the right to reject the Bid of any Bidder whom it finds, after reasonable inquiry and evaluation, to be non-responsible. OWNER may also reject the Bid of any Bidder if OWNER believes that it would not be in the best interest of the Project to make an award to that Bidder. OWNER also reserves the right to waive all informalities not involving price, time, or changes in the Work and to negotiate contract terms with the Successful Bidder. 19.02 More than one Bid for the same Work from an individual or entity under the same or different names will not be considered. Reasonable grounds for believing that any Bidder has an interest in more than one Bid for the Work may be cause for disqualification of that Bidder and the rejection of all Bids in which that Bidder has an interest. 19.03 In evaluating Bids, OWNER will consider whether or not the Bids comply with the prescribed requirements, and such alternates, unit prices and other data, as may be requested in the Bid Form or prior to the Notice of Award. 19.04 In evaluating Bidders, OWNER will consider the qualifications of Bidders and may consider the qualifications and experience of Subcontractors, Suppliers, and other individuals or entities proposed for those portions of the Work for which the identity of Subcontractors, Suppliers, and other individuals or entities must be submitted as provided in Article 12 - Subcontractors, Suppliers and others of these Instruction to Bidders. 19.05 OWNER may conduct such investigations as OWNER deems necessary to establish the responsibility, qualifications, and financial ability of Bidders, proposed Subcontractors, Suppliers, individuals, or entities to perform the Work in accordance with the Contract Documents. 19.06 If the Contract is to be awarded, OWNER will award the Contract to the Bidder whose Bid is in the best interests of the Project. ARTICLE 20 – FORM OF AGREEMENT BETWEEN OWNER AND CONTRACTOR 20.01 Unless otherwise required in the Bidding Documents, the Agreement for the Work will be written on AIA Document A101, Standard Form of Agreement Between Owner and Contractor Where the Basis of Payment Is a Stipulated Sum. ARTICLE 21 – PERFORMANCE BOND AND PAYMENT BOND 21.01 Performance and payment bonds will not be required. ARTICLE 22 - SIGNING OF AGREEMENT 22.01 When OWNER gives a Notice of Award to the Successful Bidder, it shall be accompanied by the required number of unsigned counterparts of the Agreement with the other Contract Documents which are identified in the Agreement as attached thereto. Within 15 days thereafter, Successful Bidder shall sign and deliver the required number of counterparts of the Agreement and attached documents to OWNER. Within fifteen (15) days thereafter, OWNER shall deliver one fully signed counterpart to Successful Bidder with a complete set of the Drawings with appropriate identification. ---PAGE BREAK--- BF1 BID FORM PROJECT IDENTIFICATION: OTSEGO COUNTY ROYAL CREST MOTEL DEMOLITION DELIVER BID TO: Otsego County Administration 225 West Main, Suite 203 Gaylord, MI 49735 1.01 The undersigned Bidder proposes and agrees, if this Bid is accepted, to enter into an Agreement with OWNER in the form included in the Bidding Documents to perform all Work as specified or indicated in the Bidding Documents for the prices and within the times indicated in this Bid and in accordance with the other terms and conditions of the Bidding Documents. 2.01 Bidder accepts all of the terms and conditions of the Advertisement or Invitation to Bid and Instructions to Bidders, including without limitation those dealing with the disposition of Bid security. The Bid will remain subject to acceptance for ninety (90) calendar days after the Bid opening, or for such longer period of time that Bidder may agree to in writing upon request of OWNER. 3.01 In submitting this Bid, Bidder represents, as set forth in the Agreement, that: A. Bidder has examined and carefully studied the Bidding Documents, the other related data identified in the Bidding Documents, and the following Addenda, receipt of all which is hereby acknowledged. Addendum No. , , , , B. Bidder has visited the Site and become familiar with and is satisfied as to the general, local and Site conditions that may affect cost, progress, and performance of the Work. C. Bidder is familiar with and is satisfied as to all federal, state and local Laws and Regulations that may affect cost, progress and performance of the Work. D. Bidder has carefully studied all reports of explorations and tests of subsurface conditions at or contiguous to the Site and all drawings of physical conditions in or relating to existing surface or subsurface structures at or contiguous to the Site (except Underground Facilities). E. Bidder has obtained and carefully studied (or assumes responsibility for having done so) all additional or supplementary examinations, investigations, explorations, tests, studies and data concerning conditions (surface, subsurface and Underground Facilities) at or contiguous to the Site which may affect cost, progress, or performance of the Work or which relate to any aspect of the means, methods, techniques, sequences, and procedures of construction to be employed by Bidder, including applying the specific means, methods, techniques, sequences, and procedures of construction expressly required by the Bidding Documents to be employed by Bidder, and safety precautions and programs incident thereto. F. Bidder does not consider that any further examinations, investigations, explorations, tests, studies, or data are necessary for the determination of this Bid for performance of the Work at the price(s) bid and within the times and in accordance with the other terms and conditions of the Bidding Documents. ---PAGE BREAK--- BF2 G. Bidder is aware of the general nature of work to be performed by OWNER and others at the Site that relates to the Work as indicated in the Bidding Documents. H. Bidder has correlated the information known to Bidder, information and observations obtained from visits to the Site, reports and drawings identified in the Bidding Documents, and all additional examinations, investigations, explorations, tests, studies, and data with the Bidding Documents. I. Bidder has given ENGINEER written notice of all conflicts, errors, ambiguities, or discrepancies that Bidder has discovered in the Bidding Documents, and the written resolution thereof by ENGINEER is acceptable to Bidder. J. The Bidding Documents are generally sufficient to indicate and convey understanding of all terms and conditions for the performance of the Work for which this Bid is submitted. 4.01 Bidder further represents that this Bid is genuine and not made in the interest of or on behalf of any undisclosed individual or entity and is not submitted in conformity with any agreement or rules of any group, association, organization or corporation; Bidder has not directly or indirectly induced or solicited any other Bidder to submit a false or sham Bid; Bidder has not solicited or induced any individual or entity to refrain from bidding; and Bidder has not sought by collusion to obtain for itself any advantage over any other Bidder or over OWNER. 5.01 Bidder will complete the Work in accordance with the Contract Documents for the following price(s): ---PAGE BREAK--- BF3 Division A – Building Base Lump Sum Bid For the Otsego County Royal Crest Motel Demolition. Complete with all appurtenance, as specified herein and as shown on the plans, the Bidder agrees to perform all of the work of this Contract for the following lump sum bid price. Total Lump Sum Bid Price: Total bid amount in words Dollars and cents. A. Required Bid security B. Noncollusion Affidavit of Prime Bidder (Attachment A) C. Bidder Information (Attachment B) SUBMITTED on 2020. State Contractor License No. (If applicable) 6.01 Bidder agrees to have all work completed and ready for final payment in accordance with paragraph 14.07 of the General Conditions on or before Thursday, December 31, 2020. 7.01 The following documents are attached to and made a condition of this Bid: ---PAGE BREAK--- BF4 If Bidder is: An Individual Name (typed or printed): By: (SEAL) (Individual’s signature) Doing business as: Business address: Phone No. Fax No. A Partnership Partnership Name: (SEAL) By: (Signature of general partner attach evidence of authority to sign) Name (typed or printed): Business address: Phone No. Fax No. A Corporation Corporation Name: (SEAL) State of Incorporation: Type (General Business, Professional, Service, Limited Liability): By: (Signature attach evidence of authority to sign) Name (typed or printed): Title: (CORPORATE SEAL) Attest (Signature of Corporate Secretary) Business address: Phone No. Fax No. Date of Qualification to do business is ---PAGE BREAK--- Attachment A Noncollusion Affidavit of Prime Bidder State of: County of: , being first duly sworn, deposes and says that: He/She is the of , the Bidder that has submitted the attached Bid; He/She is fully informed respecting the preparation and contents of the attached Bid and of all pertinent circumstances respecting such Bid; Such Bid is genuine and is not a collusive or sham bid; Neither the said Bidder nor any of its officers, partners, owners agents, representatives, employees or parties in interest, including this affiant, has in any way colluded, conspired, connived or agreed, either directly or indirectly, with any other Bidder, firm, or person to submit a collusive or sham Bid in connection with the Contract for which the attached Bid has been submitted or to refrain from bidding in connection with such Contract, or has in any manner, directly or indirectly, sought by agreement, or collusion or communication or conference with any other Bidder, firm, or person to fix the price or prices in the attached bid or that of any other Bidder, or, to fix any overhead, profit, or cost element of the bid price or the bid price or prices in the attached bid or that of any other Bidder, or to secure through any collusion, conspiracy, connivance, or unlawful agreement any advantage against Bay Mills Township or any person interested in the proposed Contract. The price or prices quoted in the attached Bid are fair and proper and are not tainted by any collusion, conspiracy, connivance, or unlawful agreement on the part of the Bidder or any of its agents, representatives, owners, employees, or parties of interest, including this affiant. Signed By: (Title) Subscribed and sworn to before me this day of , 2020 My Commission Expires: NCA-1 ---PAGE BREAK--- Attachment B Bidder Information GENERAL The Bidder must complete the following: A. Active Projects - Year Began Owner Contract Price Project Description 1. 2. 3. 4. B. Completed Similar Projects - Year Began Owner Contract Price Project Description 1. 2. 3. 4. C. Bidder's approximate bonding capacity as of August 21, 2020. D. Name of Bidder's superintendent who will be responsible for the project - 1. (Two alternate names are acceptable) 1. General Experience SD-1 ---PAGE BREAK--- 123 W. Main St. Suite 200 Gaylord, MI 49735 O: [PHONE REDACTED] www.c2ae.com OTSEGO COUNTY ROYAL CREST MOTEL DEMOLITION TABLE OF CONTENTS Division Section Title Pages DIVISION 01 – GENERAL REQUIREMENTS 01410 SOIL COMPACTION AND TESTING 3 01560 SPECIAL CONTROLS 2 DIVISION 02 – EXISTING CONDITIONS 02110 SITE PREPARATION 5 02211 SITE EARTHWORK 4 02901 RESTORATION AND CLEAN-UP 2 02936 TOPSOILING AND SEEDING 4 024116 STRUCTURE DEMOLITION 8 END OF TABLE OF CONTENTS 000110 - 1 ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 01410 - 1 4/9/2020 SOILS COMPACTION AND TESTING SECTION 01410 - SOILS COMPACTION AND TESTING PART 1 GENERAL 1.01 WORK INCLUDED: The work covered by this section of the specifications consists of furnishing all plant, labor, equipment and materials in connection with SOILS COMPACTION AND TESTING. 1.02 RELATED WORK: The Contractor shall compact all bedding, backfill, fills, and embankments to the percentage of maximum unit weight specified herein. All compaction operations shall be performed utilizing suitable methods and equipment specifically designed for earth compaction. Rollers shall be of a standard design and in general shall be vibratory, rubber tire or smooth steel drum for granular materials and kneading type (sheep's foot) for non-granular materials. All operations shall be performed such that they do not damage or displace any pipes, utilities or structures. Compaction by flooding or jetting shall not be allowed. Attention is directed to SECTION 01560 - SPECIAL CONTROLS. 1.03 DEFINITIONS A. GRANULAR MATERIALS: Soils having a loss by washing of 15 percent or less. B. NON-GRANULAR MATERIALS: Soils having a loss by washing of more than 15 percent. C. LOSS BY WASHING: Materials finer than a No. 200 sieve as determined by ASTM C117. D. MAXIMUM UNIT WEIGHT: Maximum dry pounds per cubic foot at the optimum moisture content as determined by the following standard tests: 1. Modified Proctor: AASHTO 180, Method C, shall be used for granular and non-granular materials at structures as noted in Part D of the appended table. 2. Standard Proctor: AASHTO T-99 as modified by MDOT shall be used for soils having a loss by wash greater than 15%. 3. Michigan Cone: The MDOT "Method of Test for the Compaction and Density of Soils (Granular)" shall be used for granular materials. E. OPTIMUM MOISTURE CONTENT: Shall be the percent moisture of the soil at which the maximum unit weight is obtained by the above tests. F. LIFT: Shall be the vertical measure of a soil layer when measured loose. PART 2 PRODUCTS 2.01 MATERIALS: Shall be as specified herein, and as noted on the plans. The Contractor shall notify the Engineer of the source of materials at least three days prior to their use to allow for testing of samples. PART 3 EXECUTION ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 01410 - 2 7/29/2020 SOILS COMPACTION AND TESTING 3.01 COMPACTION AND TESTING A. MOISTURE CONTENT: All material shall be at or near the optimum moisture content when compacted. Unless modified by the Engineer, the allowable moisture range shall be as follows: 1. Granular soils: to above the optimum 2. Non-granular soils: to above the optimum In the event the moisture content of the material exceed these limits, the material shall be allowed to dry or be dried by discing or harrowing. In the event that the moisture content is too low to obtain the required densities when compacted, water shall be added to increase the moisture content to the optimum. B. TESTING: Moisture and in-place density tests will be made on the compacted fill by the engineer at each lift and recorded in accordance to table 0140-3. The costs of tests which meet the specifications will be paid by the Owner. The costs of failing tests will be paid by the Contractor and said costs will be deducted from sums due the Contractor. The Contractor may elect to perform additional testing at his own expense for his own purposes, however, the Engineer's decision of the suitability of materials and compliance with specifications shall be final. C. TABLE OF COMPACTION OPERATIONS AND REQUIREMENTS: The appended table lists requirements for minimum in-place densities and maximum lifts for various compaction operations, material classifications, and locations. The lift thickness, moisture content, type of equipment, number of passes, and weight and speed of equipment shall be adjusted to product the required compaction density with consistent results. D. SUBSIDENCE AND SETTLEMENT: The Contractor shall be responsible to conduct all compaction operations in such a manner to avoid objectionable soil settlement. Irrespective of compaction tests results, excessive soil settlement any resulting structure or pavement damage shall be repaired by the Contractor. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 01410 - 3 4/9/2020 SOILS COMPACTION AND TESTING TABLE OF COMPACTION OPERATIONS AND REQUIREMENTS COMPACTION OPERATION MATERIAL CLASSIFI- CATION MAX. LIFT LOOSE MEASURE MIN IN-PLACE DENSITY % MAX UNIT WEIGHT A. EMBANKMENTS: 1. General 9"-12" 95% 2. Under utility structures Granular 12" 97% BITUMINOUS SURFACE: 1. Subgrade Existing Material 9"-18" 95% 2. Aggregate Base Course As Specified 3"-6" 98% NOTES: Specific material requirements shall be as specified herein or shown on the drawings. For pipes of 8 inch O.D. and less, maximum lift shall be one-half of the pipe O.D. Material as designated on the drawings or as approved by the Engineer, with exception that frost heave material, as defined in MDOT Specification 2.08.10d may not be used in top 3 feet of embankment below subgrade. 9" for non-granular, 12" for granular materials. Depth of lift indicated is below excavation at which compaction is required provided a base course is required. If a base course is not required, compacted depth shall be 18". The maximum depth of lift for hydraulic compactors which may be allowed by the Engineer will vary depending upon the compaction equipment utilized by the Contractor. The maximum depth of lift shall not exceed 50% (percent) of the maximum compaction lift stated in the compaction equipment manufacturers data sheet, provided the Contractor can demonstrate that the required density has been achieved throughout the depth of the lift. END OF SECTION 01410 ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 01560 - 1 4/9/2020 SPECIAL CONTROLS SECTION 01560 - SPECIAL CONTROLS PART 1 GENERAL 1.01 WORK INCLUDED The work covered by this section of the specifications pertains to SPECIAL CONTROLS. 1.02 SPECIFICATIONS BY REFERENCE Where reference is made in the specifications to standards of any technical society, association, governmental agency, etc., said specifications or standards shall apply and be binding as though fully repeated therein and are to be considered as a part of these specifications. 1.03 RELATED WORK The Contractor shall conduct his work in a manner to prevent air, water, and noise pollution by establishing adequate controls during the construction operations. All controls shall be in accordance with the applicable laws of the State of Michigan. A. AIR POLLUTION: The open burning of combustible wastes from clearing and grubbing operations and of waste construction materials will be permitted only with prior approval by the City. The Contractor shall dispose of all such wastes at sanitary landfill(s) licensed by the Michigan Department of Environmental Quality. 1. Dust Control: The Contractor shall maintain all traveled areas in a safe, dust-free conditions at all times. To accomplish this, the Contractor shall remove any tracked materials such as much, dirt, etc. from construction and haul roads, furnish and apply chloride treatment to temporary roads, furnish and install temporary road patches or surface, or any other approved methods or systems. B. WATER POLLUTION: The Contractor will be required to perform all construction operations in a manner that will conform to the requirements of Act 347, Soil Erosion and Sedimentation Control Act. The Contractor shall also be required to perform all work in conformance with the requirements of Act 346, Inland Lakes and Streams. The permits for construction will be obtained by the Owner. C. NOISE POLLUTION: The Contractor shall exercise judgment in the conduct of operations which by nature result in excessive noise. All such operations shall take place during reasonable daylight periods, which are defined at 7:00 a.m. through 6:00 p.m. unless otherwise stated in the governing municipal ordinance, or authorized by the Owner. D. CONSTRUCTION DEBRIS: All construction debris shall be removed from the construction site(s) at regular intervals and disposed of at solid waste landfill(s) licensed by the Michigan Department of Environmental Quality. E. HOUSEKEEPING: The project work areas shall be maintained in a neat and clean conditions. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 01560 - 2 4/9/2020 SPECIAL CONTROLS 1.04 VEHICULAR AND PEDESTRIAN TRAFFIC CONTROL The Contractor shall be responsible for providing, installing, and maintaining vehicular and pedestrian traffic control signs, lights, and barricades in conjunction with construction operations. Vehicular traffic control measures shall be in accordance with the Michigan Manual of Uniform Traffic Control Devices. A. STREET CLOSING: No street or roadway may be closed to traffic without prior written permission of the City of Gaylord. B. EXISTING TRAFFIC CONTROL SIGNS: Existing traffic control signs which conflict with construction operations may be temporarily removed. The Contractor shall provide traffic control for the duration of the sign displacement and signs shall be replaced in the proper location immediately after construction operations adjacent to the sign locations are completed. END OF SECTION ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02110 - 1 4/9/2020 SITE PREPARATION SECTION 02110 - SITE PREPARATION PART 1 GENERAL 1.01 WORK INCLUDED The work covered by this section of the specifications consists of furnishing all plant, labor, equipment and materials in connection with SITE PREPARATION. 1.02 RELATED WORK A. REQUIREMENTS: All work shall be carried on in a neat and satisfactory manner and interference with flow of traffic shall be kept to a minimum. B. RELATED SECTIONS: Including, but not limited to: 1. SECTION 01410 - SOILS COMPACTION AND TESTING 2. SECTION 01560 - SPECIAL CONTROLS 3. SECTION 02223 - BEDDING AND BACKFILLING FOR UTILITY SYSTEMS PART 2 PRODUCTS - This section not used. PART 3 EXECUTION 3.01 CLEARING Shall consist of cutting, removing from the ground, and disposing of trees, stumps, brush, shrubs, and other vegetation occurring within the project site which interfere with excavation, embankment or clear vision, or are otherwise noted on the construction drawings to be removed and includes the preservation from injury or defacement of all vegetation and objects designated to remain. Any trees or shrubs that are designated to be saved but are damaged by the Contractor's operations shall be repaired or replaced by the Contractor, as directed by the Engineer, at not additional cost to the Owner. 3.02 TREE AND STUMP REMOVAL Shall consist of removing trees or stumps where called for on the plans or directed by the Engineer, or of removing stumps which are shown on the plans as trees occurring within the project site and shall include cutting such trees, removing their stumps and roots from the ground or chipping the stumps and properly disposing of the material. Where removal of a stump may result in damage to existing utilities, the stump shall be removed by chipping to a depth of at least one foot below the finished ground surface. Other stumps may be removed by chipping when approved by the Engineer. The Contractor shall comply with requirements of the Michigan Act 72 of the Public Acts of 1945 and requirements of the Michigan Act 72 and regulations of the Michigan Department of Agriculture in regard to Dutch Elm diseased trees. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02110 - 2 4/9/2020 SITE PREPARATION 3.03 REMOVING MISCELLANEOUS STRUCTURES Shall consist of removing pavement surface and base course, curb and gutter, sidewalk, manholes and catch basins, salvaging or disposing of the resulting materials, and backfilling the resulting excavations. A. PAVEMENT, CURB AND GUTTER, SIDEWALK REMOVAL: Shall be to existing joints or a sawed joint. The sawed joint shall be cut with a concrete saw to a depth sufficient to cut the steel or, if the concrete is unreinforced, at least 3 inches. If the concrete has been covered with bituminous material, the depth of cut shall be sufficient to cut the steel or penetrate at least 3 inches into unreinforced concrete. The use of a crane and ball type pavement breaker will not be permitted within 50 feet of the pavement or other concrete structure that is to remain in place. Sufficient removal shall be made to provide for proper grades and connections in the new work. B. MANHOLE, CATCH BASIN AND INLET REMOVAL: In removing manholes, catch basins and inlets, any live sewer connected to them shall be rebuilt and properly reconnected through the removal areas, and service shall be maintained, as directed by the Engineer, during such construction operations. Unless otherwise noted, removal of the structures shall include the cost of removing the connecting pipes or sewers. Where the existing sewer or pipes are to be abandoned in place, the existing sewer or pipe shall be bulkheaded at the trench or structure wall. The cost of the bulkhead(s) shall be included in the cost of the structure removal or abandonment. 3.04 ADJUSTING UTILITY CASTINGS AND COVERS Shall include all manholes, catch basins, valve vaults, valve boxes, etc., publicly or privately owned, which are located in the project site. All work shall be done in accordance with the structure Owner's requirements. A. MANHOLE OR CATCH BASIN CASTING: Adjusting the casting shall apply where the elevation of the casting is lowered by the height of the available adjusting brick or rings or raised to a maximum of 15 inches of brick and block adjustment. This adjustment shall be done by one of the following methods: 1. Masonry Adjustment: Existing castings shall be adjusted to the proper elevation by removing the castings, and setting them to the required elevation by supporting them on a concrete collar or on masonry, so constructed as to hold them firmly in place. The adjacent pavement, curb, or curb and gutter shall be replaced to the original elevation, conditions and kind of construction, unless otherwise provided. 2. Adjusting Rings: Existing covers may be adjusted to the proper elevation by inserting an Engineer approved, variable adjustable casting into the existing frame. The adjustable casting shall be capable of diameter adjustment as well as height adjustment. B. WATER VALVE BOXES: Shall be adjusted by chipping sufficient adjacent pavement or other material, adjusting the casting, and replacing pavement or other material. Water valve boxes which cannot be adjusted properly shall be replaced with a new screw type adjustable valve box to be furnished by the Owner and installed by the Contractor. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02110 - 3 4/9/2020 SITE PREPARATION C. MONUMENT BOXES: Shall be adjusted to the proper elevation by placing an approved cast iron ring to support the cover at the correct elevation, or by removing or chipping sufficient adjacent pavement or other material to remove the casting, raising it to the proper elevation, and supporting it on Class B concrete. 3.05 REMOVE AND REPLACE MANHOLE OR CATCH BASIN CASTINGS Shall be where called for on the plans or in the specifications. The Contractor shall remove existing castings, install new castings of the style noted on the plans or in the specifications, and adjust the new castings to the proper elevation. The old castings remain the property of the Owner and shall be delivered by the Contractor to a location designated by the Owner. 3.06 RECONSTRUCTING MANHOLES OR CATCH BASINS Reconstruction of manholes or catch basins shall apply to where castings cannot be adjusted to the proper elevation due to the absence or present of sufficient adjusting brick or rings on the manhole structure. The manhole or catch basin structure shall be constructed by one of the following methods: A. Precast Structure: If the manhole is constructed of precast concrete sections, the top section(s) shall be removed and replaced with a precast concrete section(s) of such height as to allow for the proposed casting adjustment. B. Manhole Block or Brick: If the manhole is constructed of manhole block or brick, remove sufficient rows of block or brick in order to construct the manhole to the proper grade for casting adjustment. 3.07 BITUMINOUS SURFACE REMOVAL Shall consist of removing a bituminous surface from a rigid base or removing a bituminous surface from an aggregate base without the removal of the aggregate base. The method of removing the bituminous surface shall be approved by the Engineer. The removal of a bituminous surface and the aggregate base will be classed as Earth Excavation, except when the bituminous surface is more than 5 inches in thickness. The removal of bituminous surface will be paid for as Removing Pavement. 3.08 DISPOSAL OF MATERIALS Materials salvaged during the construction of the project shall become the property of the Contractor unless otherwise shown on the plans or in the proposal. Materials reserved for use by the Owner shall be removed without damage to the material and stored outside the limits of construction at the location and in the manner approved by the Owner. Materials that become the property of the Contractor shall be removed from the project before acceptance of the project. Broken concrete which is matted together by steel reinforcement and all other waste material shall be disposed in conformance with SECTION 01560 - SPECIAL CONTROLS. 3.09 RESTORATION OF DISTURBED STRUCTURES Existing structures, including pavement, curb and gutter, sidewalk and other miscellaneous structures, disturbed or damaged as a result of site preparation operations shall be restored or replaced to their original condition by the Contractor at no additional cost to the Owner. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02110 - 4 4/9/2020 SITE PREPARATION 3.10 BACKFILLING All trenches, holes and pits resulting from the breaking down or removal of foundations and miscellaneous structures within the project site shall be backfilled in conformance with SECTION 02223 Paragraph 2.02 - BACKFILL MATERIAL and compacted in conformance with SECTION 01410 - SOILS COMPACTION AND TESTING. END OF SECTION ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02110 - 5 4/9/2020 SITE PREPARATION THIS PAGE INTENTIONALLY LEFT BLANK ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02211 - 1 4/9/2020 SITE EARTHWORK SECTION 02211 - SITE EARTHWORK PART 1 GENERAL 1.01 WORK INCLUDED The work covered by this section of the specifications consists of furnishing all plant, labor, equipment, and materials in connection with SITE EARTHWORK. 1.02 RELATED WORK A. REQUIREMENTS: All work shall be carried on in a neat and satisfactory manner and interference with flow of traffic shall be kept to a minimum. B. RELATED SECTIONS: Including, but not limited to: 1. SECTION 01410 - SOILS COMPACTION AND TESTING 2. SECTION 01560 - SPECIAL CONTROLS C. COORDINATION WITH OTHER CONTRACTORS: Certain portions of the work may require completion of construction under other contracts prior to commencing work under this section. The Contractor shall coordinate his work and schedule with other contractors to result in complying with the contract completion date. PART 2 PRODUCTS 2.01 SUBBASE AND SUBGRADE UNDERCUTTING Shall conform to MDOT Granular Material Class II. 2.02 EMBANKMENT MATERIAL Materials utilized for embankment construction shall be approved by the Engineer. In general, any natural material which can be compacted to the required density, contains no organic material, and has a maximum unit weight of at least 95 pounds per cubic foot may be used. Materials containing more than 50 percent silt or any frozen material will not be allowed. Silt is defined as material having a particle size of 0.074 to 0.0005 mm. PART 3 EXECUTION 3.01 SITE EARTHWORK Work performed under this section shall consist of constructing earth grades by excavating soil or rock and by placing embankments of fills. This work shall include the salvaging and stockpiling of selected material, disposing of surplus or unsuitable material, trimming the earth grade, and maintaining the work in a finished condition until acceptance. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02211 - 2 4/9/2020 SITE EARTHWORK A. SITE PREPARATION: Undesirable material shall be removed from the grading limits and salvaged or disposed of as specified herein or as shown on the plans. 1. Removing Topsoil: Before removing topsoil, all vegetation of a height greater than one foot shall be reduced to a height of approximately 6 inches and all such vegetation and all brush, stones, rocks, and any other objectionable litter or foreign materials shall be removed from the site and disposed of in conformance with SECTION 01560 - SPECIAL CONTROLS. Equipment and methods of operations shall be such as to avoid the lifting of subsoil. If soil or weather conditions are unsuitable, the Contractor shall cease and resume removing topsoil upon orders from the Engineer. a. Embankment Areas: Where the embankment is to be 5 feet or less in height to the pavement surface, the topsoil shall be stripped from the area within limits of 1 on 1 slopes spreading outward from the finished shoulders. For embankments upon which a structure is to be built, the topsoil shall be stripped from an area within limits of 1 on 1 slopes spreading outward in all directions from the bottom of structure footing. The depth of the topsoil to be removed shall be as shown on the plans or as directed by the Engineer. b. Cut Areas: Topsoil shall be removed within the grading limits. 2. Salvaging Topsoil: The topsoil may be stockpiled outside the limits of construction or used as shown on the plans or as directed by the Engineer. Topsoil stockpiles shall be located and shaped so as to avoid placing around trunks and over root areas of trees to be preserved or in drainage courses. The topsoil shall be kept separate from other excavated material. 3. Salvaging Other Materials: If provided on the plans or in the proposal, or if directed by the Engineer, old road surfacing of gravel, crushed stone, or selected excavated materials, shall be removed from the designated areas for use in such items as earth shoulders, salvaged approaches, temporary roadway surfacing or other items requiring the use of such materials. Reasonable care shall be exercised in removing and handling the designated materials to prevent incorporation of foreign or undesirable material. When the salvaged material cannot be placed directly in the contemplated construction, the material shall be stored in stockpiles. B. SUBGRADE UNDERCUTTING: Including backfilling, shall be performed to replace material susceptible to frost heaving or differential frost action and unstable soil conditions, as determined by the Engineer. Removing topsoil will not be part of subgrade undercutting. Excavation below subgrade in cut sections, at the transition from cut to fill sections, and any excavation other than peat excavation that may be required below the topsoil in fill sections will be classified as Subgrade Undercutting. 1. Limits of Subgrade Undercutting: After the subgrade has been constructed to the approximate grade, the Engineer will inspect the grade to determine if any subgrade undercutting is required and determine the limits of such undercutting. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02211 - 3 7/29/2020 SITE EARTHWORK Where shallow fills are to be placed, the Engineer will inspect the fill area before any embankment is placed and determine the limits of the subgrade undercutting if any, before placing any embankment. All deposits of frost heave material within lines 2 feet outside the proposed surface, shall be removed to a depth as directed by the Engineer. Subgrade undercutting shall be performed within the limits established by the Engineer, and the excavated material shall become the property of the Contractor. 2. Backfilling of Subgrade Undercut Sections: Undercut sections shall be backfilled to the subgrade elevation with MDOT Granular Material Class II. The degree of compaction shall be in conformance with SECTION 01410 - SOILS COMPACTION AND TESTING. C. WASTE MATERIAL AND DEBRIS: Of whatever nature shall be removed from the site at the Contractor's expense. 1. Excess Material: From excavation operations which is not required for fill or backfill may be spread at the site in spoil areas as shown on the plans. 2. Hazardous Waste: Should such waste material as defined by EGLE be encountered during construction, the Contractor shall immediately notify the Engineer. Removal and disposal of such materials from the site shall be considered a changed condition. D. CONSTRUCTING EMBANKMENTS: Shall be done with approved materials as specified in paragraph 2.02. In addition, embankments shall be constructed with the maximum allowable lift and degree of compaction conforming to SECTION 01410 - SOILS COMPACTION AND TESTING. In general, embankment construction at outside air temperatures below 35oF. will not be allowed. If embankment construction is allowed under such conditions, the Contractor shall exclude frozen material from any portion of the embankment. Any frozen material on a partially completed fill shall be removed and disposed of prior to placing additional fill on the embankment. E. BORROW: Material secured from locations outside the project site will be considered borrow excavation. The Contractor shall perform all work and provide all materials and equipment necessary to excavate, haul and place the borrow material. The Contractor will be held liable for all damages caused by his hauling operations and will be required to pay for such damages. F. PREPARATION OF SUBGRADE SURFACE: Where the natural soils form the subbase, the subgrade shall be scarified and blended to a minimum depth of 6 inches to obtain uniformity across all lines of change in soil types. The subgrade shall be compacted in conformance with SECTION 01410 - SOILS COMPACTION AND TESTING. END OF SECTION ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02211 - 4 4/9/2020 SITE EARTHWORK THIS PAGE INTENTIONALLY LEFT BLANK ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02901-1 4/9/2020 RESTORATION AND CLEANUP SECTION 02901 - RESTORATION AND CLEAN-UP PART 1 GENERAL 1.01 WORK INCLUDED The work covered by this section of the specifications consists of furnishing all plant, labor, equipment, and materials in connection with RESTORATION AND CLEAN-UP. 1.02 RELATED WORK A. REQUIREMENTS: The Contractor shall restore all areas disturbed by his construction operations to a condition equal to or better than the existing prior to construction and shall clean-up and haul away all construction debris and litter caused by his operation. B. RELATED SECTIONS: Including, but not limited to: 1. SECTION 01560 - SPECIAL CONTROLS 2. SECTION 02231 - AGGREGATE BASE COURSE 3. SECTION 02513 - BITUMINOUS LEVELING/SURFACE COURSES 4. SECTION 02525 - CONCRETE CURB AND GUTTER 5. SECTION 02528 - CONCRETE SIDEWALK 6. SECTION 02936 - TOPSOILING AND SEEDING 7. SECTION 02938 - SODDING 8. SECTION 03001 - CONCRETE 1.03 CLEAN-UP General rough grading and clean-up shall follow immediately after installation of utilities so that no more than 1,000 lineal feet of cleanup shall remain to be completed at any time during construction. The Contractor shall remove all equipment, debris, and waste material from the construction site and material and equipment storage areas prior to final inspection and after restoration. PART 2 PRODUCTS - This section not used. PART 3 EXECUTION 3.01 PERMANENT PAVEMENT All street surfaces, driveways, curb and gutter and sidewalks removed or disturbed by construction operations shall be restored to their original condition, or better unless otherwise shown on the plans and/or details. Street base course and surfacing shall conform with SECTION 02231 - AGGREGATE BASE COURSE and SECTION 02513 - BITUMINOUS LEVELING/SURFACE COURSE. All concrete for restoration shall be air entrained Class A concrete conforming to SECTION 03001 - CONCRETE or SECTION 03300 - STRUCTURAL CONCRETE. All street, driveway and sidewalk crossings shall be restored immediately after completion of the crossing to ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 02901-2 4/9/2020 RESTORATION AND CLEANUP accommodate vehicular and pedestrian traffic. Temporary patching of pavements of bituminous base will be required in the event of final restoration is not anticipated within 5 days of the crossing construction. 3.02 MISCELLANEOUS STRUCTURES Mail boxes, fences, culverts, ditches and other existing structures shall be resorted or replaced, as required, to original or better condition in a manner acceptable to the Engineer. 3.03 BOUNDARY MARKER REPLACEMENT The Contractor shall have replaced by a Registered Land Surveyor, at his own expense, all section corners, property corners or boundary markers of any type or material that may be damaged or destroyed by his construction operation. 3.04 SEEDING Lawn areas disturbed by the Contractor's construction operations shall be topsoiled and seeded in conformance with Section 02936, Topsoiling and Seeding. Prior to topsoil or seeding, rocks, sticks, roots larger than 2" in diameter, and other debris shall be removed from areas to be seeded. In general, lawn areas shall be all areas back of the curb unless otherwise designated on the plans or noted in the specifications. 3.05 SODDING Areas designated on the drawings to be sodded shall be sodded in conformance with Section 02938, Sodding. The Contractor at his option may sod areas required or designated to be seeded. 3.06 PLANTINGS Shrubs, other plantings, and trees removed during construction, other than those specifically designated to be removed, shall be replaced with new material equal to that removed. Replacement shall be with approved stock from a State-inspected nursery and shall carry a one year replacement guarantee. END OF SECTION ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project#190040 02936-1 4/10/2020 TOPSOILING AND SEEDING SECTION 02936 - TOPSOILING AND SEEDING PART 1 GENERAL 1.01 WORK INCLUDED: The work covered by this section of the specifications consists of furnishing all plant, labor, equipment, and materials in connection with TOPSOILING AND SEEDING. 1.02 RELATED WORK A. REQUIREMENTS: The Contractor shall topsoil, grade, fertilize, seed and mulch lawn and other designated areas disturbed by construction operations. Attention is directed to Section 01560 - SPECIAL CONTROLS. PART 2 PRODUCTS 2.01 TOPSOIL: Any topsoil necessary to complete the work over and above the topsoil stockpiled during construction operations shall be furnished by the Contractor. Topsoil shall be free from brush, objectionable weeds or other litter. Additional topsoil shall consist of loose, friable loamy topsoil without admixture of subsoil or refuse, and approved by the Engineer prior to spreading. 2.02 SEED: All seed to be used shall be labeled in accordance with the U.S. Department of Agriculture Rules and Regulations under the Federal Seed Act and shall be in accordance with the State seed rules and regulations. Seed certificates or tags from the seed bags shall be submitted to the Engineer. Seed shall conform to MDOT Section 816 for roadside and Class A mixtures. 2.03 FERTILIZERS: Chemical fertilizer shall be standard commercial grade with packaging clearly marked in accordance with applicable Federal laws. Bulk fertilizer may be used when certified delivery slips are furnished by the Contractor. 2.04 MULCH BLANKET: A straw erosion control blanket shall be used in all seeded areas and shall meet the approval of the Engineer. The mulch blanket shall be Rhino Erosion King straw blanket by Rhino Seed & Landscape Supply, or similar approved equal. PART 3 EXECUTION 3.01 PREPARATION OF SEED BED A. GRADING: Grades on areas to be seeded shall be maintained in a true and even condition. Where the grades are not defined, they shall be established by the Contractor to blend with existing adjacent grades without irregularities and shall provide for proper drainage. B. FINISHING: All large clogs, lumps, and rocks over 1" in diameter, brush, roots, stumps, litter, or other foreign matter shall be raked up and removed from the area and disposed of by the Contractor. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project#190040 02936-2 4/10/2020 TOPSOILING AND SEEDING C. PLACING TOPSOIL: The surface of the subgrade immediately prior to being covered with topsoil shall be raked or otherwise loosened to a depth of not less than The topsoil shall be evenly spread over the areas by blade graders, or other approved methods, to a depth of at least 3 inches. Any irregularities in the surface resulting from topsoiling or other operations shall be corrected in order to prevent the formation of low places and pockets where water will stand. Topsoil shall not be placed when the subgrade is in a condition detrimental to seeding or proper grading. C. APPLICATION OF FERTILIZER: Fertilizer shall be distributed uniformly over the areas to be seeded at a rate which will provide 240 pounds per acre of chemical fertilizer nutrients, in equal proportions of nitrogen, phosphoric acid and potash and shall be incorporated into the soil to a depth of at least 3 inches by Brillion seeding or other acceptable methods. D. CLEAN-UP: After completion of the above operations, the surface shall be cleared of stones, roots, brush, wire, grade stakes and other objects that might be a hindrance to maintenance operations. 3.02 SEEDING A. SEEDING REQUIREMENTS: MDOT Class A seed mixture shall be used on all lawn areas. MDOT Roadside seed mixture shall be used for areas disturbed by construction and not defined as lawn area. No seeding shall be done until the Engineer has inspected the seed containers. B. SEEDING: Prior to seeding, the topsoil shall be disked, harrowed, or otherwise loosened to a depth of 3 inches minimum. Seed shall be placed by the Brillion seeding method or hyrdoseeding, unless approved otherwise. Seeding shall be accomplished between the period of April 15 into the fall as long as weather conditions permit seed bed preparation. Seeding rate shall be Class A: 220#/A, Roadside: 200#/A. C. COMPACTING: Immediately after seeding, the entire area shall be compacted by means of a cultipacker, roller or approved equipment weighing 60 to 90 pounds per linear foot of roller. The final rolling shall be a right angles to slopes to prevent water erosion. 3.03 MULCHING: Mulch blanket shall be applied over seed and fertilizer using staples, wood pegs, or other acceptable methods per the blanket manufacturer’s recommendations. 3.04 ESTABLISHMENT OF SEEDED AREAS: The Contractor shall be responsible for the proper care of the seeded area during the period when the grass is becoming established, and shall be responsible for a total grass cover. The acceptance must be demonstrated by the results. A. WATERING: The seed bed for lawn areas shall be given one watering immediately after placement sufficient to wet at least two inches of the seed bed. Additional watering at the same rate shall be accomplished at five day intervals for a period of five weeks, or a total of eight applications of water. In case of rain, the Contractor shall obtain approval of the Engineer to omit an application of water or re-schedule the watering interval. After the five week period, maintenance of the seeded areas will be assumed by the Owner or respective property owners. The Contractor will not be held responsible for any mowing of seeded areas. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project#190040 02936-3 4/10/2020 TOPSOILING AND SEEDING B. REPAIR: If any time prior to the end of the five week period during which the Contractor is responsible for watering of the seeded areas, the ground is displaced due to subsidence, or sliding or gullying on sloped areas, the Contractor shall repair and re-seed the damaged areas at his expense. C. WEEDS: After the grass has become established and it appears to have more than 10% weeds, the Contractor shall spray with an approved herbicide. END OF SECTION ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project#190040 02936-4 4/10/2020 TOPSOILING AND SEEDING THIS PAGE INTENTIONALLY LEFT BLANK ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 4/9/2020 024116 - 1 STRUCTURE DEMOLITION SECTION 024116 - STRUCTURE DEMOLITION PART 1 - GENERAL 1.1 RELATED DOCUMENTS A. Drawings and general provisions of the Contract, including General and Supplementary Conditions and Division 01 Specification Sections, apply to this Section. 1.2 SUMMARY A. Section Includes: 1. Demolition and removal of buildings. 2. Removing below-grade construction. 3. Disconnecting, capping or sealing, and removing site utilities. 4. All demolished items become the property of the Contractor. B. Related Requirements: 1. Section 02110 "Site Preparation" for site clearing and removal of above- and below-grade site improvements not part of building demolition. 2. Section 02211 “Site Earthwork” for other project requirements. 3. Drawing sheets for additional project requirements. 1.3 DEFINITIONS A. Remove: Detach items from existing construction and dispose of them off-site unless indicated to be salvaged. B. Remove and Salvage: Detach items from existing construction, in a manner to prevent damage, and store for Contractor removal and disposal from the site. Include fasteners or brackets needed for reattachment elsewhere. 1.4 MATERIALS OWNERSHIP A. Unless otherwise indicated, demolition waste becomes property of Contractor. B. Historic items, relics, antiques, and similar objects including, but not limited to, cornerstones and their contents, commemorative plaques and tablets, and other items of interest or value to Owner that may be uncovered during demolition remain the property of Owner. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 4/9/2020 024116 - 2 STRUCTURE DEMOLITION 1. Carefully salvage in a manner to prevent damage and return to Owner. 1.5 PREINSTALLATION MEETINGS A. Predemolition Conference: Conduct conference at Royal Crest Motel, Otsego County. 1. Inspect and discuss condition of construction to be demolished. 2. Review structural load limitations of existing structures. 3. Review and finalize building demolition schedule and verify availability of demolition personnel, equipment, and facilities needed to make progress and avoid delays. 4. Review and finalize protection requirements. 5. Review procedures for noise and dust control. 6. Review procedures for protection of adjacent buildings. 7. Review items to be salvaged and returned to Owner. 1.6 INFORMATIONAL SUBMITTALS A. Qualification Data: For refrigerant recovery technician. B. Engineering Survey: See Section 3.1.C this specification section for information. C. Proposed Protection Measures: Submit report, including Drawings, that indicates the measures proposed for protecting individuals and property for environmental protection. Indicate proposed locations and construction of barriers. 1. Adjacent Buildings: Detail special measures proposed to protect adjacent buildings to remain including means of egress from those buildings. D. Schedule of Building Demolition Activities: Indicate the following: 1. Detailed sequence of demolition work, with starting and ending dates for each activity. 2. Temporary interruption of utility services. 3. Shutoff and capping of utility services. E. Predemolition Photographs or Video: Show existing conditions of adjoining construction and site improvements, including finish surfaces, that might be misconstrued as damage caused by salvage and demolition operations. Comply with Section 013233 "Photographic Documentation." Submit before the Work begins. F. Statement of Refrigerant Recovery: Signed by refrigerant recovery technician responsible for recovering refrigerant, stating that all refrigerant that was present was recovered and that recovery was performed according to EPA regulations. Include name and address of technician and date refrigerant was recovered. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 024116 - 3 4/9/2020 STRUCTURE DEMOLITION 1.7 CLOSEOUT SUBMITTALS A. Inventory: Submit a list of items that have been removed and salvaged. 1.8 QUALITY ASSURANCE A. Refrigerant Recovery Technician Qualifications: Certified by EPA-approved certification program. 1.9 FIELD CONDITIONS A. Buildings to be demolished will be vacated and their use discontinued before start of the Work. B. Buildings immediately adjacent to demolition area will be occupied. Conduct building demolition so operations of occupied buildings will not be disrupted. 1. Provide not less than 72 hours' notice of activities that will affect operations of adjacent occupied buildings. 2. Maintain access to existing walkways, exits, and other facilities used by occupants of adjacent buildings. a. Do not close or obstruct walkways, exits, or other facilities used by occupants of adjacent buildings without written permission from authorities having jurisdiction. C. Conditions existing at time of inspection for bidding purpose will be maintained by Owner as far as practical. 1. Before building demolition, Owner will remove the following items: a. All items have been removed by the Owner. D. Hazardous Materials: Present in buildings and structures to be demolished. A report on the presence of hazardous materials is in the Appendix for review and use. Examine report to become aware of locations where hazardous materials are present. 1. Hazardous material remediation is specified elsewhere in the Contract Documents. 2. Do not disturb hazardous materials or items suspected of containing hazardous materials except under procedures specified by the EPA, Michigan EGLE and all other regulations. 3. Owner will provide material safety data sheets (if available) for materials that are known to be present in buildings and structures to be demolished because of building operations or processes performed there. E. On-site storage or sale of removed items or materials is not permitted. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan 1.10 COORDINATION A. Arrange demolition schedule so as not to interfere with operations of adjacent occupied buildings. PART 2 - PRODUCTS 2.1 PERFORMANCE REQUIREMENTS A. Regulatory Requirements: Comply with governing EPA notification regulations before beginning demolition. Comply with hauling and disposal regulations of authorities having jurisdiction. B. Standards: Comply with ANSI/ASSE A10.6 and NFPA 241. 2.2 SOIL MATERIALS A. Satisfactory Soils: Comply with requirements in Section 02211 " Site Earthwork" PART 3 - EXECUTION 3.1 EXAMINATION A. Verify that utilities have been disconnected and capped before starting demolition operations. B. Review Project Record Documents of existing construction or other existing condition and hazardous material information provided by Owner. Owner does not guarantee that existing conditions are same as those indicated in Project Record Documents. C. The Demolition Contractor shall engage a Professional Engineer to perform an engineering survey of the condition of the existing buildings to be demolished and adjacent off-site buildings to remain, prior to demolition to determine whether removing any element might result in structural deficiency or unplanned collapse of any portion of the structures or adjacent structures (off-site that will remain) during demolition operations. D. Steel Tendons: Locate tensioned steel tendons and include recommendations for de-tensioning. E. Verify that hazardous materials have been remediated before proceeding with building demolition operations. F. Inventory and record the condition of items to be removed and salvaged. C2AE©Project# 190040 024116 - 4 4/9/2020 STRUCTURE DEMOLITION ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan 3.2 PREPARATION A. Refrigerant: Before starting demolition, remove refrigerant from mechanical equipment according to 40 CFR 82 and regulations of authorities having jurisdiction. B. Salvaged Items: Comply with the following: 1. Clean salvaged items of dirt and demolition debris. 2. Pack or crate items after cleaning. Identify contents of containers. 3. Store items in a secure area until delivery to Owner. 4. Transport items to storage area designated by Owner. 5. Protect items from damage during transport and storage. 3.3 UTILITY SERVICES AND MECHANICAL/ELECTRICAL SYSTEMS A. Existing Utilities to be Disconnected: Locate, identify, disconnect, and seal or cap off utilities serving buildings and structures to be demolished. 1. Owner will arrange to shut off utilities when requested by Contractor. 2. Arrange to shut off utilities with utility companies. 3. If removal, relocation, or abandonment of utility services will affect adjacent occupied buildings, then provide temporary utilities that bypass buildings and structures to be demolished and that maintain continuity of service to other buildings and structures. 4. Do not start demolition work until utility disconnecting and sealing have been completed and verified in writing. 3.4 PROTECTION A. Existing Facilities: Protect adjacent walkways, loading docks, building entries, and other building facilities during demolition operations. Maintain exits from existing buildings. B. Temporary Shoring: Provide and maintain interior and exterior shoring, bracing, or structural support to preserve stability and prevent unexpected movement or collapse of construction being demolished. 1. Strengthen or add new supports when required during progress of demolition. C. Existing Utilities to Remain: Maintain utility services to remain and protect from damage during demolition operations. 1. Do not interrupt existing utilities serving adjacent occupied or operating facilities unless authorized in writing by Owner and authorities having jurisdiction. 2. Provide temporary services during interruptions to existing utilities, as acceptable to Owner and authorities having jurisdiction. C2AE©Project# 190040 024116 - 5 4/9/2020 STRUCTURE DEMOLITION ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 024116 - 6 4/9/2020 STRUCTURE DEMOLITION a. Provide at least 72 hours' notice to occupants of affected buildings if shutdown of service is required during changeover. D. Temporary Protection: Erect temporary protection, such as walks, fences, railings, canopies, and covered passageways, where required by authorities having jurisdiction and as indicated. Comply with requirements in Section 015000 "Temporary Facilities and Controls." 1. Protect adjacent buildings and facilities from damage due to demolition activities. 2. Protect existing site improvements, appurtenances, and landscaping to remain. 3. Erect a plainly visible fence around drip line of individual trees or around perimeter drip line of groups of trees to remain. 4. Provide temporary barricades and other protection required to prevent injury to people and damage to adjacent buildings and facilities to remain. 5. Provide protection to ensure safe passage of people around building demolition area and to and from occupied portions of adjacent buildings and structures. 6. Protect walls, windows, roofs, and other adjacent exterior construction that are to remain and that are exposed to building demolition operations. 7. Erect and maintain dustproof partitions and temporary enclosures to limit dust, noise, and dirt migration to occupied portions of adjacent buildings. E. Remove temporary barriers and protections where hazards no longer exist. Where open excavations or other hazardous conditions remain, leave temporary barriers and protections in place. 3.5 DEMOLITION, GENERAL A. General: Demolish indicated buildings completely. Use methods required to complete the Work within limitations of governing regulations and as follows: 1. Do not use cutting torches until work area is cleared of flammable materials. Maintain portable fire-suppression devices during flame-cutting operations. 2. Maintain fire watch during and for at least 48 hours after flame-cutting operations. 3. Maintain adequate ventilation when using cutting torches. 4. Locate building demolition equipment and remove debris and materials so as not to impose excessive loads on supporting walls, floors, or framing. B. Site Access and Temporary Controls: Conduct building demolition and debris-removal operations to ensure minimum interference with roads, streets, walks, walkways, and other adjacent occupied and used facilities. 1. Do not close or obstruct streets, walks, walkways, or other adjacent occupied or used facilities without permission from Owner and authorities having jurisdiction. Provide alternate routes around closed or obstructed trafficways if required by authorities having jurisdiction. 2. Use water mist and other suitable methods to limit spread of dust and dirt. Comply with governing environmental-protection regulations. Do not use water when it may damage adjacent construction or create hazardous or objectionable conditions, such as ice, flooding, and pollution. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 024116 - 7 4/9/2020 STRUCTURE DEMOLITION C. Explosives: Use of explosives is not permitted. 3.6 DEMOLITION BY MECHANICAL MEANS A. Proceed with demolition of structural framing members systematically, from higher to lower level. Complete building demolition operations above each floor or tier before disturbing supporting members on the next lower level. B. Remove debris from elevated portions of the building by chute, hoist, or other device that will convey debris to grade level in a controlled descent. 1. Remove structural framing members and lower to ground by method suitable to minimize ground impact and dust generation. C. Below-Grade Construction: Demolish foundation walls and other below-grade construction. 1. Remove below-grade construction, including basements, foundation walls, pools, and footings completely. D. Existing Utilities: Demolish and remove existing utilities and below-grade utility structures. E. Hydraulic Elevator Systems: Demolish and remove elevator system, including cylinder, plunger, well assembly, steel well casing and liner, oil supply lines, and tanks. 3.7 SITE RESTORATION A. Below-Grade Areas: Completely fill below-grade areas and voids resulting from building demolition operations according to backfill requirements in Section 02211 "Site Earthwork." B. Site Grading: Uniformly rough grade area of demolished construction to a smooth surface, free from irregular surface changes. Provide a smooth transition between adjacent existing grades and new grades. 3.8 REPAIRS A. repair damage to adjacent buildings caused by demolition operations. 3.9 DISPOSAL OF DEMOLISHED MATERIALS A. Remove demolition waste materials from Project site and dispose of them in an EPA-approved construction and demolition waste landfill acceptable to authorities having jurisdiction. 1. Do not allow demolished materials to accumulate on-site. 2. Remove and transport debris in a manner that will prevent spillage on adjacent surfaces and areas. ---PAGE BREAK--- Royal Crest Motel Demolition Otsego County, Michigan C2AE©Project# 190040 024116 - 8 4/9/2020 STRUCTURE DEMOLITION B. Do not burn demolished materials. 3.10 CLEANING A. Clean adjacent structures and improvements of dust, dirt, and debris caused by building demolition operations. Return adjacent areas to condition existing before building demolition operations began. 1. Clean roadways of debris caused by debris transport. END OF SECTION 024116 ---PAGE BREAK--- S. WISCONSIN W. FOURTH ST. S. ILLINOIS AVE. SHADOW LANE WOODHAVEN COURT BORDON DRIVE BORDON DRIVE NOIROT STREET VAN TYLE DICKERSON RD. W. EIGHTH ST. TED DRIVE W. MAIN ST. (M-32) MANKOWSKI ROAD IOWA ST. WEST ST. W. PETOSKEY ST. W. STEWART ST. W. JENSON ST. S. INDIANA AVE. S. CENTER AVE. S. ELM AVE. S. OAK AVE. E. SEVENTH ST. E. SIXTH ST. E. FIFTH ST. IVE ELKVIEW DETROIT & MACKINAC RAILWAY S. OTSEGO AVE. W. SIXTH ST. W. THIRD ST. S. CENTER AVE. W. MAIN ST. (M-32) S. OTSEGO AVE. MICHIGAN AVE. E. MAIN E. MITCHE E. SHELDON N. CENTER AVE. MILL ST. E. PETOSK W. PETOSKEY ST. W. JENSON ST. W. STEWART ST. W. MITCHELL ST. S. COURT AVE. S. COURT AVE. W. SHELDON ST. CARPENTER ST. WEST ST. E. FELSHA W. SEVENTH ST. S. COURT AVE. GRANDVIEW BLVD. COMMERCE BLVD. W. FIRST ST. W. SECOND ST. W. FIFTH ST. GORNICK AVE W. FOURTH ST. N. ELM AVE. N. OAK AVE. W. SHELDON ST. N. OHIO AVE. N. WISCONSIN AVE. N. ILLINOIS AVE. N. INDIANA AVE. W. SECOND ST. N. COURT AVE. N. OTSEGO AVE. S. WISCONSIN WE RECYCLE SHEET REVISIONS www.c2ae.com architecture · engineeri REV DESCRIPTION DATE PROJ. DATE: BLACK WHITE THE BAR BELOW SHOWS GRAYSCALE FROM WHITE TO SOLID BLACK 190040 APRIL 2020 ISSUED FOR BIDS . GAYLORD, MICHIGAN OTSEGO COUNTY: ROYAL CREST MOTEL DEMOLITION 1 of 2 CONSTRUCTION NOTES AND MISCELLANEOUS INFORMATION FOR CONSTRUCTION PLANS APRIL 2020 ROYAL CREST MOTEL DEMOLITION OTSEGO COUNTY GAYLORD, MICHIGAN ---PAGE BREAK--- WE RECYCLE SHEET REVISIONS www.c2ae.com architecture · engineeri REV DESCRIPTION DATE PROJ. DATE: BLACK WHITE THE BAR BELOW SHOWS GRAYSCALE FROM WHITE TO SOLID BLACK 190040 APRIL 2020 ISSUED FOR BIDS . GAYLORD, MICHIGAN OTSEGO COUNTY: ROYAL CREST MOTEL DEMOLITION DEMOLITION KEY 2 of 2 PROPOSED DEMOLITION PLAN, NOTES AND DETAILS Know what'sbelow. before you dig. Call R ---PAGE BREAK--- APPENDIX A Asbestos Survey & Lead Based Paint Sampling ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- APPENDIX B Phase II Environmental Site Assessment ---PAGE BREAK--- Sagasser & Associates, Inc. ENVIRONMENTAL ASSESSMENT AND CONSULTING SERVICES 699 South Wisconsin Avenue ♦ Gaylord, Michigan 49735 ♦ [PHONE REDACTED] ♦ Fax: [PHONE REDACTED] ♦ e-mail: [EMAIL REDACTED] Phase II Environmental Site Assessment Former Royal Crest Motel 803 South Otsego Avenue Gaylord, Michigan PREPARED BY Sagasser & Associates, Inc. 699 South Wisconsin Gaylord, Michigan Project #31902 December 2019 ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 Former Royal Crest Motel - Gaylord, Michigan TABLE OF CONTENTS 1.0 INTRODUCTION 1 1.1 PURPOSE 1 1.2 TERMS & CONDITIONS 1 1.3 SCOPE OF WORK 1 2.0 SITE DESCRIPTION 2 3.0 PHASE I ENVIRONMENTAL SITE ASSESSMENT 2 4.0 PHASE II ENVIRONMENTAL SITE ASSESSMENT ACTIVITIES & ANALYTICAL RESULTS 2 5.0 FINDINGS 4 6.0 CLOSING 4 7.0 LIMITATIONS AND EXCEPTIONS 5 8.0 QUALIFICATIONS 6 FIGURES Figure 1 Site Location Diagram Figure 2 Low Level Aerial Photograph with Soil Boring Locations Site Survey with Soil Boring Locations APPENDICES Appendix A Photographs Appendix B Soil Boring Logs Appendix C Laboratory Analytical Report Appendix D Ground Penetrating Radar Report ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 1 Former Royal Crest Motel - Gaylord, Michigan 1.0 INTRODUCTION Sagasser & Associates, Inc. has completed a Phase II Environmental Site Assessment (Phase II) of the former Royal Crest Motel located at 803 South Otsego Avenue in Gaylord, Michigan. The Subject Property is in the Southeast ¼ of Section 4, Township 30 North, Range 3 West, Gaylord, Bagley Township, Otsego County, Michigan (Subject Property). 1.1 PURPOSE The purpose of the Phase II Environmental Site Assessment was to evaluate the potential environmental impact to the Subject Property from the recognized environmental condition (REC) identified in Sagasser & Associates, Inc. Phase I Environmental Site Assessment (Phase I) report, dated July 2019. 1.2 AUTHORIZATION Sagasser & Associates, Inc. received authorization for performance of the assessment as part of a Michigan Department of Environment, Great Lakes & Energy Brownfield Site Assessment Grant to the Otsego County. 1.3 SCOPE OF WORK Sagasser & Associates, Inc. completed the Phase II Environmental Site Assessment using due care in accordance with customary practices, as ordinarily exercised by other reputable members of the profession under similar circumstances. Sagasser & Associates, Inc. completed the following scope of work: • Sagasser & Associates, Inc. personnel provided oversight for the advancement fifteen (15) soil borings utilizing a Geoprobe® for the collection of soil and groundwater samples to assess the documented historical soil and groundwater impacts from the former UST systems on the Subject Property. Borings were also advanced in areas with identified disturbed soils/areas of fill in several locations on the parcel to assess for impacts related to the general historical usage of the parcel. • Field screened the soils utilizing a photoionization detector (PID) for evidence of impacts. • Submitted fourteen (14) soil samples, one duplicate, one field blank & two groundwater samples for select laboratory analysis for the following parameters: - Full List Volatile Organic Compounds (VOCs) – EPA Method 8260 - Polynuclear Aromatic Hydrocarbons (PNAs) – EPA Method 8270 - Lead (Pb) – EPA Method 6020 • Reviewed and compared the analytical results to the established Residential Part 213 Risk-Based Screening Levels 201 Generic Cleanup Criteria & Screening Levels. The sampling activities completed as part of this assessment were conducted following systematic methods and procedures. The laboratory analyses were performed on the select samples collected, and represent the characteristics at those select sample locations at the time collected. No representation can be made concerning the future quality of these locations, or the quality of other areas of the Subject Property. No sampling and/or analysis of drinking water, building materials, surface water or air was performed as part of this specific assessment task and Sagasser & Associates, Inc. makes no representation or warranty concerning their quality. ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 2 Former Royal Crest Motel - Gaylord, Michigan 2.0 SITE DESCRIPTION The Subject Property is located at the southeast corner of South Otsego Avenue and West 7th Street and is indicated as having a parcel identification number of Tax I.D.#101-[PHONE REDACTED]-05. Three structures are located on the Subject Property. The structures are comprised of the north motel building with connecting hallway, pool, motel office, the south motel building; and a sauna/spa/game room building and represent a combined square footage of 22,000 ft2. Historical information indicates that the Subject Property was a vacant field until the 1940s when a gasoline (filling) and service station and tourist cabins were built. The Gay-Sego gasoline/service station operated from the 1950s to the late 1980s. The original Gay-Sego motel building was constructed in the 1960s with the north and south motel buildings constructed in the 1970s. The original motel building was demolished in the late 1980s followed by the construction of the new motel office, residence, and pool. The former service station building was converted to the motel office and then to a spa/sauna/gameroom. The Subject Property buildings are presently vacant. 3.0 PHASE I ENVIRONMENTAL SITE ASSESSMENT Sagasser & Associates, Inc. completed a Phase I Environmental Site Assessment of the Subject Property in July 2019. The assessment had revealed no evidence of recognized environmental conditions (RECs) in connection with the Subject Property except the following: • The historical usage of the Subject Property as a gasoline station/service garage and documented soil/groundwater impacts which exceed the Part 213 Risk-Based Screening Levels. A Baseline Environmental Assessment (BEA) was prepared for a previous owner in 2003. • The presence of 55-gallon drums of unknown contents. 4.0 PHASE II ENVIRONMENTAL SITE ASSESSMENT ACTIVITIES & ANALYTICAL RESULTS The Phase II assessment activities were performed by Sagasser & Associates, Inc. personnel on November 6, 2019, to assess if the historical usage as a gasoline/service station and overall usage had impacted the Subject Property. Sagasser & Associates, Inc. subcontracted Alluvial Earth for the use of a Geoprobe® for direct-push soil borings and sample collection. The soil and groundwater samples were appropriately preserved, stored on ice, and submitted to Eurofins/TestAmerica in Brighton, Michigan, under standard chain-of-custody protocol for analysis. The following details the assessment activities and laboratory analytical results for the samples collected. See Figure 2 and attached survey for soil boring locations. Note: SG-1 is labeled as B-10 and the remainder of the boring locations are numbered sequentially after that on the survey. The soil boring logs are presented as Appendix B & the laboratory analytical report is presented as Appendix C. Soil Borings B-1 through B-3 Soil borings B-1 through B-3 were located along the west side of the spa building (former service station) in the approximate vicinity of the former dispenser island(s). The soils encountered during boring advancement were comprised of fine to medium sand with varying amounts of fine gravel to 20 feet below ground surface (bgs). The soils were field screened with a PID and elevated PID readings were recorded. The elevated readings were attributed to heating up the baggies of soils in the truck due to frigid conditions prior to field screening. No obvious odors or staining were noted/observed in the soils. ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 3 Former Royal Crest Motel - Gaylord, Michigan A heated empty baggie was screened with the PID which identified similar elevated readings. Soil samples were collected from soil boring B-1 at 2.5’, boring B-2 at and boring B-3 at The soil samples were analyzed for VOC, PNAs, and lead. The analytical results for B-1, B-2 & B-3 were reported as non-detect for all VOCs and PNAs and below the Statewide Background Default Level for lead. See Photographs 1, 2, 3 & 15 for views of boring locations. Soil Borings B-4 through B-10 & SG-1 Soil borings B-4 through B-10 were advanced within and around the perimeter of the former UST basin as identified by GPR. The soils encountered during boring advancement were comprised of fine to medium sand with varying amounts of fine gravel from just below the surface to 25 feet bgs. The soils were field screened with a PID and elevated PID readings were recorded which again is attributed to the plastic baggies. Soil samples were collected from each of the borings at the following depths: B-4-10’, B- 5-15’, B-6-15’, B-7-15’, B-8-15’ & B-9-15’. The analytical results for the soil samples were non-detect for all VOCs and PNAs and below the Statewide Background Default Level for lead. Soil gas sample points were installed in soil borings B-5 & B-7 at a depth of 5 feet bgs. Soil boring SG-1 was advanced to a depth of 5 feet bgs at the northwest corner of the former spa building specifically for the installation of a soil gas sample point. A soil sample was collected from 5 feet bgs which was non-detect for VOCs & PNAs and below the Statewide Background Default Levels for lead. Soil boring B-10 was blind drilled to 90 feet bgs to assess for groundwater impacts in the vicinity of the former UST basin. Groundwater was measured at ~72 feet bgs, a shallower depth than anticipated based on historical data. A temporary well was installed and groundwater samples were collected from two intervals, 74’-79’ & 85’-90’ to assess both a shallow and deeper aquifer depths. The groundwater samples were collected utilizing a Waterra to low flow hand purge the temporary well. The groundwater samples were submitted for laboratory analysis of VOC, PNAs, and dissolved lead (only the 74’-79’ sample interval). The groundwater analytical results from B-10-74’-79’ were non-detect for all VOCs, PNAs, and lead. The groundwater results for B-10-85’-90’ were non-detect for all VOCs and PNAs excepting a low concentration of acetone [25 parts per billion (ppb)]. The acetone is attributed to a laboratory artifact and is also well below all cleanup criteria. See Photographs 4 through 10 & 16 for views of boring locations. Soil Borings B-11 through B-14 Soil borings B-11 through B-14 were advanced in the parking areas within the motel area. The borings were advanced within areas identified by GPR with disturbed soils/areas of fill. The soil borings were advanced to 10-15 feet bgs with soils being comprised of fine to medium sand with occasional coarse gravel. The soils were field screed with a PID and no elevated readings were record. No staining or obvious odors were observed/noted in the soils during field screening and characterization. No recovery of soils was encountered in select intervals of two borings. Soil samples were collected from 15 feet bgs in B-11, 10 feet bgs in B-12, 5 feet bgs in B-13, and 10 feet bgs in B-14. The analytical results for the soil samples were non-detect for all VOCs and PNAs and below the Statewide Background Default Level for lead. See Photographs 11 through 14 for views of boring locations B-11 through B-14. ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 4 Former Royal Crest Motel - Gaylord, Michigan 5.0 FINDINGS The purpose of the Phase II Environmental Site Assessment was to evaluate the potential environmental impact to the Subject Property from the recognized environmental condition, the historical usage of the as a former gasoline/service station with identified soil and groundwater impacts, and the overall historical usage of the property as detailed in the July 2019 Phase I report prepared by Sagasser & Associates, Inc. Based on the results of the Phase II assessment activities to assess the former UST systems, it does not appear that soil and groundwater impacts remain on the Subject Property. During the advancement of the soil borings, no elevated PID readings, stained soils, or obvious odors were noted. The analytical results for all of the soil samples collected from the former dispenser areas and UST basin were non- detect for all parameters. The two groundwater samples, a shallow and deep, were non-detect for petroleum VOCs and dissolved lead. The observed soil conditions and analytical results for the soil borings advanced within the disturbed soils/areas of fill within the parking areas on the Subject Property did not identify any impacts. Based on the results of the Phase II assessment activities, no further assessment activities of the UST systems and disturbed soils/areas of fill appear warranted at this time. 6.0 CLOSING Sagasser & Associates, Inc. sincerely appreciated the opportunity to provide our services. In the event that questions arise regarding the contents of this report or if you should need any further assistance, please feel free to contact us. Respectfully submitted, Sagasser & Associates, Inc. Scot Egleston Senior Environmental Scientist Kevin D. Sagasser, P.E. Senior Project Engineer ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 5 Former Royal Crest Motel - Gaylord, Michigan 7.0 LIMITATIONS AND EXCEPTIONS Sagasser & Associates, Inc. has performed the scope of work using due care in accordance with good and customary practices, as ordinarily exercised by other reputable members of the profession under similar circumstances. The nature of the services performed inevitably results in uncertainties with respect to exact contaminant conditions and/or subsurface characteristics, and certain interpolations and assumptions are often necessary. Therefore, Sagasser & Associates, Inc. makes no warranty or guarantee, expressed or implied, with respect to the services performed. The sampling activities completed as part of this assessment were conducted following systematic methods and procedures. The laboratory analyses were performed on the select samples collected, and represent the characteristics at those select sample locations at the time collected. No representation can be made concerning the future quality of these locations, or the quality of other areas of the Subject Property. No sampling or analysis of surface water, drinking water or air was performed and Sagasser & Associates, Inc. makes no representation or warranty concerning their quality. This report has been prepared for the exclusive use of the Client and the Client's representatives. Maps and sketches are provided for informational purposes and should not be considered surveys or engineering studies. Sagasser & Associates, Inc. conclusions and recommendation are based on the data gathered at the date of this report. In the event additional information is obtained subsequent to the report submittal, it will be submitted, intact, for the Client's review. Sagasser & Associates, Inc. accepts no liability for information obtained subsequent to report submittal. The conclusions and recommendations are based on Sagasser & Associates, Inc. interpretation of the data gathered. Sagasser & Associates, Inc. recommends that legal counsel be consulted regarding potential liabilities and/or determination of responsible parties with respect to the findings of this report. ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 6 Former Royal Crest Motel – Gaylord, Michigan 8.0 QUALIFICATIONS Personnel at Sagasser & Associates, Inc. have completed numerous environmental assessment and remediation projects ranging in scope from hydrogeologic investigations to spill prevention, control and countermeasure (SPCC) plans. Sagasser & Associates, Inc. personnel have completed specific training courses in performing Phase I Environmental Site Assessments and Phase II Preliminary Contamination Assessments, and have completed hundreds of Phase I site assessments throughout the country. The assessment was completed by Scot Egleston under the direction of Kevin D. Sagasser, P.E. Mr. Sagasser has over thirty years of diversified experience in the environmental field, primarily in environmental consulting and engineering. He has significant experience in development and performance of various environmental site investigations such as Phase I site assessments, preliminary contamination assessments, non-intrusive geophysical surveys, and hydrogeologic/remedial investigations. He has supervised and managed numerous site investigation projects, underground storage tank closures and soil/ground water contaminant remediation programs. Mr. Egleston is working as an environmental scientist with Sagasser & Associates, Inc. He has Bachelor’s of Science degrees in Environmental Science and Zoology with twenty-three years of experience in environmental consulting. ---PAGE BREAK--- Phase II Environmental Site Assessment Project #31902 Former Royal Crest Motel - Gaylord, Michigan FIGURES ---PAGE BREAK--- SITE LOCATION DIAGRAM FIGURE 1 Sagasser & Associates, Inc. Environmental Assessment & Consulting Services FORMER ROYAL CREST MOTEL 803 SOUTH OTSEGO AVENUE GAYLORD, MICHIGAN PROJECT: 31902 DATE: DEC 2019 SUBJECT PROPERTY N ---PAGE BREAK--- SITE PLAN – BORING LOCATIONS Figure 2 Sagasser & Associates, Inc. Environmental Assessment and Consulting Services Former Royal Crest Motel 803 South Otsego Avenue Gaylord, Otsego County, Michigan Project #31902 DECEMBER 2019 OTSEGO AVENUE FORMER UST BASIN FORMER GAS STATION 0 25’ 50’ NORTH SCALE SOIL BORING SOIL BORING WITH SOIL GAS GROUNDWATER SAMPLE B-10 B-2 B-1 B-13 B-14 B-11 B-12 B-8 B-6 B-7 B-3 SG-1 B-9 B-4 B-5 ---PAGE BREAK--- Phase II Environmental Site Assessment Project #31902 Former Royal Crest Motel - Gaylord, Michigan APPENDIX A PHOTOGRAPHS ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 1 Former Royal Crest Motel – Gaylord, Michigan PHOTO NO. 1: View of soil boring location B-1 looking southerly. PHOTO NO. 2: View of soil boring location B-2 looking southerly. Photograph by: Scot Egleston Date: November 6, 2019 ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 2 Former Royal Crest Motel – Gaylord, Michigan PHOTO NO. 3: View of soil boring location B-3 looking southerly. PHOTO NO. 4: View of soil boring location B-4 looking southerly. Photograph by: Scot Egleston Date: November 6, 2019 ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 3 Former Royal Crest Motel – Gaylord, Michigan PHOTO NO. 5: View of soil boring location B-5 looking southeasterly. PHOTO NO. 6: View of soil boring location B-6 looking northeasterly. Photograph by: Scot Egleston Date: November 6, 2019 ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 4 Former Royal Crest Motel – Gaylord, Michigan PHOTO NO. 7: View of soil boring location B-7 looking easterly. PHOTO NO. 8: View of soil boring location B-9 looking southeasterly. Photograph by: Scot Egleston Date: November 6, 2019 ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 5 Former Royal Crest Motel – Gaylord, Michigan PHOTO NO. 9: View of soil boring location SG-1. PHOTO NO. 10: View of soil boring location B-10. Photograph by: Scot Egleston Date: November 6, 2019 ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 6 Former Royal Crest Motel – Gaylord, Michigan PHOTO NO. 11: View of soil boring location B-11 looking easterly. PHOTO NO. 12: View of soil boring location B-12 looking easterly. Photograph by: Scot Egleston Date: November 6, 2019 ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 7 Former Royal Crest Motel – Gaylord, Michigan PHOTO NO. 13: View of soil boring location B-13 looking northerly. PHOTO NO. 14: View of soil boring location B-14 looking easterly. Photographs by: Scot Egleston Date: November 6, 2019 ---PAGE BREAK--- Sagasser & Associates, Inc. Phase II Environmental Site Assessment Project #31902 8 Former Royal Crest Motel – Gaylord, Michigan PHOTO NO. 15: View of soil boring locations collected in former dispenser island location. PHOTO NO. 16: View of soil boring locations at former UST basin location. Photographs by: Scot Egleston Date: November 6, 2019 B-1 B-2 B-3 SG-1 B-10 B-3 B-7 B-4 B-5 B-6 B-9 B-10 B-8 ---PAGE BREAK--- Phase II Environmental Site Assessment Project #31902 Former Royal Crest Motel - Gaylord, Michigan APPENDIX B SOIL BORING LOGS ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- Phase II Environmental Site Assessment Project #31902 Former Royal Crest Motel - Gaylord, Michigan APPENDIX C LABORATORY ANALYTICAL REPORT ---PAGE BREAK--- ANALYTICAL REPORT Eurofins TestAmerica, Michigan 10448 Citation Drive Suite 200 Brighton, MI 48116 Tel: (810)229-2763 Laboratory Job ID: 190-21518-1 Client Project/Site: Royal Crest For: Sagasser & Associates Inc 699 South Wisconsin Avenue Gaylord, Michigan 49735 Attn: Scot Egleston Authorized for release by: 11/19/2019 7:11:09 AM Sue Schafer, Project Manager II (810)229-2763 [EMAIL REDACTED] This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Table of Contents Client: Sagasser & Associates Inc Project/Site: Royal Crest Laboratory Job ID: 190-21518-1 Page 2 of 64 Eurofins TestAmerica, Michigan 11/19/2019 Cover Page . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 Table of Contents . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2 Sample Summary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3 Case Narrative . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4 Client Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6 QC Sample Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 44 Definitions/Glossary . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 57 Chain of Custody . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 58 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Sample Summary Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID Client Sample ID Received Collected Matrix Asset ID 190-21518-1 B-1-2.5' Soil 11/06/19 10:06 11/08/19 10:11 190-21518-2 B-2-5' Soil 11/06/19 10:27 11/08/19 10:11 190-21518-3 B-3-5' Soil 11/06/19 10:40 11/08/19 10:11 190-21518-4 B-4-10' Soil 11/06/19 11:25 11/08/19 10:11 190-21518-5 B-5-15' Soil 11/06/19 11:42 11/08/19 10:11 190-21518-6 B-6-15' Soil 11/06/19 12:05 11/08/19 10:11 190-21518-7 B-7-15' Soil 11/06/19 12:30 11/08/19 10:11 190-21518-8 B-8-15' Soil 11/06/19 12:56 11/08/19 10:11 190-21518-9 B-9-15' Soil 11/06/19 13:20 11/08/19 10:11 190-21518-10 B-11-15' Soil 11/06/19 15:18 11/08/19 10:11 190-21518-11 B-12-10' Soil 11/06/19 15:30 11/08/19 10:11 190-21518-12 B-13-5' Soil 11/06/19 15:50 11/08/19 10:11 190-21518-13 B-14-10' Soil 11/06/19 16:40 11/08/19 10:11 190-21518-14 SG-1-5' Soil 11/06/19 13:30 11/08/19 10:11 190-21518-15 Duplicate Soil 11/06/19 00:00 11/08/19 10:11 190-21518-16 Field Blank Soil 11/06/19 13:35 11/08/19 10:11 190-21518-17 B-10-85'-90' Ground Water 11/06/19 14:35 11/08/19 10:11 190-21518-18 B-10-74'-79' Ground Water 11/06/19 14:55 11/08/19 10:11 Eurofins TestAmerica, Michigan Page 3 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Case Narrative Client: Sagasser & Associates Inc Job ID: 190-21518-1 Project/Site: Royal Crest Job ID: 190-21518-1 Laboratory: Eurofins TestAmerica, Michigan Narrative Job Narrative 190-21518-1 Comments No additional comments. Receipt The samples were received on 11/8/2019 10:11 AM; the samples arrived in good condition, properly preserved and, where required, on ice. The temperature of the cooler at receipt was 4.6º C. GC/MS VOA Method 5035: This terra core was received with a low methanol volume. B-14-10' (190-21518-13) and was prepped from a bulk jar that was taken from the sample receiving refrigerator. Both sets of data are reported. Method 8260B: Surrogate recovery for the following sample was outside the upper control limit: B-14-10' (190-21518-13). This sample did not contain any target analytes; therefore, re-extraction and/or re-analysis was not performed. Method 8260B: The laboratory control sample (LCS) for analytical batch 240-411253 recovered outside control limits for the following analyte: Cyclohexane. This analyte was biased high in the LCS and was not detected in the associated samples; therefore, the data has been reported. B-10-85'-90' (190-21518-17), B-10-74'-79' (190-21518-18) and (LCS 240-411253/4) Method 8260B: The laboratory control sample (LCS) for analytical batch 240-411253 recovered outside control limits for the following analyte: Ethylene dibromide. This has been identified as a poor performing analyte when analyzed using this method; therefore, re-extraction/re-analysis was not performed. B-10-85'-90' (190-21518-17), B-10-74'-79' (190-21518-18) and (LCS 240-411253/4) Method 8260B: The laboratory control sample (LCS) analyzed in batch 240-411253 was below the recovery control criteria for multiple analyte(s): This variance only affects results measured above the reporting limit. A MRL standard at or below the reporting limit (RL) was analyzed with the affected samples and found to be acceptable. This demonstrates the analyte reporting limit is valid, and it is acceptable to report ND results (non-detects). The samples associated with the LCS were non-detects for the affected analytes; therefore, the results were reported. The following samples are impacted: B-10-85'-90' (190-21518-17), B-10-74'-79' (190-21518-18) and (LCS 240-411253/4) Method 8260B: The pH of the sample(s) was greater than 2. The samples were analyzed within the normal 14 day holding time; however, experimental evidence suggests that some aromatic compounds in wastewater samples, notably, Benzene, Toluene, and are susceptible to biological degradation if samples are not preserved to a pH of 2. B-10-85'-90' (190-21518-17) and B-10-74'-79' (190-21518-18) No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. GC/MS Semi VOA No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Metals No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Organic Prep Method 3510C: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MS/MSD) associated with preparation batch 240-410213. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. VOA Prep Eurofins TestAmerica, Michigan Page 4 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Case Narrative Client: Sagasser & Associates Inc Job ID: 190-21518-1 Project/Site: Royal Crest Job ID: 190-21518-1 (Continued) Laboratory: Eurofins TestAmerica, Michigan (Continued) No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Eurofins TestAmerica, Michigan Page 5 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-1 Client Sample ID: B-1-2.5' Matrix: Soil Date Collected: 11/06/19 10:06 Percent Solids: 89.9 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1300 1300 ug/Kg ☼ 11/11/19 18:30 11/12/19 16:11 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Benzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Bromoform <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Bromomethane <330 1300 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 2-Butanone (MEK) <1300 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Carbon disulfide <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Carbon tetrachloride <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Chlorobenzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Chlorodibromomethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Chloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Chloroform <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Chloromethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ cis-1,2-Dichloroethene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ cis-1,3-Dichloropropene <330 650 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Cyclohexane <650 650 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,2-Dibromo-3-Chloropropane <650 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,2-Dichlorobenzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,3-Dichlorobenzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,4-Dichlorobenzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Dichlorobromomethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Dichlorodifluoromethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,1-Dichloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,2-Dichloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,1-Dichloroethene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,2-Dichloropropane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,2-Dibromoethane (EDB) <330 1300 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 2-Hexanone <1300 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Isopropylbenzene <330 1600 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Methyl acetate <1600 650 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ <650 650 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Methylene Chloride <650 1600 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ <1600 1300 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 4-Methyl-2-pentanone (MIBK) <1300 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Methyl tert-butyl ether <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ m-Xylene & p-Xylene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Naphthalene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ o-Xylene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Styrene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,1,2,2-Tetrachloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Tetrachloroethene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Toluene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ trans-1,2-Dichloroethene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ trans-1,3-Dichloropropene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,2,4-Trichlorobenzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,1,1-Trichloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ 1,1,2-Trichloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Trichloroethene <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Trichlorofluoromethane <330 Eurofins TestAmerica, Michigan Page 6 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-1 Client Sample ID: B-1-2.5' Matrix: Soil Date Collected: 11/06/19 10:06 Percent Solids: 89.9 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <330 330 ug/Kg ☼ 11/11/19 18:30 11/12/19 16:11 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ <330 330 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Vinyl chloride <330 650 ug/Kg 11/11/19 18:30 11/12/19 16:11 1 ☼ Xylenes, Total <650 4-Bromofluorobenzene (Surr) 104 51 - 124 11/11/19 18:30 11/12/19 16:11 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 96 11/11/19 18:30 11/12/19 16:11 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 115 11/11/19 18:30 11/12/19 16:11 1 47 - 136 Toluene-d8 (Surr) 113 11/11/19 18:30 11/12/19 16:11 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <290 290 ug/Kg ☼ 11/14/19 09:48 11/17/19 15:25 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Benzo[a]anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Benzo[a]pyrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Benzo[b]fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Benzo[g,h,i]perylene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Benzo[k]fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Dibenz(a,h)anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Fluorene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Indeno[1,2,3-cd]pyrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Naphthalene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Phenanthrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:25 1 ☼ Pyrene <290 2-Fluorobiphenyl (Surr) 80 35 - 120 11/14/19 09:48 11/17/19 15:25 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 76 11/14/19 09:48 11/17/19 15:25 1 26 - 120 Nitrobenzene-d5 (Surr) 76 11/14/19 09:48 11/17/19 15:25 1 28 - 120 Phenol-d5 (Surr) 83 11/14/19 09:48 11/17/19 15:25 1 28 - 120 Terphenyl-d14 (Surr) 93 11/14/19 09:48 11/17/19 15:25 1 39 - 120 2,4,6-Tribromophenol (Surr) 41 11/14/19 09:48 11/17/19 15:25 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 2500 390 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:15 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 89.9 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 10.1 Eurofins TestAmerica, Michigan Page 7 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-2 Client Sample ID: B-2-5' Matrix: Soil Date Collected: 11/06/19 10:27 Percent Solids: 90.1 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1200 1200 ug/Kg ☼ 11/11/19 18:30 11/12/19 16:36 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Benzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Bromoform <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Bromomethane <300 1200 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 2-Butanone (MEK) <1200 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Carbon disulfide <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Carbon tetrachloride <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Chlorobenzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Chlorodibromomethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Chloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Chloroform <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Chloromethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ cis-1,2-Dichloroethene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ cis-1,3-Dichloropropene <300 590 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Cyclohexane <590 590 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,2-Dibromo-3-Chloropropane <590 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,2-Dichlorobenzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,3-Dichlorobenzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,4-Dichlorobenzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Dichlorobromomethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Dichlorodifluoromethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,1-Dichloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,2-Dichloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,1-Dichloroethene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,2-Dichloropropane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,2-Dibromoethane (EDB) <300 1200 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 2-Hexanone <1200 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Isopropylbenzene <300 1500 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Methyl acetate <1500 590 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ <590 590 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Methylene Chloride <590 1500 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ <1500 1200 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 4-Methyl-2-pentanone (MIBK) <1200 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Methyl tert-butyl ether <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ m-Xylene & p-Xylene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Naphthalene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ o-Xylene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Styrene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,1,2,2-Tetrachloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Tetrachloroethene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Toluene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ trans-1,2-Dichloroethene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ trans-1,3-Dichloropropene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,2,4-Trichlorobenzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,1,1-Trichloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ 1,1,2-Trichloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Trichloroethene <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Trichlorofluoromethane <300 Eurofins TestAmerica, Michigan Page 8 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-2 Client Sample ID: B-2-5' Matrix: Soil Date Collected: 11/06/19 10:27 Percent Solids: 90.1 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <300 300 ug/Kg ☼ 11/11/19 18:30 11/12/19 16:36 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ <300 300 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Vinyl chloride <300 590 ug/Kg 11/11/19 18:30 11/12/19 16:36 1 ☼ Xylenes, Total <590 4-Bromofluorobenzene (Surr) 95 51 - 124 11/11/19 18:30 11/12/19 16:36 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 87 11/11/19 18:30 11/12/19 16:36 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 108 11/11/19 18:30 11/12/19 16:36 1 47 - 136 Toluene-d8 (Surr) 102 11/11/19 18:30 11/12/19 16:36 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <290 290 ug/Kg ☼ 11/14/19 09:48 11/17/19 15:50 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Benzo[a]anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Benzo[a]pyrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Benzo[b]fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Benzo[g,h,i]perylene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Benzo[k]fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Dibenz(a,h)anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Fluorene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Indeno[1,2,3-cd]pyrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Naphthalene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Phenanthrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 15:50 1 ☼ Pyrene <290 2-Fluorobiphenyl (Surr) 81 35 - 120 11/14/19 09:48 11/17/19 15:50 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 77 11/14/19 09:48 11/17/19 15:50 1 26 - 120 Nitrobenzene-d5 (Surr) 83 11/14/19 09:48 11/17/19 15:50 1 28 - 120 Phenol-d5 (Surr) 86 11/14/19 09:48 11/17/19 15:50 1 28 - 120 Terphenyl-d14 (Surr) 100 11/14/19 09:48 11/17/19 15:50 1 39 - 120 2,4,6-Tribromophenol (Surr) 52 11/14/19 09:48 11/17/19 15:50 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 1700 360 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:26 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 90.1 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 9.9 Eurofins TestAmerica, Michigan Page 9 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-3 Client Sample ID: B-3-5' Matrix: Soil Date Collected: 11/06/19 10:40 Percent Solids: 85.4 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1300 1300 ug/Kg ☼ 11/11/19 18:30 11/12/19 17:00 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Benzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Bromoform <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Bromomethane <330 1300 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 2-Butanone (MEK) <1300 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Carbon disulfide <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Carbon tetrachloride <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Chlorobenzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Chlorodibromomethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Chloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Chloroform <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Chloromethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ cis-1,2-Dichloroethene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ cis-1,3-Dichloropropene <330 660 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Cyclohexane <660 660 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,2-Dibromo-3-Chloropropane <660 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,2-Dichlorobenzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,3-Dichlorobenzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,4-Dichlorobenzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Dichlorobromomethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Dichlorodifluoromethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,1-Dichloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,2-Dichloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,1-Dichloroethene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,2-Dichloropropane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,2-Dibromoethane (EDB) <330 1300 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 2-Hexanone <1300 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Isopropylbenzene <330 1600 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Methyl acetate <1600 660 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ <660 660 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Methylene Chloride <660 1600 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ <1600 1300 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 4-Methyl-2-pentanone (MIBK) <1300 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Methyl tert-butyl ether <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ m-Xylene & p-Xylene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Naphthalene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ o-Xylene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Styrene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,1,2,2-Tetrachloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Tetrachloroethene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Toluene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ trans-1,2-Dichloroethene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ trans-1,3-Dichloropropene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,2,4-Trichlorobenzene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,1,1-Trichloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ 1,1,2-Trichloroethane <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Trichloroethene <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Trichlorofluoromethane <330 Eurofins TestAmerica, Michigan Page 10 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-3 Client Sample ID: B-3-5' Matrix: Soil Date Collected: 11/06/19 10:40 Percent Solids: 85.4 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <330 330 ug/Kg ☼ 11/11/19 18:30 11/12/19 17:00 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ <330 330 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Vinyl chloride <330 660 ug/Kg 11/11/19 18:30 11/12/19 17:00 1 ☼ Xylenes, Total <660 4-Bromofluorobenzene (Surr) 95 51 - 124 11/11/19 18:30 11/12/19 17:00 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 87 11/11/19 18:30 11/12/19 17:00 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 108 11/11/19 18:30 11/12/19 17:00 1 47 - 136 Toluene-d8 (Surr) 104 11/11/19 18:30 11/12/19 17:00 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <310 310 ug/Kg ☼ 11/14/19 09:48 11/17/19 16:15 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Anthracene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Benzo[a]anthracene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Benzo[a]pyrene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Benzo[b]fluoranthene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Benzo[g,h,i]perylene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Benzo[k]fluoranthene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Dibenz(a,h)anthracene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Fluoranthene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Fluorene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Indeno[1,2,3-cd]pyrene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Naphthalene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Phenanthrene <310 310 ug/Kg 11/14/19 09:48 11/17/19 16:15 1 ☼ Pyrene <310 2-Fluorobiphenyl (Surr) 73 35 - 120 11/14/19 09:48 11/17/19 16:15 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 71 11/14/19 09:48 11/17/19 16:15 1 26 - 120 Nitrobenzene-d5 (Surr) 75 11/14/19 09:48 11/17/19 16:15 1 28 - 120 Phenol-d5 (Surr) 79 11/14/19 09:48 11/17/19 16:15 1 28 - 120 Terphenyl-d14 (Surr) 87 11/14/19 09:48 11/17/19 16:15 1 39 - 120 2,4,6-Tribromophenol (Surr) 47 11/14/19 09:48 11/17/19 16:15 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 3400 400 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:28 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 85.4 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 14.6 Eurofins TestAmerica, Michigan Page 11 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-4 Client Sample ID: B-4-10' Matrix: Soil Date Collected: 11/06/19 11:25 Percent Solids: 94.1 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1100 1100 ug/Kg ☼ 11/11/19 18:30 11/12/19 17:25 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Benzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Bromoform <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Bromomethane <270 1100 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 2-Butanone (MEK) <1100 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Carbon disulfide <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Carbon tetrachloride <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Chlorobenzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Chlorodibromomethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Chloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Chloroform <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Chloromethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ cis-1,2-Dichloroethene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ cis-1,3-Dichloropropene <270 550 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Cyclohexane <550 550 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,2-Dibromo-3-Chloropropane <550 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,2-Dichlorobenzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,3-Dichlorobenzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,4-Dichlorobenzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Dichlorobromomethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Dichlorodifluoromethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,1-Dichloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,2-Dichloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,1-Dichloroethene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,2-Dichloropropane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,2-Dibromoethane (EDB) <270 1100 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 2-Hexanone <1100 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Isopropylbenzene <270 1400 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Methyl acetate <1400 550 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ <550 550 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Methylene Chloride <550 1400 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ <1400 1100 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 4-Methyl-2-pentanone (MIBK) <1100 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Methyl tert-butyl ether <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ m-Xylene & p-Xylene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Naphthalene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ o-Xylene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Styrene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,1,2,2-Tetrachloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Tetrachloroethene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Toluene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ trans-1,2-Dichloroethene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ trans-1,3-Dichloropropene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,2,4-Trichlorobenzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,1,1-Trichloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ 1,1,2-Trichloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Trichloroethene <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Trichlorofluoromethane <270 Eurofins TestAmerica, Michigan Page 12 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-4 Client Sample ID: B-4-10' Matrix: Soil Date Collected: 11/06/19 11:25 Percent Solids: 94.1 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <270 270 ug/Kg ☼ 11/11/19 18:30 11/12/19 17:25 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ <270 270 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Vinyl chloride <270 550 ug/Kg 11/11/19 18:30 11/12/19 17:25 1 ☼ Xylenes, Total <550 4-Bromofluorobenzene (Surr) 99 51 - 124 11/11/19 18:30 11/12/19 17:25 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 87 11/11/19 18:30 11/12/19 17:25 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 110 11/11/19 18:30 11/12/19 17:25 1 47 - 136 Toluene-d8 (Surr) 107 11/11/19 18:30 11/12/19 17:25 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <280 280 ug/Kg ☼ 11/14/19 09:48 11/17/19 16:41 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Benzo[a]anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Benzo[a]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Benzo[b]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Benzo[g,h,i]perylene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Benzo[k]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Dibenz(a,h)anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Fluorene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Indeno[1,2,3-cd]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Naphthalene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Phenanthrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 16:41 1 ☼ Pyrene <280 2-Fluorobiphenyl (Surr) 81 35 - 120 11/14/19 09:48 11/17/19 16:41 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 78 11/14/19 09:48 11/17/19 16:41 1 26 - 120 Nitrobenzene-d5 (Surr) 83 11/14/19 09:48 11/17/19 16:41 1 28 - 120 Phenol-d5 (Surr) 84 11/14/19 09:48 11/17/19 16:41 1 28 - 120 Terphenyl-d14 (Surr) 95 11/14/19 09:48 11/17/19 16:41 1 39 - 120 2,4,6-Tribromophenol (Surr) 41 11/14/19 09:48 11/17/19 16:41 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 6700 360 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:35 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 94.1 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 5.9 Eurofins TestAmerica, Michigan Page 13 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-5 Client Sample ID: B-5-15' Matrix: Soil Date Collected: 11/06/19 11:42 Percent Solids: 97.3 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1000 1000 ug/Kg ☼ 11/11/19 18:30 11/12/19 17:50 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Benzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Bromoform <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Bromomethane <260 1000 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 2-Butanone (MEK) <1000 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Carbon disulfide <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Carbon tetrachloride <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Chlorobenzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Chlorodibromomethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Chloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Chloroform <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Chloromethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ cis-1,2-Dichloroethene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ cis-1,3-Dichloropropene <260 510 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Cyclohexane <510 510 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,2-Dibromo-3-Chloropropane <510 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,2-Dichlorobenzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,3-Dichlorobenzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,4-Dichlorobenzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Dichlorobromomethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Dichlorodifluoromethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,1-Dichloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,2-Dichloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,1-Dichloroethene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,2-Dichloropropane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,2-Dibromoethane (EDB) <260 1000 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 2-Hexanone <1000 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Isopropylbenzene <260 1300 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Methyl acetate <1300 510 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ <510 510 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Methylene Chloride <510 1300 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ <1300 1000 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 4-Methyl-2-pentanone (MIBK) <1000 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Methyl tert-butyl ether <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ m-Xylene & p-Xylene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Naphthalene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ o-Xylene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Styrene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,1,2,2-Tetrachloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Tetrachloroethene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Toluene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ trans-1,2-Dichloroethene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ trans-1,3-Dichloropropene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,2,4-Trichlorobenzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,1,1-Trichloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ 1,1,2-Trichloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Trichloroethene <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Trichlorofluoromethane <260 Eurofins TestAmerica, Michigan Page 14 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-5 Client Sample ID: B-5-15' Matrix: Soil Date Collected: 11/06/19 11:42 Percent Solids: 97.3 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <260 260 ug/Kg ☼ 11/11/19 18:30 11/12/19 17:50 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ <260 260 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Vinyl chloride <260 510 ug/Kg 11/11/19 18:30 11/12/19 17:50 1 ☼ Xylenes, Total <510 4-Bromofluorobenzene (Surr) 99 51 - 124 11/11/19 18:30 11/12/19 17:50 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 92 11/11/19 18:30 11/12/19 17:50 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 113 11/11/19 18:30 11/12/19 17:50 1 47 - 136 Toluene-d8 (Surr) 107 11/11/19 18:30 11/12/19 17:50 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <270 270 ug/Kg ☼ 11/14/19 09:48 11/17/19 17:06 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Anthracene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Benzo[a]anthracene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Benzo[a]pyrene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Benzo[b]fluoranthene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Benzo[g,h,i]perylene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Benzo[k]fluoranthene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Dibenz(a,h)anthracene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Fluoranthene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Fluorene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Indeno[1,2,3-cd]pyrene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Naphthalene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Phenanthrene <270 270 ug/Kg 11/14/19 09:48 11/17/19 17:06 1 ☼ Pyrene <270 2-Fluorobiphenyl (Surr) 86 35 - 120 11/14/19 09:48 11/17/19 17:06 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 80 11/14/19 09:48 11/17/19 17:06 1 26 - 120 Nitrobenzene-d5 (Surr) 87 11/14/19 09:48 11/17/19 17:06 1 28 - 120 Phenol-d5 (Surr) 90 11/14/19 09:48 11/17/19 17:06 1 28 - 120 Terphenyl-d14 (Surr) 103 11/14/19 09:48 11/17/19 17:06 1 39 - 120 2,4,6-Tribromophenol (Surr) 55 11/14/19 09:48 11/17/19 17:06 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 620 340 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:38 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 97.3 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 2.7 Eurofins TestAmerica, Michigan Page 15 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-6 Client Sample ID: B-6-15' Matrix: Soil Date Collected: 11/06/19 12:05 Percent Solids: 93.1 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1100 1100 ug/Kg ☼ 11/11/19 18:30 11/12/19 18:15 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Benzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Bromoform <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Bromomethane <280 1100 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 2-Butanone (MEK) <1100 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Carbon disulfide <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Carbon tetrachloride <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Chlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Chlorodibromomethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Chloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Chloroform <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Chloromethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ cis-1,2-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ cis-1,3-Dichloropropene <280 560 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Cyclohexane <560 560 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,2-Dibromo-3-Chloropropane <560 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,2-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,3-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,4-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Dichlorobromomethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Dichlorodifluoromethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,1-Dichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,2-Dichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,1-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,2-Dichloropropane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,2-Dibromoethane (EDB) <280 1100 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 2-Hexanone <1100 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Isopropylbenzene <280 1400 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Methyl acetate <1400 560 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ <560 560 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Methylene Chloride <560 1400 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ <1400 1100 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 4-Methyl-2-pentanone (MIBK) <1100 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Methyl tert-butyl ether <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ m-Xylene & p-Xylene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Naphthalene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ o-Xylene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Styrene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,1,2,2-Tetrachloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Tetrachloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Toluene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ trans-1,2-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ trans-1,3-Dichloropropene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,2,4-Trichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,1,1-Trichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ 1,1,2-Trichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Trichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Trichlorofluoromethane <280 Eurofins TestAmerica, Michigan Page 16 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-6 Client Sample ID: B-6-15' Matrix: Soil Date Collected: 11/06/19 12:05 Percent Solids: 93.1 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <280 280 ug/Kg ☼ 11/11/19 18:30 11/12/19 18:15 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Vinyl chloride <280 560 ug/Kg 11/11/19 18:30 11/12/19 18:15 1 ☼ Xylenes, Total <560 4-Bromofluorobenzene (Surr) 95 51 - 124 11/11/19 18:30 11/12/19 18:15 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 78 11/11/19 18:30 11/12/19 18:15 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 106 11/11/19 18:30 11/12/19 18:15 1 47 - 136 Toluene-d8 (Surr) 104 11/11/19 18:30 11/12/19 18:15 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <280 280 ug/Kg ☼ 11/14/19 09:48 11/17/19 17:31 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Benzo[a]anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Benzo[a]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Benzo[b]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Benzo[g,h,i]perylene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Benzo[k]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Dibenz(a,h)anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Fluorene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Indeno[1,2,3-cd]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Naphthalene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Phenanthrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:31 1 ☼ Pyrene <280 2-Fluorobiphenyl (Surr) 79 35 - 120 11/14/19 09:48 11/17/19 17:31 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 74 11/14/19 09:48 11/17/19 17:31 1 26 - 120 Nitrobenzene-d5 (Surr) 79 11/14/19 09:48 11/17/19 17:31 1 28 - 120 Phenol-d5 (Surr) 84 11/14/19 09:48 11/17/19 17:31 1 28 - 120 Terphenyl-d14 (Surr) 91 11/14/19 09:48 11/17/19 17:31 1 39 - 120 2,4,6-Tribromophenol (Surr) 38 11/14/19 09:48 11/17/19 17:31 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 800 390 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:40 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 93.1 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 6.9 Eurofins TestAmerica, Michigan Page 17 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-7 Client Sample ID: B-7-15' Matrix: Soil Date Collected: 11/06/19 12:30 Percent Solids: 93.2 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1100 1100 ug/Kg ☼ 11/11/19 18:30 11/12/19 18:39 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Benzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Bromoform <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Bromomethane <290 1100 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 2-Butanone (MEK) <1100 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Carbon disulfide <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Carbon tetrachloride <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Chlorobenzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Chlorodibromomethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Chloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Chloroform <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Chloromethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ cis-1,2-Dichloroethene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ cis-1,3-Dichloropropene <290 570 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Cyclohexane <570 570 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,2-Dibromo-3-Chloropropane <570 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,2-Dichlorobenzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,3-Dichlorobenzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,4-Dichlorobenzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Dichlorobromomethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Dichlorodifluoromethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,1-Dichloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,2-Dichloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,1-Dichloroethene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,2-Dichloropropane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,2-Dibromoethane (EDB) <290 1100 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 2-Hexanone <1100 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Isopropylbenzene <290 1400 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Methyl acetate <1400 570 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ <570 570 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Methylene Chloride <570 1400 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ <1400 1100 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 4-Methyl-2-pentanone (MIBK) <1100 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Methyl tert-butyl ether <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ m-Xylene & p-Xylene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Naphthalene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ o-Xylene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Styrene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,1,2,2-Tetrachloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Tetrachloroethene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Toluene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ trans-1,2-Dichloroethene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ trans-1,3-Dichloropropene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,2,4-Trichlorobenzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,1,1-Trichloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ 1,1,2-Trichloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Trichloroethene <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Trichlorofluoromethane <290 Eurofins TestAmerica, Michigan Page 18 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-7 Client Sample ID: B-7-15' Matrix: Soil Date Collected: 11/06/19 12:30 Percent Solids: 93.2 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <290 290 ug/Kg ☼ 11/11/19 18:30 11/12/19 18:39 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ <290 290 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Vinyl chloride <290 570 ug/Kg 11/11/19 18:30 11/12/19 18:39 1 ☼ Xylenes, Total <570 4-Bromofluorobenzene (Surr) 96 51 - 124 11/11/19 18:30 11/12/19 18:39 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 81 11/11/19 18:30 11/12/19 18:39 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 107 11/11/19 18:30 11/12/19 18:39 1 47 - 136 Toluene-d8 (Surr) 104 11/11/19 18:30 11/12/19 18:39 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <280 280 ug/Kg ☼ 11/14/19 09:48 11/17/19 17:56 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Benzo[a]anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Benzo[a]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Benzo[b]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Benzo[g,h,i]perylene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Benzo[k]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Dibenz(a,h)anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Fluorene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Indeno[1,2,3-cd]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Naphthalene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Phenanthrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 17:56 1 ☼ Pyrene <280 2-Fluorobiphenyl (Surr) 78 35 - 120 11/14/19 09:48 11/17/19 17:56 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 76 11/14/19 09:48 11/17/19 17:56 1 26 - 120 Nitrobenzene-d5 (Surr) 79 11/14/19 09:48 11/17/19 17:56 1 28 - 120 Phenol-d5 (Surr) 85 11/14/19 09:48 11/17/19 17:56 1 28 - 120 Terphenyl-d14 (Surr) 92 11/14/19 09:48 11/17/19 17:56 1 39 - 120 2,4,6-Tribromophenol (Surr) 39 11/14/19 09:48 11/17/19 17:56 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 880 360 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:42 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 93.2 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 6.8 Eurofins TestAmerica, Michigan Page 19 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-8 Client Sample ID: B-8-15' Matrix: Soil Date Collected: 11/06/19 12:56 Percent Solids: 93.5 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1100 1100 ug/Kg ☼ 11/11/19 18:30 11/12/19 19:04 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Benzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Bromoform <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Bromomethane <280 1100 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 2-Butanone (MEK) <1100 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Carbon disulfide <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Carbon tetrachloride <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Chlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Chlorodibromomethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Chloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Chloroform <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Chloromethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ cis-1,2-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ cis-1,3-Dichloropropene <280 560 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Cyclohexane <560 560 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,2-Dibromo-3-Chloropropane <560 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,2-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,3-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,4-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Dichlorobromomethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Dichlorodifluoromethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,1-Dichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,2-Dichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,1-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,2-Dichloropropane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,2-Dibromoethane (EDB) <280 1100 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 2-Hexanone <1100 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Isopropylbenzene <280 1400 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Methyl acetate <1400 560 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ <560 560 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Methylene Chloride <560 1400 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ <1400 1100 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 4-Methyl-2-pentanone (MIBK) <1100 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Methyl tert-butyl ether <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ m-Xylene & p-Xylene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Naphthalene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ o-Xylene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Styrene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,1,2,2-Tetrachloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Tetrachloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Toluene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ trans-1,2-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ trans-1,3-Dichloropropene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,2,4-Trichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,1,1-Trichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ 1,1,2-Trichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Trichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Trichlorofluoromethane <280 Eurofins TestAmerica, Michigan Page 20 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-8 Client Sample ID: B-8-15' Matrix: Soil Date Collected: 11/06/19 12:56 Percent Solids: 93.5 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <280 280 ug/Kg ☼ 11/11/19 18:30 11/12/19 19:04 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Vinyl chloride <280 560 ug/Kg 11/11/19 18:30 11/12/19 19:04 1 ☼ Xylenes, Total <560 4-Bromofluorobenzene (Surr) 98 51 - 124 11/11/19 18:30 11/12/19 19:04 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 91 11/11/19 18:30 11/12/19 19:04 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 114 11/11/19 18:30 11/12/19 19:04 1 47 - 136 Toluene-d8 (Surr) 107 11/11/19 18:30 11/12/19 19:04 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <280 280 ug/Kg ☼ 11/14/19 09:48 11/17/19 18:22 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Benzo[a]anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Benzo[a]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Benzo[b]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Benzo[g,h,i]perylene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Benzo[k]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Dibenz(a,h)anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Fluorene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Indeno[1,2,3-cd]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Naphthalene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Phenanthrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 18:22 1 ☼ Pyrene <280 2-Fluorobiphenyl (Surr) 79 35 - 120 11/14/19 09:48 11/17/19 18:22 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 78 11/14/19 09:48 11/17/19 18:22 1 26 - 120 Nitrobenzene-d5 (Surr) 79 11/14/19 09:48 11/17/19 18:22 1 28 - 120 Phenol-d5 (Surr) 86 11/14/19 09:48 11/17/19 18:22 1 28 - 120 Terphenyl-d14 (Surr) 95 11/14/19 09:48 11/17/19 18:22 1 39 - 120 2,4,6-Tribromophenol (Surr) 47 11/14/19 09:48 11/17/19 18:22 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 680 290 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:44 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 93.5 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 6.5 Eurofins TestAmerica, Michigan Page 21 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-9 Client Sample ID: B-9-15' Matrix: Soil Date Collected: 11/06/19 13:20 Percent Solids: 92.0 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1100 1100 ug/Kg ☼ 11/11/19 18:30 11/12/19 19:29 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Benzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Bromoform <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Bromomethane <280 1100 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 2-Butanone (MEK) <1100 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Carbon disulfide <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Carbon tetrachloride <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Chlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Chlorodibromomethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Chloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Chloroform <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Chloromethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ cis-1,2-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ cis-1,3-Dichloropropene <280 570 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Cyclohexane <570 570 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,2-Dibromo-3-Chloropropane <570 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,2-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,3-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,4-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Dichlorobromomethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Dichlorodifluoromethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,1-Dichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,2-Dichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,1-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,2-Dichloropropane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,2-Dibromoethane (EDB) <280 1100 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 2-Hexanone <1100 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Isopropylbenzene <280 1400 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Methyl acetate <1400 570 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ <570 570 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Methylene Chloride <570 1400 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ <1400 1100 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 4-Methyl-2-pentanone (MIBK) <1100 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Methyl tert-butyl ether <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ m-Xylene & p-Xylene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Naphthalene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ o-Xylene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Styrene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,1,2,2-Tetrachloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Tetrachloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Toluene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ trans-1,2-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ trans-1,3-Dichloropropene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,2,4-Trichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,1,1-Trichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ 1,1,2-Trichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Trichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Trichlorofluoromethane <280 Eurofins TestAmerica, Michigan Page 22 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-9 Client Sample ID: B-9-15' Matrix: Soil Date Collected: 11/06/19 13:20 Percent Solids: 92.0 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <280 280 ug/Kg ☼ 11/11/19 18:30 11/12/19 19:29 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Vinyl chloride <280 570 ug/Kg 11/11/19 18:30 11/12/19 19:29 1 ☼ Xylenes, Total <570 4-Bromofluorobenzene (Surr) 98 51 - 124 11/11/19 18:30 11/12/19 19:29 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 90 11/11/19 18:30 11/12/19 19:29 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 115 11/11/19 18:30 11/12/19 19:29 1 47 - 136 Toluene-d8 (Surr) 106 11/11/19 18:30 11/12/19 19:29 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <290 290 ug/Kg ☼ 11/14/19 09:48 11/17/19 18:47 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Benzo[a]anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Benzo[a]pyrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Benzo[b]fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Benzo[g,h,i]perylene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Benzo[k]fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Dibenz(a,h)anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Fluorene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Indeno[1,2,3-cd]pyrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Naphthalene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Phenanthrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 18:47 1 ☼ Pyrene <290 2-Fluorobiphenyl (Surr) 82 35 - 120 11/14/19 09:48 11/17/19 18:47 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 76 11/14/19 09:48 11/17/19 18:47 1 26 - 120 Nitrobenzene-d5 (Surr) 83 11/14/19 09:48 11/17/19 18:47 1 28 - 120 Phenol-d5 (Surr) 86 11/14/19 09:48 11/17/19 18:47 1 28 - 120 Terphenyl-d14 (Surr) 98 11/14/19 09:48 11/17/19 18:47 1 39 - 120 2,4,6-Tribromophenol (Surr) 51 11/14/19 09:48 11/17/19 18:47 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 1400 390 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:46 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 92.0 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 8.0 Eurofins TestAmerica, Michigan Page 23 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-10 Client Sample ID: B-11-15' Matrix: Soil Date Collected: 11/06/19 15:18 Percent Solids: 89.9 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1200 1200 ug/Kg ☼ 11/11/19 18:30 11/12/19 19:53 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Benzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Bromoform <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Bromomethane <300 1200 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 2-Butanone (MEK) <1200 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Carbon disulfide <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Carbon tetrachloride <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Chlorobenzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Chlorodibromomethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Chloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Chloroform <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Chloromethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ cis-1,2-Dichloroethene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ cis-1,3-Dichloropropene <300 610 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Cyclohexane <610 610 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,2-Dibromo-3-Chloropropane <610 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,2-Dichlorobenzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,3-Dichlorobenzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,4-Dichlorobenzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Dichlorobromomethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Dichlorodifluoromethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,1-Dichloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,2-Dichloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,1-Dichloroethene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,2-Dichloropropane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,2-Dibromoethane (EDB) <300 1200 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 2-Hexanone <1200 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Isopropylbenzene <300 1500 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Methyl acetate <1500 610 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ <610 610 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Methylene Chloride <610 1500 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ <1500 1200 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 4-Methyl-2-pentanone (MIBK) <1200 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Methyl tert-butyl ether <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ m-Xylene & p-Xylene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Naphthalene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ o-Xylene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Styrene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,1,2,2-Tetrachloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Tetrachloroethene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Toluene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ trans-1,2-Dichloroethene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ trans-1,3-Dichloropropene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,2,4-Trichlorobenzene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,1,1-Trichloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ 1,1,2-Trichloroethane <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Trichloroethene <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Trichlorofluoromethane <300 Eurofins TestAmerica, Michigan Page 24 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-10 Client Sample ID: B-11-15' Matrix: Soil Date Collected: 11/06/19 15:18 Percent Solids: 89.9 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <300 300 ug/Kg ☼ 11/11/19 18:30 11/12/19 19:53 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ <300 300 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Vinyl chloride <300 610 ug/Kg 11/11/19 18:30 11/12/19 19:53 1 ☼ Xylenes, Total <610 4-Bromofluorobenzene (Surr) 95 51 - 124 11/11/19 18:30 11/12/19 19:53 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 84 11/11/19 18:30 11/12/19 19:53 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 111 11/11/19 18:30 11/12/19 19:53 1 47 - 136 Toluene-d8 (Surr) 103 11/11/19 18:30 11/12/19 19:53 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <300 300 ug/Kg ☼ 11/14/19 09:48 11/17/19 19:12 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Anthracene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Benzo[a]anthracene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Benzo[a]pyrene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Benzo[b]fluoranthene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Benzo[g,h,i]perylene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Benzo[k]fluoranthene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Dibenz(a,h)anthracene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Fluoranthene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Fluorene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Indeno[1,2,3-cd]pyrene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Naphthalene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Phenanthrene <300 300 ug/Kg 11/14/19 09:48 11/17/19 19:12 1 ☼ Pyrene <300 2-Fluorobiphenyl (Surr) 78 35 - 120 11/14/19 09:48 11/17/19 19:12 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 72 11/14/19 09:48 11/17/19 19:12 1 26 - 120 Nitrobenzene-d5 (Surr) 79 11/14/19 09:48 11/17/19 19:12 1 28 - 120 Phenol-d5 (Surr) 85 11/14/19 09:48 11/17/19 19:12 1 28 - 120 Terphenyl-d14 (Surr) 87 11/14/19 09:48 11/17/19 19:12 1 39 - 120 2,4,6-Tribromophenol (Surr) 33 11/14/19 09:48 11/17/19 19:12 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 1300 320 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:49 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 89.9 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 10.1 Eurofins TestAmerica, Michigan Page 25 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-11 Client Sample ID: B-12-10' Matrix: Soil Date Collected: 11/06/19 15:30 Percent Solids: 92.9 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1200 1200 ug/Kg ☼ 11/11/19 18:30 11/12/19 20:18 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Benzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Bromoform <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Bromomethane <290 1200 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 2-Butanone (MEK) <1200 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Carbon disulfide <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Carbon tetrachloride <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Chlorobenzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Chlorodibromomethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Chloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Chloroform <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Chloromethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ cis-1,2-Dichloroethene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ cis-1,3-Dichloropropene <290 580 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Cyclohexane <580 580 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,2-Dibromo-3-Chloropropane <580 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,2-Dichlorobenzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,3-Dichlorobenzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,4-Dichlorobenzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Dichlorobromomethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Dichlorodifluoromethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,1-Dichloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,2-Dichloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,1-Dichloroethene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,2-Dichloropropane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,2-Dibromoethane (EDB) <290 1200 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 2-Hexanone <1200 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Isopropylbenzene <290 1400 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Methyl acetate <1400 580 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ <580 580 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Methylene Chloride <580 1400 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ <1400 1200 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 4-Methyl-2-pentanone (MIBK) <1200 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Methyl tert-butyl ether <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ m-Xylene & p-Xylene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Naphthalene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ o-Xylene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Styrene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,1,2,2-Tetrachloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Tetrachloroethene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Toluene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ trans-1,2-Dichloroethene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ trans-1,3-Dichloropropene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,2,4-Trichlorobenzene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,1,1-Trichloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ 1,1,2-Trichloroethane <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Trichloroethene <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Trichlorofluoromethane <290 Eurofins TestAmerica, Michigan Page 26 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-11 Client Sample ID: B-12-10' Matrix: Soil Date Collected: 11/06/19 15:30 Percent Solids: 92.9 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <290 290 ug/Kg ☼ 11/11/19 18:30 11/12/19 20:18 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ <290 290 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Vinyl chloride <290 580 ug/Kg 11/11/19 18:30 11/12/19 20:18 1 ☼ Xylenes, Total <580 4-Bromofluorobenzene (Surr) 90 51 - 124 11/11/19 18:30 11/12/19 20:18 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 78 11/11/19 18:30 11/12/19 20:18 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 102 11/11/19 18:30 11/12/19 20:18 1 47 - 136 Toluene-d8 (Surr) 103 11/11/19 18:30 11/12/19 20:18 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <280 280 ug/Kg ☼ 11/14/19 09:48 11/17/19 19:37 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Benzo[a]anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Benzo[a]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Benzo[b]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Benzo[g,h,i]perylene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Benzo[k]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Dibenz(a,h)anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Fluorene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Indeno[1,2,3-cd]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Naphthalene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Phenanthrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 19:37 1 ☼ Pyrene <280 2-Fluorobiphenyl (Surr) 78 35 - 120 11/14/19 09:48 11/17/19 19:37 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 72 11/14/19 09:48 11/17/19 19:37 1 26 - 120 Nitrobenzene-d5 (Surr) 78 11/14/19 09:48 11/17/19 19:37 1 28 - 120 Phenol-d5 (Surr) 82 11/14/19 09:48 11/17/19 19:37 1 28 - 120 Terphenyl-d14 (Surr) 90 11/14/19 09:48 11/17/19 19:37 1 39 - 120 2,4,6-Tribromophenol (Surr) 49 11/14/19 09:48 11/17/19 19:37 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 5300 330 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:51 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 92.9 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 7.1 Eurofins TestAmerica, Michigan Page 27 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-12 Client Sample ID: B-13-5' Matrix: Soil Date Collected: 11/06/19 15:50 Percent Solids: 93.7 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1100 1100 ug/Kg ☼ 11/11/19 18:30 11/12/19 20:43 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Benzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Bromoform <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Bromomethane <270 1100 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 2-Butanone (MEK) <1100 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Carbon disulfide <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Carbon tetrachloride <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Chlorobenzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Chlorodibromomethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Chloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Chloroform <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Chloromethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ cis-1,2-Dichloroethene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ cis-1,3-Dichloropropene <270 540 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Cyclohexane <540 540 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,2-Dibromo-3-Chloropropane <540 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,2-Dichlorobenzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,3-Dichlorobenzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,4-Dichlorobenzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Dichlorobromomethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Dichlorodifluoromethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,1-Dichloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,2-Dichloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,1-Dichloroethene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,2-Dichloropropane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,2-Dibromoethane (EDB) <270 1100 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 2-Hexanone <1100 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Isopropylbenzene <270 1400 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Methyl acetate <1400 540 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ <540 540 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Methylene Chloride <540 1400 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ <1400 1100 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 4-Methyl-2-pentanone (MIBK) <1100 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Methyl tert-butyl ether <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ m-Xylene & p-Xylene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Naphthalene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ o-Xylene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Styrene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,1,2,2-Tetrachloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Tetrachloroethene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Toluene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ trans-1,2-Dichloroethene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ trans-1,3-Dichloropropene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,2,4-Trichlorobenzene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,1,1-Trichloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ 1,1,2-Trichloroethane <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Trichloroethene <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Trichlorofluoromethane <270 Eurofins TestAmerica, Michigan Page 28 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-12 Client Sample ID: B-13-5' Matrix: Soil Date Collected: 11/06/19 15:50 Percent Solids: 93.7 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <270 270 ug/Kg ☼ 11/11/19 18:30 11/12/19 20:43 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ <270 270 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Vinyl chloride <270 540 ug/Kg 11/11/19 18:30 11/12/19 20:43 1 ☼ Xylenes, Total <540 4-Bromofluorobenzene (Surr) 95 51 - 124 11/11/19 18:30 11/12/19 20:43 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 80 11/11/19 18:30 11/12/19 20:43 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 104 11/11/19 18:30 11/12/19 20:43 1 47 - 136 Toluene-d8 (Surr) 105 11/11/19 18:30 11/12/19 20:43 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <280 280 ug/Kg ☼ 11/14/19 09:48 11/17/19 20:03 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Benzo[a]anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Benzo[a]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Benzo[b]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Benzo[g,h,i]perylene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Benzo[k]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Dibenz(a,h)anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Fluorene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Indeno[1,2,3-cd]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Naphthalene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Phenanthrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:03 1 ☼ Pyrene <280 2-Fluorobiphenyl (Surr) 62 35 - 120 11/14/19 09:48 11/17/19 20:03 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 49 11/14/19 09:48 11/17/19 20:03 1 26 - 120 Nitrobenzene-d5 (Surr) 49 11/14/19 09:48 11/17/19 20:03 1 28 - 120 Phenol-d5 (Surr) 59 11/14/19 09:48 11/17/19 20:03 1 28 - 120 Terphenyl-d14 (Surr) 84 11/14/19 09:48 11/17/19 20:03 1 39 - 120 2,4,6-Tribromophenol (Surr) 55 11/14/19 09:48 11/17/19 20:03 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 3700 290 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:53 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 93.7 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 6.3 Eurofins TestAmerica, Michigan Page 29 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-13 Client Sample ID: B-14-10' Matrix: Soil Date Collected: 11/06/19 16:40 Percent Solids: 94.6 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <2000 2000 ug/Kg ☼ 11/11/19 18:30 11/12/19 21:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Benzene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Bromoform <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Bromomethane <500 2000 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 2-Butanone (MEK) <2000 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Carbon disulfide <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Carbon tetrachloride <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Chlorobenzene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Chlorodibromomethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Chloroethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Chloroform <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Chloromethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ cis-1,2-Dichloroethene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ cis-1,3-Dichloropropene <500 1000 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Cyclohexane <1000 1000 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,2-Dibromo-3-Chloropropane <1000 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,2-Dichlorobenzene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,3-Dichlorobenzene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,4-Dichlorobenzene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Dichlorobromomethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Dichlorodifluoromethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,1-Dichloroethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,2-Dichloroethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,1-Dichloroethene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,2-Dichloropropane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,2-Dibromoethane (EDB) <500 2000 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 2-Hexanone <2000 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Isopropylbenzene <500 2500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Methyl acetate <2500 1000 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ <1000 1000 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Methylene Chloride <1000 2500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ <2500 2000 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 4-Methyl-2-pentanone (MIBK) <2000 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Methyl tert-butyl ether <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ m-Xylene & p-Xylene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Naphthalene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ o-Xylene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Styrene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,1,2,2-Tetrachloroethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Tetrachloroethene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Toluene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ trans-1,2-Dichloroethene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ trans-1,3-Dichloropropene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,2,4-Trichlorobenzene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,1,1-Trichloroethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ 1,1,2-Trichloroethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Trichloroethene <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Trichlorofluoromethane <500 Eurofins TestAmerica, Michigan Page 30 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-13 Client Sample ID: B-14-10' Matrix: Soil Date Collected: 11/06/19 16:40 Percent Solids: 94.6 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <500 500 ug/Kg ☼ 11/11/19 18:30 11/12/19 21:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ <500 500 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Vinyl chloride <500 1000 ug/Kg 11/11/19 18:30 11/12/19 21:08 1 ☼ Xylenes, Total <1000 4-Bromofluorobenzene (Surr) 262 X 51 - 124 11/11/19 18:30 11/12/19 21:08 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 208 X 11/11/19 18:30 11/12/19 21:08 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 283 X 11/11/19 18:30 11/12/19 21:08 1 47 - 136 Toluene-d8 (Surr) 288 X 11/11/19 18:30 11/12/19 21:08 1 55 - 123 Method: 8260B - Volatile Organic Compounds (GC/MS) - RE RL Acetone <1100 1100 ug/Kg ☼ 11/11/19 19:37 11/13/19 14:59 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Benzene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Bromoform <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Bromomethane <270 1100 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 2-Butanone (MEK) <1100 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Carbon disulfide <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Carbon tetrachloride <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Chlorobenzene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Chlorodibromomethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Chloroethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Chloroform <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Chloromethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ cis-1,2-Dichloroethene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ cis-1,3-Dichloropropene <270 540 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Cyclohexane <540 540 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,2-Dibromo-3-Chloropropane <540 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,2-Dichlorobenzene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,3-Dichlorobenzene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,4-Dichlorobenzene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Dichlorobromomethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Dichlorodifluoromethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,1-Dichloroethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,2-Dichloroethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,1-Dichloroethene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,2-Dichloropropane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,2-Dibromoethane (EDB) <270 1100 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 2-Hexanone <1100 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Isopropylbenzene <270 1400 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Methyl acetate <1400 540 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ <540 540 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Methylene Chloride <540 1400 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ <1400 1100 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 4-Methyl-2-pentanone (MIBK) <1100 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Methyl tert-butyl ether <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ m-Xylene & p-Xylene <270 Eurofins TestAmerica, Michigan Page 31 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-13 Client Sample ID: B-14-10' Matrix: Soil Date Collected: 11/06/19 16:40 Percent Solids: 94.6 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) - RE (Continued) RL Naphthalene <270 270 ug/Kg ☼ 11/11/19 19:37 11/13/19 14:59 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ o-Xylene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Styrene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,1,2,2-Tetrachloroethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Tetrachloroethene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Toluene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ trans-1,2-Dichloroethene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ trans-1,3-Dichloropropene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,2,4-Trichlorobenzene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,1,1-Trichloroethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,1,2-Trichloroethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Trichloroethene <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Trichlorofluoromethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ 1,1,2-Trichloro-1,2,2-trifluoroethane <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ <270 270 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Vinyl chloride <270 540 ug/Kg 11/11/19 19:37 11/13/19 14:59 1 ☼ Xylenes, Total <540 4-Bromofluorobenzene (Surr) 88 51 - 124 11/11/19 19:37 11/13/19 14:59 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 80 11/11/19 19:37 11/13/19 14:59 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 102 11/11/19 19:37 11/13/19 14:59 1 47 - 136 Toluene-d8 (Surr) 95 11/11/19 19:37 11/13/19 14:59 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <280 280 ug/Kg ☼ 11/14/19 09:48 11/17/19 20:53 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Benzo[a]anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Benzo[a]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Benzo[b]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Benzo[g,h,i]perylene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Benzo[k]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Dibenz(a,h)anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Fluorene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Indeno[1,2,3-cd]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Naphthalene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Phenanthrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:53 1 ☼ Pyrene <280 2-Fluorobiphenyl (Surr) 74 35 - 120 11/14/19 09:48 11/17/19 20:53 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 73 11/14/19 09:48 11/17/19 20:53 1 26 - 120 Nitrobenzene-d5 (Surr) 79 11/14/19 09:48 11/17/19 20:53 1 28 - 120 Phenol-d5 (Surr) 82 11/14/19 09:48 11/17/19 20:53 1 28 - 120 Eurofins TestAmerica, Michigan Page 32 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-13 Client Sample ID: B-14-10' Matrix: Soil Date Collected: 11/06/19 16:40 Percent Solids: 94.6 Date Received: 11/08/19 10:11 Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) Terphenyl-d14 (Surr) 95 39 - 120 11/14/19 09:48 11/17/19 20:53 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2,4,6-Tribromophenol (Surr) 45 11/14/19 09:48 11/17/19 20:53 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 590 340 ug/Kg ☼ 11/11/19 14:00 11/13/19 21:56 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 94.6 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 5.4 Eurofins TestAmerica, Michigan Page 33 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-14 Client Sample ID: SG-1-5' Matrix: Soil Date Collected: 11/06/19 13:30 Percent Solids: 91.2 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1100 1100 ug/Kg ☼ 11/11/19 18:30 11/12/19 21:32 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Benzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Bromoform <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Bromomethane <280 1100 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 2-Butanone (MEK) <1100 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Carbon disulfide <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Carbon tetrachloride <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Chlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Chlorodibromomethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Chloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Chloroform <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Chloromethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ cis-1,2-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ cis-1,3-Dichloropropene <280 560 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Cyclohexane <560 560 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,2-Dibromo-3-Chloropropane <560 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,2-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,3-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,4-Dichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Dichlorobromomethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Dichlorodifluoromethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,1-Dichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,2-Dichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,1-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,2-Dichloropropane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,2-Dibromoethane (EDB) <280 1100 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 2-Hexanone <1100 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Isopropylbenzene <280 1400 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Methyl acetate <1400 560 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ <560 560 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Methylene Chloride <560 1400 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ <1400 1100 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 4-Methyl-2-pentanone (MIBK) <1100 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Methyl tert-butyl ether <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ m-Xylene & p-Xylene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Naphthalene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ o-Xylene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Styrene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,1,2,2-Tetrachloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Tetrachloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Toluene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ trans-1,2-Dichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ trans-1,3-Dichloropropene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,2,4-Trichlorobenzene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,1,1-Trichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ 1,1,2-Trichloroethane <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Trichloroethene <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Trichlorofluoromethane <280 Eurofins TestAmerica, Michigan Page 34 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-14 Client Sample ID: SG-1-5' Matrix: Soil Date Collected: 11/06/19 13:30 Percent Solids: 91.2 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <280 280 ug/Kg ☼ 11/11/19 18:30 11/12/19 21:32 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ <280 280 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Vinyl chloride <280 560 ug/Kg 11/11/19 18:30 11/12/19 21:32 1 ☼ Xylenes, Total <560 4-Bromofluorobenzene (Surr) 103 51 - 124 11/11/19 18:30 11/12/19 21:32 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 88 11/11/19 18:30 11/12/19 21:32 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 116 11/11/19 18:30 11/12/19 21:32 1 47 - 136 Toluene-d8 (Surr) 107 11/11/19 18:30 11/12/19 21:32 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <290 290 ug/Kg ☼ 11/14/19 09:48 11/17/19 21:18 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Benzo[a]anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Benzo[a]pyrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Benzo[b]fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Benzo[g,h,i]perylene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Benzo[k]fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Dibenz(a,h)anthracene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Fluoranthene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Fluorene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Indeno[1,2,3-cd]pyrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Naphthalene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Phenanthrene <290 290 ug/Kg 11/14/19 09:48 11/17/19 21:18 1 ☼ Pyrene <290 2-Fluorobiphenyl (Surr) 69 35 - 120 11/14/19 09:48 11/17/19 21:18 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 66 11/14/19 09:48 11/17/19 21:18 1 26 - 120 Nitrobenzene-d5 (Surr) 70 11/14/19 09:48 11/17/19 21:18 1 28 - 120 Phenol-d5 (Surr) 72 11/14/19 09:48 11/17/19 21:18 1 28 - 120 Terphenyl-d14 (Surr) 84 11/14/19 09:48 11/17/19 21:18 1 39 - 120 2,4,6-Tribromophenol (Surr) 43 11/14/19 09:48 11/17/19 21:18 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 1700 300 ug/Kg ☼ 11/11/19 14:00 11/13/19 22:02 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 91.2 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 8.8 Eurofins TestAmerica, Michigan Page 35 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-15 Client Sample ID: Duplicate Matrix: Soil Date Collected: 11/06/19 00:00 Percent Solids: 96.2 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1100 1100 ug/Kg ☼ 11/11/19 18:30 11/12/19 21:57 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Benzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Bromoform <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Bromomethane <260 1100 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 2-Butanone (MEK) <1100 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Carbon disulfide <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Carbon tetrachloride <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Chlorobenzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Chlorodibromomethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Chloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Chloroform <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Chloromethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ cis-1,2-Dichloroethene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ cis-1,3-Dichloropropene <260 530 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Cyclohexane <530 530 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,2-Dibromo-3-Chloropropane <530 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,2-Dichlorobenzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,3-Dichlorobenzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,4-Dichlorobenzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Dichlorobromomethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Dichlorodifluoromethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,1-Dichloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,2-Dichloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,1-Dichloroethene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,2-Dichloropropane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,2-Dibromoethane (EDB) <260 1100 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 2-Hexanone <1100 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Isopropylbenzene <260 1300 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Methyl acetate <1300 530 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ <530 530 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Methylene Chloride <530 1300 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ <1300 1100 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 4-Methyl-2-pentanone (MIBK) <1100 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Methyl tert-butyl ether <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ m-Xylene & p-Xylene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Naphthalene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ o-Xylene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Styrene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,1,2,2-Tetrachloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Tetrachloroethene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Toluene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ trans-1,2-Dichloroethene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ trans-1,3-Dichloropropene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,2,4-Trichlorobenzene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,1,1-Trichloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ 1,1,2-Trichloroethane <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Trichloroethene <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Trichlorofluoromethane <260 Eurofins TestAmerica, Michigan Page 36 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-15 Client Sample ID: Duplicate Matrix: Soil Date Collected: 11/06/19 00:00 Percent Solids: 96.2 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <260 260 ug/Kg ☼ 11/11/19 18:30 11/12/19 21:57 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ <260 260 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Vinyl chloride <260 530 ug/Kg 11/11/19 18:30 11/12/19 21:57 1 ☼ Xylenes, Total <530 4-Bromofluorobenzene (Surr) 97 51 - 124 11/11/19 18:30 11/12/19 21:57 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 79 11/11/19 18:30 11/12/19 21:57 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 106 11/11/19 18:30 11/12/19 21:57 1 47 - 136 Toluene-d8 (Surr) 100 11/11/19 18:30 11/12/19 21:57 1 55 - 123 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <280 280 ug/Kg ☼ 11/14/19 09:48 11/17/19 20:28 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Benzo[a]anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Benzo[a]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Benzo[b]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Benzo[g,h,i]perylene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Benzo[k]fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Dibenz(a,h)anthracene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Fluoranthene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Fluorene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Indeno[1,2,3-cd]pyrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Naphthalene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Phenanthrene <280 280 ug/Kg 11/14/19 09:48 11/17/19 20:28 1 ☼ Pyrene <280 2-Fluorobiphenyl (Surr) 79 35 - 120 11/14/19 09:48 11/17/19 20:28 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 78 11/14/19 09:48 11/17/19 20:28 1 26 - 120 Nitrobenzene-d5 (Surr) 81 11/14/19 09:48 11/17/19 20:28 1 28 - 120 Phenol-d5 (Surr) 86 11/14/19 09:48 11/17/19 20:28 1 28 - 120 Terphenyl-d14 (Surr) 94 11/14/19 09:48 11/17/19 20:28 1 39 - 120 2,4,6-Tribromophenol (Surr) 41 11/14/19 09:48 11/17/19 20:28 1 10 - 120 Method: 6020 - Metals (ICP/MS) RL Lead 1900 350 ug/Kg ☼ 11/11/19 14:00 11/13/19 22:05 2 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier General Chemistry RL Percent Solids 96.2 0.1 % 11/11/19 16:08 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 0.1 % 11/11/19 16:08 1 Percent Moisture 3.8 Eurofins TestAmerica, Michigan Page 37 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-16 Client Sample ID: Field Blank Matrix: Soil Date Collected: 11/06/19 13:35 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <1000 1000 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Benzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Bromoform <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Bromomethane <250 1000 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 2-Butanone (MEK) <1000 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Carbon disulfide <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Carbon tetrachloride <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Chlorobenzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Chlorodibromomethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Chloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Chloroform <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Chloromethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 cis-1,2-Dichloroethene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 cis-1,3-Dichloropropene <250 500 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Cyclohexane <500 500 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,2-Dibromo-3-Chloropropane <500 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,2-Dichlorobenzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,3-Dichlorobenzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,4-Dichlorobenzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Dichlorobromomethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Dichlorodifluoromethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,1-Dichloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,2-Dichloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,1-Dichloroethene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,2-Dichloropropane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,2-Dibromoethane (EDB) <250 1000 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 2-Hexanone <1000 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Isopropylbenzene <250 1300 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Methyl acetate <1300 500 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 <500 500 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Methylene Chloride <500 1300 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 <1300 1000 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 4-Methyl-2-pentanone (MIBK) <1000 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Methyl tert-butyl ether <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 m-Xylene & p-Xylene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Naphthalene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 o-Xylene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Styrene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,1,2,2-Tetrachloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Tetrachloroethene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Toluene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 trans-1,2-Dichloroethene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 trans-1,3-Dichloropropene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,2,4-Trichlorobenzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,1,1-Trichloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 1,1,2-Trichloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Trichloroethene <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Trichlorofluoromethane <250 Eurofins TestAmerica, Michigan Page 38 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-16 Client Sample ID: Field Blank Matrix: Soil Date Collected: 11/06/19 13:35 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 <250 250 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Vinyl chloride <250 500 ug/Kg 11/11/19 18:30 11/12/19 22:22 1 Xylenes, Total <500 4-Bromofluorobenzene (Surr) 104 51 - 124 11/11/19 18:30 11/12/19 22:22 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 91 11/11/19 18:30 11/12/19 22:22 1 49 - 122 1,2-Dichloroethane-d4 (Surr) 116 11/11/19 18:30 11/12/19 22:22 1 47 - 136 Toluene-d8 (Surr) 113 11/11/19 18:30 11/12/19 22:22 1 55 - 123 Eurofins TestAmerica, Michigan Page 39 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-17 Client Sample ID: B-10-85'-90' Matrix: Ground Water Date Collected: 11/06/19 14:35 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone 25 10 ug/L 11/16/19 16:02 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 1.0 ug/L 11/16/19 16:02 1 Benzene <1.0 1.0 ug/L 11/16/19 16:02 1 Bromodichloromethane <1.0 1.0 ug/L 11/16/19 16:02 1 Bromoform <1.0 1.0 ug/L 11/16/19 16:02 1 Bromomethane <1.0 10 ug/L 11/16/19 16:02 1 2-Butanone (MEK) <10 5.0 ug/L 11/16/19 16:02 1 Carbon disulfide <5.0 1.0 ug/L 11/16/19 16:02 1 Carbon tetrachloride <1.0 1.0 ug/L 11/16/19 16:02 1 Chlorobenzene <1.0 1.0 ug/L 11/16/19 16:02 1 Chloroethane <1.0 1.0 ug/L 11/16/19 16:02 1 Chloroform <1.0 1.0 ug/L 11/16/19 16:02 1 Chloromethane <1.0 1.0 ug/L 11/16/19 16:02 1 cis-1,2-Dichloroethene <1.0 1.0 ug/L 11/16/19 16:02 1 cis-1,3-Dichloropropene <1.0 1.0 ug/L 11/16/19 16:02 1 Cyclohexane <1.0 * 1.0 ug/L 11/16/19 16:02 1 Dibromochloromethane <1.0 * 1.0 ug/L 11/16/19 16:02 1 1,2-Dibromo-3-Chloropropane <1.0 1.0 ug/L 11/16/19 16:02 1 1,2-Dibromoethane (EDB) <1.0 * 1.0 ug/L 11/16/19 16:02 1 1,2-Dichlorobenzene <1.0 1.0 ug/L 11/16/19 16:02 1 1,3-Dichlorobenzene <1.0 1.0 ug/L 11/16/19 16:02 1 1,4-Dichlorobenzene <1.0 1.0 ug/L 11/16/19 16:02 1 Dichlorodifluoromethane <1.0 1.0 ug/L 11/16/19 16:02 1 1,1-Dichloroethane <1.0 1.0 ug/L 11/16/19 16:02 1 1,2-Dichloroethane <1.0 1.0 ug/L 11/16/19 16:02 1 1,1-Dichloroethene <1.0 1.0 ug/L 11/16/19 16:02 1 1,2-Dichloropropane <1.0 1.0 ug/L 11/16/19 16:02 1 <1.0 10 ug/L 11/16/19 16:02 1 2-Hexanone <10 1.0 ug/L 11/16/19 16:02 1 Isopropylbenzene <1.0 10 ug/L 11/16/19 16:02 1 Methyl acetate <10 1.0 ug/L 11/16/19 16:02 1 <1.0 5.0 ug/L 11/16/19 16:02 1 Methylene Chloride <5.0 5.0 ug/L 11/16/19 16:02 1 <5.0 10 ug/L 11/16/19 16:02 1 4-Methyl-2-pentanone (MIBK) <10 1.0 ug/L 11/16/19 16:02 1 Methyl tert-butyl ether <1.0 2.0 ug/L 11/16/19 16:02 1 m-Xylene & p-Xylene <2.0 1.0 ug/L 11/16/19 16:02 1 Naphthalene <1.0 1.0 ug/L 11/16/19 16:02 1 o-Xylene <1.0 1.0 ug/L 11/16/19 16:02 1 Styrene <1.0 1.0 ug/L 11/16/19 16:02 1 1,1,2,2-Tetrachloroethane <1.0 1.0 ug/L 11/16/19 16:02 1 Tetrachloroethene <1.0 1.0 ug/L 11/16/19 16:02 1 Toluene <1.0 1.0 ug/L 11/16/19 16:02 1 trans-1,2-Dichloroethene <1.0 1.0 ug/L 11/16/19 16:02 1 trans-1,3-Dichloropropene <1.0 * 1.0 ug/L 11/16/19 16:02 1 1,2,4-Trichlorobenzene <1.0 1.0 ug/L 11/16/19 16:02 1 1,1,1-Trichloroethane <1.0 1.0 ug/L 11/16/19 16:02 1 1,1,2-Trichloroethane <1.0 * 1.0 ug/L 11/16/19 16:02 1 Trichloroethene <1.0 1.0 ug/L 11/16/19 16:02 1 Trichlorofluoromethane <1.0 Eurofins TestAmerica, Michigan Page 40 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-17 Client Sample ID: B-10-85'-90' Matrix: Ground Water Date Collected: 11/06/19 14:35 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <1.0 1.0 ug/L 11/16/19 16:02 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 1.0 ug/L 11/16/19 16:02 1 <1.0 1.0 ug/L 11/16/19 16:02 1 <1.0 1.0 ug/L 11/16/19 16:02 1 Vinyl chloride <1.0 2.0 ug/L 11/16/19 16:02 1 Xylenes, Total <2.0 4-Bromofluorobenzene (Surr) 83 47 - 134 11/16/19 16:02 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 118 11/16/19 16:02 1 78 - 129 1,2-Dichloroethane-d4 (Surr) 101 11/16/19 16:02 1 75 - 130 Toluene-d8 (Surr) 99 11/16/19 16:02 1 69 - 122 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Anthracene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Benzo[a]anthracene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Benzo[b]fluoranthene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Benzo[k]fluoranthene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Benzo[g,h,i]perylene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Benzo[a]pyrene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Dibenz(a,h)anthracene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Fluoranthene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Fluorene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Indeno[1,2,3-cd]pyrene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Naphthalene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Phenanthrene <9.3 9.3 ug/L 11/11/19 09:41 11/14/19 09:34 1 Pyrene <9.3 2-Fluorobiphenyl (Surr) 81 46 - 120 11/11/19 09:41 11/14/19 09:34 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 74 11/11/19 09:41 11/14/19 09:34 1 27 - 123 2,4,6-Tribromophenol (Surr) 78 11/11/19 09:41 11/14/19 09:34 1 33 - 120 Nitrobenzene-d5 (Surr) 76 11/11/19 09:41 11/14/19 09:34 1 46 - 120 Phenol-d5 (Surr) 67 11/11/19 09:41 11/14/19 09:34 1 23 - 120 Terphenyl-d14 (Surr) 83 11/11/19 09:41 11/14/19 09:34 1 53 - 120 Eurofins TestAmerica, Michigan Page 41 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-18 Client Sample ID: B-10-74'-79' Matrix: Ground Water Date Collected: 11/06/19 14:55 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) RL Acetone <10 10 ug/L 11/16/19 16:28 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 1.0 ug/L 11/16/19 16:28 1 Benzene <1.0 1.0 ug/L 11/16/19 16:28 1 Bromodichloromethane <1.0 1.0 ug/L 11/16/19 16:28 1 Bromoform <1.0 1.0 ug/L 11/16/19 16:28 1 Bromomethane <1.0 10 ug/L 11/16/19 16:28 1 2-Butanone (MEK) <10 5.0 ug/L 11/16/19 16:28 1 Carbon disulfide <5.0 1.0 ug/L 11/16/19 16:28 1 Carbon tetrachloride <1.0 1.0 ug/L 11/16/19 16:28 1 Chlorobenzene <1.0 1.0 ug/L 11/16/19 16:28 1 Chloroethane <1.0 1.0 ug/L 11/16/19 16:28 1 Chloroform <1.0 1.0 ug/L 11/16/19 16:28 1 Chloromethane <1.0 1.0 ug/L 11/16/19 16:28 1 cis-1,2-Dichloroethene <1.0 1.0 ug/L 11/16/19 16:28 1 cis-1,3-Dichloropropene <1.0 1.0 ug/L 11/16/19 16:28 1 Cyclohexane <1.0 * 1.0 ug/L 11/16/19 16:28 1 Dibromochloromethane <1.0 * 1.0 ug/L 11/16/19 16:28 1 1,2-Dibromo-3-Chloropropane <1.0 1.0 ug/L 11/16/19 16:28 1 1,2-Dibromoethane (EDB) <1.0 * 1.0 ug/L 11/16/19 16:28 1 1,2-Dichlorobenzene <1.0 1.0 ug/L 11/16/19 16:28 1 1,3-Dichlorobenzene <1.0 1.0 ug/L 11/16/19 16:28 1 1,4-Dichlorobenzene <1.0 1.0 ug/L 11/16/19 16:28 1 Dichlorodifluoromethane <1.0 1.0 ug/L 11/16/19 16:28 1 1,1-Dichloroethane <1.0 1.0 ug/L 11/16/19 16:28 1 1,2-Dichloroethane <1.0 1.0 ug/L 11/16/19 16:28 1 1,1-Dichloroethene <1.0 1.0 ug/L 11/16/19 16:28 1 1,2-Dichloropropane <1.0 1.0 ug/L 11/16/19 16:28 1 <1.0 10 ug/L 11/16/19 16:28 1 2-Hexanone <10 1.0 ug/L 11/16/19 16:28 1 Isopropylbenzene <1.0 10 ug/L 11/16/19 16:28 1 Methyl acetate <10 1.0 ug/L 11/16/19 16:28 1 <1.0 5.0 ug/L 11/16/19 16:28 1 Methylene Chloride <5.0 5.0 ug/L 11/16/19 16:28 1 <5.0 10 ug/L 11/16/19 16:28 1 4-Methyl-2-pentanone (MIBK) <10 1.0 ug/L 11/16/19 16:28 1 Methyl tert-butyl ether <1.0 2.0 ug/L 11/16/19 16:28 1 m-Xylene & p-Xylene <2.0 1.0 ug/L 11/16/19 16:28 1 Naphthalene <1.0 1.0 ug/L 11/16/19 16:28 1 o-Xylene <1.0 1.0 ug/L 11/16/19 16:28 1 Styrene <1.0 1.0 ug/L 11/16/19 16:28 1 1,1,2,2-Tetrachloroethane <1.0 1.0 ug/L 11/16/19 16:28 1 Tetrachloroethene <1.0 1.0 ug/L 11/16/19 16:28 1 Toluene <1.0 1.0 ug/L 11/16/19 16:28 1 trans-1,2-Dichloroethene <1.0 1.0 ug/L 11/16/19 16:28 1 trans-1,3-Dichloropropene <1.0 * 1.0 ug/L 11/16/19 16:28 1 1,2,4-Trichlorobenzene <1.0 1.0 ug/L 11/16/19 16:28 1 1,1,1-Trichloroethane <1.0 1.0 ug/L 11/16/19 16:28 1 1,1,2-Trichloroethane <1.0 * 1.0 ug/L 11/16/19 16:28 1 Trichloroethene <1.0 1.0 ug/L 11/16/19 16:28 1 Trichlorofluoromethane <1.0 Eurofins TestAmerica, Michigan Page 42 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Client Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Lab Sample ID: 190-21518-18 Client Sample ID: B-10-74'-79' Matrix: Ground Water Date Collected: 11/06/19 14:55 Date Received: 11/08/19 10:11 Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) RL 1,1,2-Trichloro-1,2,2-trifluoroethane <1.0 1.0 ug/L 11/16/19 16:28 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 1.0 ug/L 11/16/19 16:28 1 <1.0 1.0 ug/L 11/16/19 16:28 1 <1.0 1.0 ug/L 11/16/19 16:28 1 Vinyl chloride <1.0 2.0 ug/L 11/16/19 16:28 1 Xylenes, Total <2.0 4-Bromofluorobenzene (Surr) 77 47 - 134 11/16/19 16:28 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery Dibromofluoromethane (Surr) 118 11/16/19 16:28 1 78 - 129 1,2-Dichloroethane-d4 (Surr) 95 11/16/19 16:28 1 75 - 130 Toluene-d8 (Surr) 96 11/16/19 16:28 1 69 - 122 Method: 8270C - Semivolatile Organic Compounds (GC/MS) RL Acenaphthene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Anthracene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Benzo[a]anthracene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Benzo[b]fluoranthene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Benzo[k]fluoranthene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Benzo[g,h,i]perylene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Benzo[a]pyrene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Dibenz(a,h)anthracene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Fluoranthene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Fluorene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Indeno[1,2,3-cd]pyrene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Naphthalene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Phenanthrene <9.6 9.6 ug/L 11/11/19 09:41 11/14/19 09:57 1 Pyrene <9.6 2-Fluorobiphenyl (Surr) 75 46 - 120 11/11/19 09:41 11/14/19 09:57 1 Surrogate Dil Fac Analyzed Prepared Qualifier Limits %Recovery 2-Fluorophenol (Surr) 68 11/11/19 09:41 11/14/19 09:57 1 27 - 123 2,4,6-Tribromophenol (Surr) 82 11/11/19 09:41 11/14/19 09:57 1 33 - 120 Nitrobenzene-d5 (Surr) 60 11/11/19 09:41 11/14/19 09:57 1 46 - 120 Phenol-d5 (Surr) 61 11/11/19 09:41 11/14/19 09:57 1 23 - 120 Terphenyl-d14 (Surr) 71 11/11/19 09:41 11/14/19 09:57 1 53 - 120 Method: 6020 - Metals (ICP/MS) - Total Recoverable RL Lead <1.0 1.0 ug/L 11/11/19 14:00 11/13/19 19:07 1 Analyte Dil Fac Analyzed Prepared Unit D Result Qualifier Eurofins TestAmerica, Michigan Page 43 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8260B - Volatile Organic Compounds (GC/MS) Client Sample ID: Method Blank Lab Sample ID: MB 240-410327/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 410440 Prep Batch: 410327 RL Acetone <1000 1000 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Benzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Bromoform <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Bromomethane <1000 1000 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 2-Butanone (MEK) <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Carbon disulfide <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Carbon tetrachloride <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Chlorobenzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Chloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Chloroform <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Chloromethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 cis-1,2-Dichloroethene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 cis-1,3-Dichloropropene <500 500 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Cyclohexane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Chlorodibromomethane <500 500 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,2-Dibromo-3-Chloropropane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,2-Dichlorobenzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,3-Dichlorobenzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Dichlorobromomethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,4-Dichlorobenzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Dichlorodifluoromethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,1-Dichloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,2-Dichloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,1-Dichloroethene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,2-Dichloropropane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,2-Dibromoethane (EDB) <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 <1000 1000 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 2-Hexanone <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Isopropylbenzene <1300 1300 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Methyl acetate <500 500 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 <500 500 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Methylene Chloride <1300 1300 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 <1000 1000 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 4-Methyl-2-pentanone (MIBK) <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Methyl tert-butyl ether <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 m-Xylene & p-Xylene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Naphthalene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 o-Xylene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Styrene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,1,2,2-Tetrachloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Tetrachloroethene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Toluene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 trans-1,2-Dichloroethene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 trans-1,3-Dichloropropene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,2,4-Trichlorobenzene <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,1,1-Trichloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,1,2-Trichloroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Trichloroethene Eurofins TestAmerica, Michigan Page 44 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method Blank Lab Sample ID: MB 240-410327/1-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 410440 Prep Batch: 410327 RL Trichlorofluoromethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 1,1,2-Trichloro-1,2,2-trifluoroethane <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 <250 250 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Vinyl chloride <500 500 ug/Kg 11/11/19 18:30 11/12/19 13:43 1 Xylenes, Total 4-Bromofluorobenzene (Surr) 84 51 - 124 11/12/19 13:43 1 MB MB Surrogate 11/11/19 18:30 Dil Fac Prepared Analyzed Qualifier Limits %Recovery 80 11/11/19 18:30 11/12/19 13:43 1 Dibromofluoromethane (Surr) 49 - 122 96 11/11/19 18:30 11/12/19 13:43 1 1,2-Dichloroethane-d4 (Surr) 47 - 136 96 11/11/19 18:30 11/12/19 13:43 1 Toluene-d8 (Surr) 55 - 123 Client Sample ID: Lab Control Sample Lab Sample ID: LCS 240-410327/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 410440 Prep Batch: 410327 Acetone 2000 1510 ug/Kg 75 47 - 157 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Benzene 1000 890 ug/Kg 89 75 - 120 Bromoform 1000 589 ug/Kg 59 44 - 131 Bromomethane 1000 <250 ug/Kg 16 10 - 158 2-Butanone (MEK) 2000 1570 ug/Kg 79 61 - 131 Carbon disulfide 1000 671 ug/Kg 67 33 - 144 Carbon tetrachloride 1000 761 ug/Kg 76 54 - 130 Chlorobenzene 1000 945 ug/Kg 95 79 - 120 Chloroethane 1000 <250 ug/Kg 13 10 - 159 Chloroform 1000 893 ug/Kg 89 74 - 120 Chloromethane 1000 754 ug/Kg 75 40 - 127 cis-1,2-Dichloroethene 1000 875 ug/Kg 88 76 - 120 cis-1,3-Dichloropropene 1000 840 ug/Kg 84 62 - 124 Cyclohexane 1000 884 ug/Kg 88 57 - 126 Chlorodibromomethane 1000 753 ug/Kg 75 60 - 121 1,2-Dibromo-3-Chloropropane 1000 618 ug/Kg 62 35 - 137 1,2-Dichlorobenzene 1000 927 ug/Kg 93 74 - 120 1,3-Dichlorobenzene 1000 952 ug/Kg 95 74 - 120 Dichlorobromomethane 1000 789 ug/Kg 79 63 - 121 1,4-Dichlorobenzene 1000 968 ug/Kg 97 74 - 120 Dichlorodifluoromethane 1000 618 ug/Kg 62 18 - 137 1,1-Dichloroethane 1000 855 ug/Kg 86 69 - 120 1,2-Dichloroethane 1000 991 ug/Kg 99 66 - 120 1,1-Dichloroethene 1000 833 ug/Kg 83 48 - 140 1,2-Dichloropropane 1000 887 ug/Kg 89 77 - 120 1,2-Dibromoethane (EDB) 1000 892 ug/Kg 89 73 - 126 1000 957 ug/Kg 96 75 - 120 2-Hexanone 2000 1430 ug/Kg 72 54 - 135 Isopropylbenzene 1000 948 ug/Kg 95 74 - 120 Methyl acetate 2000 1560 ug/Kg 78 63 - 120 Eurofins TestAmerica, Michigan Page 45 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample Lab Sample ID: LCS 240-410327/2-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 410440 Prep Batch: [PHONE REDACTED] 923 ug/Kg 92 62 - 124 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Methylene Chloride 1000 817 ug/Kg 82 48 - 142 4-Methyl-2-pentanone (MIBK) 2000 1420 ug/Kg 71 56 - 124 Methyl tert-butyl ether 1000 855 ug/Kg 85 66 - 120 m-Xylene & p-Xylene 1000 947 ug/Kg 95 76 - 120 Naphthalene 1000 767 ug/Kg 77 43 - 127 o-Xylene 1000 929 ug/Kg 93 76 - 120 Styrene 1000 944 ug/Kg 94 70 - 120 1,1,2,2-Tetrachloroethane 1000 932 ug/Kg 93 61 - 134 Tetrachloroethene 1000 916 ug/Kg 92 75 - 124 Toluene 1000 985 ug/Kg 98 76 - 120 trans-1,2-Dichloroethene 1000 909 ug/Kg 91 74 - 125 trans-1,3-Dichloropropene 1000 807 ug/Kg 81 58 - 120 1,2,4-Trichlorobenzene 1000 818 ug/Kg 82 56 - 120 1,1,1-Trichloroethane 1000 824 ug/Kg 82 60 - 126 1,1,2-Trichloroethane 1000 916 ug/Kg 92 78 - 120 Trichloroethene 1000 890 ug/Kg 89 75 - 123 Trichlorofluoromethane 1000 882 ug/Kg 88 33 - 152 1,1,2-Trichloro-1,2,2-trifluoroetha ne 1000 899 ug/Kg 90 58 - 144 1000 989 ug/Kg 99 69 - 122 1000 1030 ug/Kg 103 68 - 126 Vinyl chloride 1000 828 ug/Kg 83 39 - 140 Xylenes, Total 2000 1880 ug/Kg 94 77 - 120 4-Bromofluorobenzene (Surr) 51 - 124 Surrogate 87 LCS LCS Qualifier Limits %Recovery 82 Dibromofluoromethane (Surr) 49 - 122 91 1,2-Dichloroethane-d4 (Surr) 47 - 136 91 Toluene-d8 (Surr) 55 - 123 Client Sample ID: Lab Control Sample Lab Sample ID: LCS 240-410327/4-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 410647 Prep Batch: [PHONE REDACTED] 1100 J ug/Kg 55 50 - 134 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits 4-Bromofluorobenzene (Surr) 51 - 124 Surrogate 81 LCS LCS Qualifier Limits %Recovery 76 Dibromofluoromethane (Surr) 49 - 122 89 1,2-Dichloroethane-d4 (Surr) 47 - 136 90 Toluene-d8 (Surr) 55 - 123 Eurofins TestAmerica, Michigan Page 46 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 240-410327/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 410440 Prep Batch: 410327 Acetone 2000 1530 ug/Kg 77 47 - 157 2 40 Analyte LCSD LCSD D Unit Result Qualifier %Rec Spike Added %Rec. Limits Limit RPD RPD Benzene 1000 890 ug/Kg 89 75 - 120 0 40 Bromoform 1000 611 ug/Kg 61 44 - 131 4 40 Bromomethane 1000 <250 ug/Kg 16 10 - 158 3 40 2-Butanone (MEK) 2000 1730 ug/Kg 86 61 - 131 9 40 Carbon disulfide 1000 655 ug/Kg 66 33 - 144 2 40 Carbon tetrachloride 1000 746 ug/Kg 75 54 - 130 2 40 Chlorobenzene 1000 964 ug/Kg 96 79 - 120 2 40 Chloroethane 1000 <250 ug/Kg 10 10 - 159 22 40 Chloroform 1000 896 ug/Kg 90 74 - 120 0 40 Chloromethane 1000 742 ug/Kg 74 40 - 127 2 40 cis-1,2-Dichloroethene 1000 891 ug/Kg 89 76 - 120 2 40 cis-1,3-Dichloropropene 1000 846 ug/Kg 85 62 - 124 1 40 Cyclohexane 1000 853 ug/Kg 85 57 - 126 4 40 Chlorodibromomethane 1000 774 ug/Kg 77 60 - 121 3 40 1,2-Dibromo-3-Chloropropane 1000 675 ug/Kg 68 35 - 137 9 40 1,2-Dichlorobenzene 1000 951 ug/Kg 95 74 - 120 2 40 1,3-Dichlorobenzene 1000 971 ug/Kg 97 74 - 120 2 40 Dichlorobromomethane 1000 793 ug/Kg 79 63 - 121 0 40 1,4-Dichlorobenzene 1000 969 ug/Kg 97 74 - 120 0 40 Dichlorodifluoromethane 1000 560 ug/Kg 56 18 - 137 10 40 1,1-Dichloroethane 1000 861 ug/Kg 86 69 - 120 1 40 1,2-Dichloroethane 1000 983 ug/Kg 98 66 - 120 1 40 1,1-Dichloroethene 1000 820 ug/Kg 82 48 - 140 2 40 1,2-Dichloropropane 1000 885 ug/Kg 88 77 - 120 0 40 1,2-Dibromoethane (EDB) 1000 934 ug/Kg 93 73 - 126 5 40 1000 965 ug/Kg 97 75 - 120 1 40 2-Hexanone 2000 1670 ug/Kg 83 54 - 135 15 40 Isopropylbenzene 1000 954 ug/Kg 95 74 - 120 1 40 Methyl acetate 2000 1690 ug/Kg 85 63 - 120 8 40 1000 876 ug/Kg 88 62 - 124 5 40 Methylene Chloride 1000 809 ug/Kg 81 48 - 142 1 40 4-Methyl-2-pentanone (MIBK) 2000 1560 ug/Kg 78 56 - 124 10 40 Methyl tert-butyl ether 1000 902 ug/Kg 90 66 - 120 5 40 m-Xylene & p-Xylene 1000 983 ug/Kg 98 76 - 120 4 40 Naphthalene 1000 822 ug/Kg 82 43 - 127 7 40 o-Xylene 1000 963 ug/Kg 96 76 - 120 4 40 Styrene 1000 977 ug/Kg 98 70 - 120 3 40 1,1,2,2-Tetrachloroethane 1000 997 ug/Kg 100 61 - 134 7 40 Tetrachloroethene 1000 949 ug/Kg 95 75 - 124 4 40 Toluene 1000 1010 ug/Kg 101 76 - 120 3 40 trans-1,2-Dichloroethene 1000 903 ug/Kg 90 74 - 125 1 40 trans-1,3-Dichloropropene 1000 846 ug/Kg 85 58 - 120 5 40 1,2,4-Trichlorobenzene 1000 800 ug/Kg 80 56 - 120 2 40 1,1,1-Trichloroethane 1000 841 ug/Kg 84 60 - 126 2 40 1,1,2-Trichloroethane 1000 992 ug/Kg 99 78 - 120 8 40 Trichloroethene 1000 877 ug/Kg 88 75 - 123 1 40 Trichlorofluoromethane 1000 829 ug/Kg 83 33 - 152 6 40 Eurofins TestAmerica, Michigan Page 47 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 240-410327/3-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 410440 Prep Batch: 410327 1,1,2-Trichloro-1,2,2-trifluoroetha ne 1000 861 ug/Kg 86 58 - 144 4 40 Analyte LCSD LCSD D Unit Result Qualifier %Rec Spike Added %Rec. Limits Limit RPD RPD 1000 1000 ug/Kg 100 69 - 122 1 40 1000 1020 ug/Kg 102 68 - 126 1 40 Vinyl chloride 1000 792 ug/Kg 79 39 - 140 4 40 Xylenes, Total 2000 1950 ug/Kg 97 77 - 120 4 40 4-Bromofluorobenzene (Surr) 51 - 124 Surrogate 88 LCSD LCSD Qualifier Limits %Recovery 82 Dibromofluoromethane (Surr) 49 - 122 91 1,2-Dichloroethane-d4 (Surr) 47 - 136 92 Toluene-d8 (Surr) 55 - 123 Client Sample ID: Lab Control Sample Dup Lab Sample ID: LCSD 240-410327/5-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 410647 Prep Batch: [PHONE REDACTED] 1110 J ug/Kg 55 50 - 134 1 40 Analyte LCSD LCSD D Unit Result Qualifier %Rec Spike Added %Rec. Limits Limit RPD RPD 4-Bromofluorobenzene (Surr) 51 - 124 Surrogate 83 LCSD LCSD Qualifier Limits %Recovery 78 Dibromofluoromethane (Surr) 49 - 122 93 1,2-Dichloroethane-d4 (Surr) 47 - 136 92 Toluene-d8 (Surr) 55 - 123 Client Sample ID: Method Blank Lab Sample ID: MB 240-411253/7 Matrix: Water Prep Type: Total/NA Analysis Batch: 411253 RL Acetone <10 10 ug/L 11/16/19 13:52 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier <1.0 1.0 ug/L 11/16/19 13:52 1 Benzene <1.0 1.0 ug/L 11/16/19 13:52 1 Bromoform <1.0 1.0 ug/L 11/16/19 13:52 1 Bromomethane <10 10 ug/L 11/16/19 13:52 1 2-Butanone (MEK) <5.0 5.0 ug/L 11/16/19 13:52 1 Carbon disulfide <1.0 1.0 ug/L 11/16/19 13:52 1 Carbon tetrachloride <1.0 1.0 ug/L 11/16/19 13:52 1 Chlorobenzene <1.0 1.0 ug/L 11/16/19 13:52 1 Chloroethane <1.0 1.0 ug/L 11/16/19 13:52 1 Chloroform <1.0 1.0 ug/L 11/16/19 13:52 1 Chloromethane <1.0 1.0 ug/L 11/16/19 13:52 1 cis-1,2-Dichloroethene <1.0 1.0 ug/L 11/16/19 13:52 1 cis-1,3-Dichloropropene <1.0 1.0 ug/L 11/16/19 13:52 1 Cyclohexane <1.0 1.0 ug/L 11/16/19 13:52 1 Dibromochloromethane <1.0 1.0 ug/L 11/16/19 13:52 1 1,2-Dibromo-3-Chloropropane <1.0 1.0 ug/L 11/16/19 13:52 1 1,2-Dichlorobenzene Eurofins TestAmerica, Michigan Page 48 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method Blank Lab Sample ID: MB 240-411253/7 Matrix: Water Prep Type: Total/NA Analysis Batch: 411253 RL 1,3-Dichlorobenzene <1.0 1.0 ug/L 11/16/19 13:52 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier <1.0 1.0 ug/L 11/16/19 13:52 1 Bromodichloromethane <1.0 1.0 ug/L 11/16/19 13:52 1 1,4-Dichlorobenzene <1.0 1.0 ug/L 11/16/19 13:52 1 Dichlorodifluoromethane <1.0 1.0 ug/L 11/16/19 13:52 1 1,1-Dichloroethane <1.0 1.0 ug/L 11/16/19 13:52 1 1,2-Dichloroethane <1.0 1.0 ug/L 11/16/19 13:52 1 1,1-Dichloroethene <1.0 1.0 ug/L 11/16/19 13:52 1 1,2-Dichloropropane <1.0 1.0 ug/L 11/16/19 13:52 1 1,2-Dibromoethane (EDB) <1.0 1.0 ug/L 11/16/19 13:52 1 <10 10 ug/L 11/16/19 13:52 1 2-Hexanone <1.0 1.0 ug/L 11/16/19 13:52 1 Isopropylbenzene <10 10 ug/L 11/16/19 13:52 1 Methyl acetate <1.0 1.0 ug/L 11/16/19 13:52 1 <5.0 5.0 ug/L 11/16/19 13:52 1 Methylene Chloride <5.0 5.0 ug/L 11/16/19 13:52 1 <10 10 ug/L 11/16/19 13:52 1 4-Methyl-2-pentanone (MIBK) <1.0 1.0 ug/L 11/16/19 13:52 1 Methyl tert-butyl ether <2.0 2.0 ug/L 11/16/19 13:52 1 m-Xylene & p-Xylene <1.0 1.0 ug/L 11/16/19 13:52 1 Naphthalene <1.0 1.0 ug/L 11/16/19 13:52 1 o-Xylene <1.0 1.0 ug/L 11/16/19 13:52 1 Styrene <1.0 1.0 ug/L 11/16/19 13:52 1 1,1,2,2-Tetrachloroethane <1.0 1.0 ug/L 11/16/19 13:52 1 Tetrachloroethene <1.0 1.0 ug/L 11/16/19 13:52 1 Toluene <1.0 1.0 ug/L 11/16/19 13:52 1 trans-1,2-Dichloroethene <1.0 1.0 ug/L 11/16/19 13:52 1 trans-1,3-Dichloropropene <1.0 1.0 ug/L 11/16/19 13:52 1 1,2,4-Trichlorobenzene <1.0 1.0 ug/L 11/16/19 13:52 1 1,1,1-Trichloroethane <1.0 1.0 ug/L 11/16/19 13:52 1 1,1,2-Trichloroethane <1.0 1.0 ug/L 11/16/19 13:52 1 Trichloroethene <1.0 1.0 ug/L 11/16/19 13:52 1 Trichlorofluoromethane <1.0 1.0 ug/L 11/16/19 13:52 1 1,1,2-Trichloro-1,2,2-trifluoroethane <1.0 1.0 ug/L 11/16/19 13:52 1 <1.0 1.0 ug/L 11/16/19 13:52 1 <1.0 1.0 ug/L 11/16/19 13:52 1 Vinyl chloride <2.0 2.0 ug/L 11/16/19 13:52 1 Xylenes, Total 4-Bromofluorobenzene (Surr) 83 47 - 134 11/16/19 13:52 1 MB MB Surrogate Dil Fac Prepared Analyzed Qualifier Limits %Recovery 109 11/16/19 13:52 1 Dibromofluoromethane (Surr) 78 - 129 98 11/16/19 13:52 1 1,2-Dichloroethane-d4 (Surr) 75 - 130 98 11/16/19 13:52 1 Toluene-d8 (Surr) 69 - 122 Eurofins TestAmerica, Michigan Page 49 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample Lab Sample ID: LCS 240-411253/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 411253 Acetone 20.0 12.6 ug/L 63 33 - 155 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Benzene 10.0 9.71 ug/L 97 77 - 123 Bromoform 10.0 6.28 ug/L 63 47 - 133 Bromomethane 10.0 9.54 ug/L 95 48 - 144 2-Butanone (MEK) 20.0 13.9 ug/L 69 41 - 151 Carbon disulfide 10.0 8.59 ug/L 86 67 - 127 Carbon tetrachloride 10.0 11.7 ug/L 117 61 - 142 Chlorobenzene 10.0 9.66 ug/L 97 80 - 120 Chloroethane 10.0 11.4 ug/L 114 41 - 147 Chloroform 10.0 10.2 ug/L 102 74 - 127 Chloromethane 10.0 12.9 ug/L 129 46 - 148 cis-1,2-Dichloroethene 10.0 9.97 ug/L 100 75 - 124 cis-1,3-Dichloropropene 10.0 7.51 ug/L 75 68 - 128 Cyclohexane 10.0 14.5 * ug/L 145 69 - 133 Dibromochloromethane 10.0 7.42 * ug/L 74 75 - 120 1,2-Dibromo-3-Chloropropane 10.0 4.87 ug/L 49 34 - 136 1,2-Dichlorobenzene 10.0 8.93 ug/L 89 74 - 120 1,3-Dichlorobenzene 10.0 9.61 ug/L 96 74 - 120 Bromodichloromethane 10.0 8.61 ug/L 86 73 - 122 1,4-Dichlorobenzene 10.0 9.58 ug/L 96 75 - 120 Dichlorodifluoromethane 10.0 5.76 ug/L 58 35 - 137 1,1-Dichloroethane 10.0 12.1 ug/L 121 74 - 126 1,2-Dichloroethane 10.0 10.2 ug/L 102 66 - 129 1,1-Dichloroethene 10.0 8.96 ug/L 90 73 - 129 1,2-Dichloropropane 10.0 11.4 ug/L 114 79 - 127 1,2-Dibromoethane (EDB) 10.0 6.14 * ug/L 61 73 - 120 10.0 9.95 ug/L 99 80 - 120 2-Hexanone 20.0 14.1 ug/L 70 43 - 142 Isopropylbenzene 10.0 9.72 ug/L 97 73 - 123 Methyl acetate 20.0 17.4 ug/L 87 47 - 140 10.0 8.48 ug/L 85 64 - 123 Methylene Chloride 10.0 7.58 ug/L 76 63 - 134 4-Methyl-2-pentanone (MIBK) 20.0 16.7 ug/L 83 43 - 145 Methyl tert-butyl ether 10.0 6.81 ug/L 68 57 - 127 m-Xylene & p-Xylene 10.0 9.60 ug/L 96 79 - 121 Naphthalene 10.0 4.97 ug/L 50 28 - 130 o-Xylene 10.0 9.48 ug/L 95 75 - 123 Styrene 10.0 9.00 ug/L 90 75 - 121 1,1,2,2-Tetrachloroethane 10.0 4.92 ug/L 49 45 - 151 Tetrachloroethene 10.0 11.4 ug/L 114 70 - 125 Toluene 10.0 8.71 ug/L 87 79 - 122 trans-1,2-Dichloroethene 10.0 9.35 ug/L 93 74 - 130 trans-1,3-Dichloropropene 10.0 5.64 * ug/L 56 64 - 120 1,2,4-Trichlorobenzene 10.0 8.08 ug/L 81 47 - 120 1,1,1-Trichloroethane 10.0 11.3 ug/L 113 65 - 141 1,1,2-Trichloroethane 10.0 6.79 * ug/L 68 79 - 121 Trichloroethene 10.0 10.7 ug/L 107 71 - 121 Trichlorofluoromethane 10.0 11.0 ug/L 110 52 - 148 Eurofins TestAmerica, Michigan Page 50 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8260B - Volatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample Lab Sample ID: LCS 240-411253/4 Matrix: Water Prep Type: Total/NA Analysis Batch: 411253 1,1,2-Trichloro-1,2,2-trifluoroetha ne 10.0 11.6 ug/L 116 54 - 148 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits 10.0 9.17 ug/L 92 66 - 129 10.0 8.86 ug/L 89 65 - 130 Vinyl chloride 10.0 10.4 ug/L 104 61 - 134 Xylenes, Total 20.0 19.1 ug/L 95 78 - 122 4-Bromofluorobenzene (Surr) 47 - 134 Surrogate 85 LCS LCS Qualifier Limits %Recovery 113 Dibromofluoromethane (Surr) 78 - 129 89 1,2-Dichloroethane-d4 (Surr) 75 - 130 95 Toluene-d8 (Surr) 69 - 122 Method: 8270C - Semivolatile Organic Compounds (GC/MS) Client Sample ID: Method Blank Lab Sample ID: MB 240-410213/21-A Matrix: Water Prep Type: Total/NA Analysis Batch: 410782 Prep Batch: 410213 RL Acenaphthene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Anthracene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Benzo[a]anthracene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Benzo[b]fluoranthene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Benzo[g,h,i]perylene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Benzo[a]pyrene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Benzo[k]fluoranthene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Dibenz(a,h)anthracene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Fluoranthene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Fluorene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Indeno[1,2,3-cd]pyrene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Naphthalene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Phenanthrene <10 10 ug/L 11/11/19 09:41 11/14/19 06:00 1 Pyrene 2-Fluorobiphenyl (Surr) 88 46 - 120 11/14/19 06:00 1 MB MB Surrogate 11/11/19 09:41 Dil Fac Prepared Analyzed Qualifier Limits %Recovery 109 11/11/19 09:41 11/14/19 06:00 1 2-Fluorophenol (Surr) 27 - 123 78 11/11/19 09:41 11/14/19 06:00 1 Nitrobenzene-d5 (Surr) 46 - 120 70 11/11/19 09:41 11/14/19 06:00 1 Phenol-d5 (Surr) 23 - 120 59 11/11/19 09:41 11/14/19 06:00 1 2,4,6-Tribromophenol (Surr) 33 - 120 99 11/11/19 09:41 11/14/19 06:00 1 Terphenyl-d14 (Surr) 53 - 120 Eurofins TestAmerica, Michigan Page 51 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Lab Control Sample Lab Sample ID: LCS 240-410213/22-A Matrix: Water Prep Type: Total/NA Analysis Batch: 410782 Prep Batch: 410213 Acenaphthene 32.0 25.6 ug/L 80 60 - 120 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits 32.0 25.4 ug/L 79 62 - 120 Anthracene 32.0 26.4 ug/L 82 60 - 120 Benzo[a]anthracene 32.0 28.0 ug/L 88 62 - 120 Benzo[b]fluoranthene 32.0 26.6 ug/L 83 64 - 120 Benzo[g,h,i]perylene 32.0 28.2 ug/L 88 63 - 120 Benzo[a]pyrene 32.0 25.5 ug/L 80 61 - 120 Benzo[k]fluoranthene 32.0 26.4 ug/L 83 63 - 120 32.0 28.7 ug/L 90 61 - 120 Dibenz(a,h)anthracene 32.0 26.2 ug/L 82 62 - 120 Fluoranthene 32.0 27.6 ug/L 86 62 - 120 Fluorene 32.0 25.9 ug/L 81 61 - 120 Indeno[1,2,3-cd]pyrene 32.0 25.3 ug/L 79 64 - 120 32.0 25.6 ug/L 80 58 - 120 Naphthalene 32.0 26.3 ug/L 82 57 - 120 Phenanthrene 32.0 26.6 ug/L 83 59 - 120 Pyrene 32.0 28.8 ug/L 90 61 - 120 2-Fluorobiphenyl (Surr) 46 - 120 Surrogate 92 LCS LCS Qualifier Limits %Recovery 113 2-Fluorophenol (Surr) 27 - 123 94 Nitrobenzene-d5 (Surr) 46 - 120 77 Phenol-d5 (Surr) 23 - 120 109 2,4,6-Tribromophenol (Surr) 33 - 120 103 Terphenyl-d14 (Surr) 53 - 120 Client Sample ID: Method Blank Lab Sample ID: MB 240-410860/20-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 411282 Prep Batch: 410860 RL Acenaphthene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Anthracene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Benzo[a]anthracene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Benzo[b]fluoranthene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Benzo[g,h,i]perylene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Benzo[a]pyrene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Benzo[k]fluoranthene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Dibenz(a,h)anthracene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Fluoranthene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Fluorene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Indeno[1,2,3-cd]pyrene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Naphthalene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Phenanthrene <260 260 ug/Kg 11/14/19 09:48 11/17/19 14:34 1 Pyrene Eurofins TestAmerica, Michigan Page 52 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: Method Blank Lab Sample ID: MB 240-410860/20-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 411282 Prep Batch: 410860 2-Fluorobiphenyl (Surr) 77 35 - 120 11/17/19 14:34 1 MB MB Surrogate 11/14/19 09:48 Dil Fac Prepared Analyzed Qualifier Limits %Recovery 73 11/14/19 09:48 11/17/19 14:34 1 2-Fluorophenol (Surr) 26 - 120 80 11/14/19 09:48 11/17/19 14:34 1 Nitrobenzene-d5 (Surr) 28 - 120 81 11/14/19 09:48 11/17/19 14:34 1 Phenol-d5 (Surr) 28 - 120 50 11/14/19 09:48 11/17/19 14:34 1 2,4,6-Tribromophenol (Surr) 10 - 120 99 11/14/19 09:48 11/17/19 14:34 1 Terphenyl-d14 (Surr) 39 - 120 Client Sample ID: Lab Control Sample Lab Sample ID: LCS 240-410860/21-A Matrix: Solid Prep Type: Total/NA Analysis Batch: 411282 Prep Batch: 410860 Acenaphthene 667 467 ug/Kg 70 45 - 120 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits 667 455 ug/Kg 68 45 - 120 Anthracene 667 555 ug/Kg 83 52 - 120 Benzo[a]anthracene 667 579 ug/Kg 87 52 - 120 Benzo[b]fluoranthene 667 548 ug/Kg 82 52 - 120 Benzo[g,h,i]perylene 667 522 ug/Kg 78 54 - 120 Benzo[a]pyrene 667 549 ug/Kg 82 50 - 120 Benzo[k]fluoranthene 667 572 ug/Kg 86 54 - 120 667 555 ug/Kg 83 53 - 120 Dibenz(a,h)anthracene 667 536 ug/Kg 80 50 - 120 Fluoranthene 667 580 ug/Kg 87 54 - 120 Fluorene 667 478 ug/Kg 72 48 - 120 Indeno[1,2,3-cd]pyrene 667 532 ug/Kg 80 52 - 120 667 472 ug/Kg 71 42 - 120 Naphthalene 667 452 ug/Kg 68 39 - 120 Phenanthrene 667 519 ug/Kg 78 50 - 120 Pyrene 667 574 ug/Kg 86 50 - 120 2-Fluorobiphenyl (Surr) 35 - 120 Surrogate 76 LCS LCS Qualifier Limits %Recovery 74 2-Fluorophenol (Surr) 26 - 120 81 Nitrobenzene-d5 (Surr) 28 - 120 82 Phenol-d5 (Surr) 28 - 120 43 2,4,6-Tribromophenol (Surr) 10 - 120 100 Terphenyl-d14 (Surr) 39 - 120 Client Sample ID: SG-1-5' Lab Sample ID: 190-21518-14 MS Matrix: Soil Prep Type: Total/NA Analysis Batch: 411282 Prep Batch: 410860 Acenaphthene <290 730 550 ug/Kg 75 41 - 120 ☼ Analyte MS MS D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits <290 730 537 ug/Kg 74 39 - 120 ☼ Anthracene <290 730 618 ug/Kg 85 43 - 106 ☼ Benzo[a]anthracene <290 730 610 ug/Kg 84 32 - 120 ☼ Benzo[b]fluoranthene <290 730 580 ug/Kg 80 27 - 126 ☼ Eurofins TestAmerica, Michigan Page 53 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: SG-1-5' Lab Sample ID: 190-21518-14 MS Matrix: Soil Prep Type: Total/NA Analysis Batch: 411282 Prep Batch: 410860 Benzo[g,h,i]perylene <290 730 566 ug/Kg 78 29 - 122 ☼ Analyte MS MS D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Benzo[a]pyrene <290 730 570 ug/Kg 78 35 - 120 ☼ Benzo[k]fluoranthene <290 730 559 ug/Kg 77 39 - 120 ☼ <290 730 596 ug/Kg 81 31 - 121 ☼ Dibenz(a,h)anthracene <290 730 569 ug/Kg 78 36 - 120 ☼ Fluoranthene <290 730 615 ug/Kg 84 30 - 125 ☼ Fluorene <290 730 552 ug/Kg 76 44 - 120 ☼ Indeno[1,2,3-cd]pyrene <290 730 561 ug/Kg 77 34 - 120 ☼ <290 730 542 ug/Kg 74 10 - 133 ☼ Naphthalene <290 730 518 ug/Kg 71 30 - 120 ☼ Phenanthrene <290 730 586 ug/Kg 80 31 - 120 ☼ Pyrene <290 730 591 ug/Kg 81 28 - 122 ☼ 2-Fluorobiphenyl (Surr) 35 - 120 Surrogate 79 MS MS Qualifier Limits %Recovery 76 2-Fluorophenol (Surr) 26 - 120 89 Nitrobenzene-d5 (Surr) 28 - 120 86 Phenol-d5 (Surr) 28 - 120 61 2,4,6-Tribromophenol (Surr) 10 - 120 91 Terphenyl-d14 (Surr) 39 - 120 Client Sample ID: SG-1-5' Lab Sample ID: 190-21518-14 MSD Matrix: Soil Prep Type: Total/NA Analysis Batch: 411282 Prep Batch: 410860 Acenaphthene <290 722 513 ug/Kg 71 41 - 120 7 34 ☼ Analyte MSD MSD D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Limit RPD RPD <290 722 505 ug/Kg 70 39 - 120 6 34 ☼ Anthracene <290 722 582 ug/Kg 81 43 - 106 6 32 ☼ Benzo[a]anthracene <290 722 612 ug/Kg 85 32 - 120 0 37 ☼ Benzo[b]fluoranthene <290 722 559 ug/Kg 77 27 - 126 4 40 ☼ Benzo[g,h,i]perylene <290 722 542 ug/Kg 75 29 - 122 4 40 ☼ Benzo[a]pyrene <290 722 561 ug/Kg 78 35 - 120 2 38 ☼ Benzo[k]fluoranthene <290 722 569 ug/Kg 79 39 - 120 2 37 ☼ <290 722 595 ug/Kg 82 31 - 121 0 37 ☼ Dibenz(a,h)anthracene <290 722 559 ug/Kg 77 36 - 120 2 38 ☼ Fluoranthene <290 722 591 ug/Kg 82 30 - 125 4 31 ☼ Fluorene <290 722 525 ug/Kg 73 44 - 120 5 32 ☼ Indeno[1,2,3-cd]pyrene <290 722 547 ug/Kg 76 34 - 120 3 40 ☼ <290 722 528 ug/Kg 73 10 - 133 3 40 ☼ Naphthalene <290 722 503 ug/Kg 70 30 - 120 3 40 ☼ Phenanthrene <290 722 579 ug/Kg 79 31 - 120 1 35 ☼ Pyrene <290 722 578 ug/Kg 80 28 - 122 2 30 ☼ 2-Fluorobiphenyl (Surr) 35 - 120 Surrogate 73 MSD MSD Qualifier Limits %Recovery 79 2-Fluorophenol (Surr) 26 - 120 83 Nitrobenzene-d5 (Surr) 28 - 120 Eurofins TestAmerica, Michigan Page 54 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: 8270C - Semivolatile Organic Compounds (GC/MS) (Continued) Client Sample ID: SG-1-5' Lab Sample ID: 190-21518-14 MSD Matrix: Soil Prep Type: Total/NA Analysis Batch: 411282 Prep Batch: 410860 Phenol-d5 (Surr) 28 - 120 Surrogate 83 MSD MSD Qualifier Limits %Recovery 56 2,4,6-Tribromophenol (Surr) 10 - 120 91 Terphenyl-d14 (Surr) 39 - 120 Method: 6020 - Metals (ICP/MS) Client Sample ID: Method Blank Lab Sample ID: MB 240-410264/1-A ^2 Matrix: Solid Prep Type: Total/NA Analysis Batch: 410823 Prep Batch: 410264 RL Lead <400 400 ug/Kg 11/11/19 14:00 11/13/19 21:11 2 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 240-410264/2-A ^2 Matrix: Solid Prep Type: Total/NA Analysis Batch: 410823 Prep Batch: 410264 Lead 50000 48700 ug/Kg 97 80 - 120 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Client Sample ID: B-1-2.5' Lab Sample ID: 190-21518-1 MS Matrix: Soil Prep Type: Total/NA Analysis Batch: 410823 Prep Batch: 410264 Lead 2500 51000 51900 ug/Kg 97 75 - 125 ☼ Analyte MS MS D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Client Sample ID: B-1-2.5' Lab Sample ID: 190-21518-1 MSD Matrix: Soil Prep Type: Total/NA Analysis Batch: 410823 Prep Batch: 410264 Lead 2500 51000 51400 ug/Kg 96 75 - 125 1 20 ☼ Analyte MSD MSD D Unit Result Qualifier %Rec Spike Added Sample Result Sample Qualifier %Rec. Limits Limit RPD RPD Client Sample ID: Method Blank Lab Sample ID: MB 240-410255/1-A Matrix: Water Prep Type: Total Recoverable Analysis Batch: 410823 Prep Batch: 410255 RL Lead <1.0 1.0 ug/L 11/11/19 14:00 11/13/19 18:48 1 MB MB Analyte Dil Fac Analyzed Prepared D Unit Result Qualifier Client Sample ID: Lab Control Sample Lab Sample ID: LCS 240-410255/2-A Matrix: Water Prep Type: Total Recoverable Analysis Batch: 410823 Prep Batch: 410255 Lead 500 442 ug/L 88 80 - 120 Analyte LCS LCS D Unit Result Qualifier %Rec Spike Added %Rec. Limits Eurofins TestAmerica, Michigan Page 55 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- QC Sample Results Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Method: Moisture - Percent Moisture Client Sample ID: B-7-15' Lab Sample ID: 190-21518-7 DU Matrix: Soil Prep Type: Total/NA Analysis Batch: 410266 Percent Solids 93.2 94.5 % 1 20 Analyte DU DU D Unit Result Qualifier Sample Result Sample Qualifier Limit RPD RPD Percent Moisture 6.8 5.5 F3 % 21 20 Eurofins TestAmerica, Michigan Page 56 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Definitions/Glossary Job ID: 190-21518-1 Client: Sagasser & Associates Inc Project/Site: Royal Crest Qualifiers GC/MS VOA Qualifier Description * LCS or LCSD is outside acceptance limits. Qualifier J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. X Surrogate is outside control limits General Chemistry Qualifier Description F3 Duplicate RPD exceeds the control limit Qualifier Glossary These commonly used abbreviations may or may not be present in this report. ¤ Listed under the column to designate that the result is reported on a dry weight basis Abbreviation %R Percent Recovery CFL Contains Free Liquid CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) PQL Practical Quantitation Limit QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) Eurofins TestAmerica, Michigan Page 57 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Page 58 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Page 59 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Page 60 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Page 61 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Page 62 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Page 63 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Page 64 of 64 11/19/2019 1 2 3 4 5 6 7 8 ---PAGE BREAK--- Phase II Environmental Site Assessment Project #31902 Former Royal Crest Motel - Gaylord, Michigan APPENDIX D GROUND PENETRATING RADAR REPORT ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com July 26, 2019 Kevin Sagasser Sagasser & Associates, Inc. 699 South Wisconsin Avenue Gaylord, MI 49735 Survey Site: Royal Crest Motel-805 South Otsego Avenue-Gaylord, MI Project Objective: Utilize Ground Penetrating Radar and ElectroMagnetic locating to investigate for any evidence of remaining underground structures, evidence of removal of previously existing underground structures, evidence of remaining footings or debris from previously existing buildings, and location of underground utilities in the areas indicated in the drawing provided by Kevin Sagasser of Sagasser & Associates. GPR Information and Background: GPR has been used extensively in the past for geological and archeological exploration and mapping; however, it has only been since 2001 that GPR had the capability to image shallow targets. The system used for this project has the ability to image targets to a depth of 12 feet with an accuracy of ± 2 inches. The 400 MHz antenna broadcasts a microwave energy pulse of less than 1/6th watt at a rate of 100 ns. This energy pulse is timed as it propagates through a material noting when a return pulse arrives. The time and strength of the return pulse is captured and analyzed and interpreted graphically. This process is shown in the figure of a 1500 MHz antenna below. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Project Procedures: Scans were completed every 5 feet in a grid pattern throughout the defined areas using Ground Penetrating Radar. Also, electromagnetic locating was used to verify locations of utilities found and/or find any utilities that were not discovered by the Ground Penetrating Radar. Any utilities, remaining underground storage tanks, septic areas, and significant soil debris were marked on site, photographed, and identified on the drawing attached to this report. Any utility with known origin or purpose was marked according to the MISS DIG standards listed below. Any unknown anomalies, remaining underground storage tanks, or unknown utilities were marked in pink. Communication-Orange Electric-Red Sewer-Green or Brown Gas-Yellow Water-Blue All data was collected on July 22, 2019. Project Results: There were no anomalies found indicative of remaining underground storage tanks. There were four areas of excavation/backfilled soils found scattered throughout the survey area. One of the excavation/backfilled areas was consistent with the documented underground storage tank removal area on the northwest corner of the property. The other three excavation/backfilled areas are from unknown sources or causes. These excavation areas were marked on site in white paint. The following utilities were marked on site: natural gas marked in yellow, sewer marked in green, communications in orange, and water marked in blue. All results of the data collected are documented in the attached drawing and pictures of markings are also attached. The pictures attached have a number that corresponds with the drawing attached to give area of where the picture was taken. Sincerely, Nick Schwartz Facility Management Consultants International [EMAIL REDACTED] (616) 730-3331 ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 1 shows excavation/backfill area marked in white. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 2 shows excavation/backfill area marked in white paint. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 3 shows excavation/backfill area marked in white. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 4 shows excavation/backfill area marked in white. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 5 shows water marked in blue. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 6 shows natural gas marked in yellow and water in blue. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 7 shows natural gas marked in blue and excavation/backfill area in white. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 8 shows communications marked in orange and unknown marked in pink. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 9 shows communications marked in orange and natural gas in yellow. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 10 shows water marked in blue. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 11 shows sewer marked in green and communications in orange. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image 12 shows communications marked in orange. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image taken by drone footage after GPR survey was completed. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Image taken by drone footage after GPR survey was completed. ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Raw Data Images: Excavation/Backfill Area ---PAGE BREAK--- Improve profitability. Reduce risk. Manage liability. www.facilitiescompliance.com Water Pipe ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- APPENDIX C Brand Land Surveying LLC ‘Draft’ Certificate of Survey ---PAGE BREAK--- D:\survey_data\SURVEY\T30N-R3W\04195063.dwg ---PAGE BREAK--- D:\survey_data\SURVEY\T30N-R3W\04195063.dwg ---PAGE BREAK--- APPENDIX D Wade-Trim Certificate of Survey ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- ---PAGE BREAK--- COUNTY OF OTSEGO Administrative Policy Manual Page Number 1 of 9 Policy No Subject Date Issued 500.01 Purchasing 4/13/04 Application Revised General Fund Functions General Fund Departments 46th Trial Court Other Jointly Governed Organizations Special Revenue Functions Parks and Recreation Library Social Welfare (Family Independence Agency) Commission on Aging Other Special Revenue Funds Building Authority Business-Type Functions Delinquent Tax Revolving Commissary Bus System Administrative Services Building and Grounds Component Units University Center Road Commission Ambulance Other: 08/14/12 Applicable Forms Contact Department Contact Phone Number Contact Fax Number Administration [PHONE REDACTED] [PHONE REDACTED] Contact E-Mail [EMAIL REDACTED] Summary The purpose of this policy is to establish procedures for the purchase of all supplies, equipment, vehicles, and all construction or altering of County facilities for any department of the County of Otsego in a manner that maximizes the purchasing value of public funds in procurement. This policy includes capital leases on any such item as listed above. When the procurement involves the expenditure of federal or state assistance or contract funds, the procurement shall be conducted in accordance with any mandatory applicable federal or state laws and regulations. Nothing in this policy shall prevent any public agency from complying with the terms and conditions of any grant, gift or bequest that is otherwise consistent with law. Professional service contracts and contracts for specific, non-repetitive services are exempt from the requirements of this Policy with the exception of the requirements contained in Sections 2.18 and 2.19 of the Policy. Procedures 1. Definitions 1.1 Capital Outlay Items: Non-expendable items itemized in the County’s capital improvement budget/plan. 1.2 Competitive Bids: Prices received from vendors on items or services $10,001 or more. Competitive bids are received as sealed bids only and are opened at advertised public bid openings. The requirement for sealed competitive bids shall not apply to intergovernmental contracts, contracts for professional services, contracts for specific, non-repetitive services, or emergency repairs, or for the reauthorization of contracts, which have been previously approved by the Otsego County Board of Commissioners. 1.3 Expendable/Recurrent Supplies: Routine supplies needed to carry on the County’s daily ---PAGE BREAK--- COUNTY OF OTSEGO Administrative Policy Manual Page Number 2 of 9 Procedures business (i.e. food, medical supplies, office supplies). Expendable supplies are generally acquired using preferred vendors. 1.4 Final Approver: Person(s) designated to utilize the electronic purchasing system with the authority to convert requisitions to purchase orders. 1.5 Formal Bidding: Formal bidding procedure should be used for purchases from $5,001 to $10,000. It includes solicitation of written bids through the mail, e-mail, and facsimile. 1.6 Informal Bidding: Purchases of $501 to $5000 are subject to informal bidding. Informal bids (quotes) includes solicitation of written bids and may be solicited by telephone, personal contact, or in writing. 1.7 Public Bid Opening: A place, date and time established to open competitive bids received on items and/or services being procured. Adequate public notice of the invitation for bids shall be given not less than 7 calendar days prior to the date set forth therein for the opening of bids. Such notice may include publication in a newspaper of general circulation within the County for a reasonable time prior to the bid opening. 1.8 Request for Proposal (RFP): A document issued by the County Administrator, which contains specifications and County bidding procedures for procurement of items and/or services. An RFP is sent out to vendors as a mechanism to solicit for competitive bids. 1.9 Request for Quotation (RFQ): A document (less formal than an RFP) issued by the County Administrator/Management Team Member, which contains specifications for the procurement of items and/or services. An RFQ is sent out to vendors as a mechanism to solicit for competitive quotes. 1.10 Professional Service Contract: A Contract for unique, technical, and/or infrequent functions performed by an independent contractor qualified by education, experience, and/or technical ability to provide services. In most cases, these services are of a specific project nature, and are not a continuing, ongoing responsibility of the institution. 1.11 Service Contract: an agreement whereby a contractor supplies time, effort and/or expertise instead of a good (tangible product). 2. POLICY: The County utilizes an electronic accounting system with a purchasing module that includes a requisition and purchase order system. Every purchase on behalf of the County (unless specifically exempted) shall require a requisition and purchase order. Except as otherwise specified herein, purchases / contracts will be awarded to a contractor or bidder based on price, record of performance, availability, dependability and experience. All purchases by contract, or otherwise, as herein authorized, will be in accordance with such appropriations as have been made by the Board of Commissioners for the support of the respective departments. ---PAGE BREAK--- COUNTY OF OTSEGO Administrative Policy Manual Page Number 3 of 9 Procedures It shall be unethical for any County employee to participate directly or indirectly in a procurement contract when (the County employee knows that) the County employee or any member of the County employee’s immediate family has a financial interest pertaining to the procurement contract. 2.1 Basic Purchases: Items valued at $500 or less are considered basic purchases. There are not any bidding requirements for these purchases; however, the requisition and purchase order system must be utilized. Management Team Members or their designee(s) are authorized to draft requisitions and act as the final approver. The responsible party shall exercise reasonable scrutiny when expending funds under the $500 threshold. 2.2 Informal Bidding: Purchases of $501 to $5000 are subject to informal bidding. Individual employees, with approval of the County Administrator, may solicit informal bids as outlined below. Bids must be written. The County Administrator (their designee when absent) must act as final approver. A. Bid Information: To insure fairness in, each vendor solicited should be given the same information. This information should include:  Description of items to be purchased  Special terms and/or specifications  Desired delivery date B. Record of Bids: All bids solicited shall be in writing and will be electronically recorded in the requisition “Post It” note window. Each record should contain:  Bid Information  Record of all bids  Manager’s explanation if lowest priced vendor not selected. 2.3 Formal Bidding: Purchases from $5,001 to $10,000 are subject to the formal bidding procedure. The respective department shall follow the formal bidding process. The Management Team Member must approve with the County Administrator or designee acting as the final approver. It includes solicitation of written quotations/bids through direct contact, public advertisement or any combination of the same. A. The solicitation/advertisement must include the following:  Identification of item(s) to be bid upon  Location bids are to be submitted  Date and time of bid deadline for submission  Contact for further information  Statement of County’s rights to reject bids  Contract compliance terms  Product specifications B. Record of Bids: All bids solicited shall be electronically recorded in the ---PAGE BREAK--- COUNTY OF OTSEGO Administrative Policy Manual Page Number 4 of 9 Procedures requisition “Post It” note window. Each record should contain:  Bid Information  Record of all bids  Department Head explanation if lowest priced vendor not selected. 2.4 Competitive Bidding: Purchases with an anticipated obligation of $10,001 or more are required to have sealed, competitive bidding and comply with Public Act 167 and 168 of 1993. Two competitive bids are required for purchases of $10,001 or more. Professional services, contracts for specific, non-repetitive services, and intergovernmental contracts and emergency repairs, or reauthorization of contracts that have been previously approved are exempted from this policy. The inability to obtain two competitive bids, upon due diligence, shall not prevent the County from awarding the bid. A copy of all bid document material must be provided to the Administration Department. A. If a bid document must be prepared ($10,001 or more), it shall include:  Bid Reference Number as assigned by the Administration Department  Bid advertisement  Bid preparation instructions  Proposal  Contract  General conditions  Special conditions  General specifications  Detailed specifications  State or Federal guidelines (if necessary) The County reserves the right to accept, reject or negotiate any or all bids, to waive or not waive informalities or irregularities in bids or bidding procedures, to rebid the project/purchase, and to accept any bid determined by the County to be in the best interest of the County, regardless of price. The reason for rejection may include past performance issues, and compatibility with existing equipment or software. Local Vendors, as defined below, are hereby granted a 5% cost variance for low bid determination. A “local vendor” is defined as a business that has had a fixed office or distribution point located in and having a street address within the county for at least six months immediately prior to the issuance of the request for competitive bids (post office boxes do not qualify as a business address). In addition, the business must employ at least one full-time or two part-time employees whose primary residence is located within Otsego County, or if the business has no employees, shall be at least fifty percent owned by one or more persons whose primary residence(s) is located within Otsego County. B. All bids shall be opened at the time, date and place specified, and the opening and inspection of all bids shall be made by the County Administrator. A complete ---PAGE BREAK--- COUNTY OF OTSEGO Administrative Policy Manual Page Number 5 of 9 Procedures summary of the bids, including the bidding firm’s name, cost, qualifying data, and any other relevant information, shall be kept on file. Final approval, acceptance and selection of bids that are low bid and meet specifications shall be recommended by the County Administrator to the Board of Commissioners. 2.5 Expendable Supplies: For each expendable category of purchases, the County Administrator, with the assistance of the respective department staff (i.e. maintenance/jail food staff), will compile and maintain a list of preferred suppliers. Such lists will be reviewed and updated periodically. Typically one – three vendors will be listed to provide comparison pricing and selection options. 2.6 Open Purchase Orders: Open Purchase Orders shall be utilized for vendors that provide routine repetitive services. Open Purchase Orders may be opened and closed within any calendar month. Examples of authorized open purchase orders include: oil changes, car wash and other similar services. 2.7 Emergency Purchase Orders: In case of emergency needs, appropriate departments (maintenance, sheriff) are authorized to make emergency procurements of supplies, services or construction items when there exists a threat to public health, welfare or safety. Electronic access shall be provided to authorize the issuance of emergency purchase orders. Emergency procurements shall be made with such competition as is practicable under the circumstances and the cost shall not exceed $5,000. An emergency purchase of up to $10,000 may be made by the County Administrator without prior approval by the chair or vice-chair of the Board of Commissioners. The very nature of emergency expenditures may necessitate a significant financial decision without prior approval. All emergency expenditures in excess of $10,000 shall be reported to the Board of Commissioners, in writing, within three business days. In the case of emergency repairs where delays may cause further damage to county property, the County Administrator is authorized to spend up to $10,000 without prior approval by the chair or Vice-Chair. Emergency repairs in excess of $10,000 may be made by the County Administrator with advanced authorization from the chair or vice-chair. 2.8 Cooperative Government Contracts: Bidding requirements shall be waived if the County is able to secure favorable prices on purchases by joining with other local governments, or participating with the State of Michigan or the Federal Government in purchasing. The County Administrator is authorized to enter into the necessary agreements or contracts on behalf of the County. 2.9 Exempted Purchases: Exempted purchases include maintenance agreement billings, utility billings, contracted service invoices, insurance payments, and other like services as noted in the Otsego County Payables Policy. The appropriate account number and signature of a Management Team member is required for exempted purchases, and shall appear across the invoice. ---PAGE BREAK--- COUNTY OF OTSEGO Administrative Policy Manual Page Number 6 of 9 Procedures 2.10 Payment Procedure: The respective Management Team member will be responsible for inspection of all orders, upon receipt of the order and prior to the acceptance of the delivery. Upon acceptance of items, verification that the packing slip matches the purchase order must accompany the invoice in order to obtain payment. Whenever a department rejects any orders, the County Administrator shall be notified immediately and given the reason for the rejection. 2.11 Capital Leases: The process for bidding capital leases shall be similar to other purchases. Should the price of the purchase not be reasonably known prior to engaging the bidding process, the Formal Bidding Process shall be used. 2.12 Bid Specification Changes: All changes in bid specifications shall be reported to all known potential bidders. Such notification shall provide appropriate time for all such potential bidders to have adequate time to make adjustments to their bids. 2.13 Demo Models: Bidding requirements shall be waived if the County is able to secure favorable prices on purchases by purchasing a demonstration model. 2.14 Rebidding: Should it become necessary to rebid a project/purchase, the County Administrator may waive the newspaper posting requirement for Competitive Bids, with notification being given to the Budget & Finance Committee members. 2.15 Amending contracts on projects requiring bids: The County Administrator may approve minor amendments to capital project contracts up to an amount of $5,000, not to exceed more than 10% of the original contract amount. The County Administrator may approve minor amendments to capital project contracts up to an amount of $10,000, not to exceed 10% of the original contract amount, with pre-notification to the Budget & Finance Committee. Any contract amendment beyond the limits specified above requires approval by the Board of Commissioners. 2.16 Bond Requirements: Bid bonds are required for construction or repair projects in the amount of $100,000 or more. Bid bonds and performance bonds are required for construction or repair projects in the amount of $250,000 or more. Bid bonds shall be in the amount of 10% of the total contract price. Performance bonds will be in the amount of 100% of the total contract price. Bond requirements cannot be waived. 2.17 Lien Waivers: For construction or repair projects in the amount of $50,000 or more, the contractor is required to provide partial lien waivers, verifying all subcontractors and suppliers have been paid for their work to date, for payment requests beyond 25% of the total contract price. The final 10% of the contract price can be paid prior to receipt of lien waivers. The contractor will provide final lien waivers within 30 days of contract completion. In the event that a contractor does not provide the required lien waivers, the contract will not be eligible for future County projects without the consent of the County Infrastructure Committee. ---PAGE BREAK--- COUNTY OF OTSEGO Administrative Policy Manual Page Number 7 of 9 Procedures 2.18 Insurance Requirements: All contractors and/or vendors are required to maintain the following Insurance: A. Workers Compensation and Employers’ Liability, Michigan Statutory Limits of Liability. B. Commercial General Liability Insurance C. Motor Vehicle Liability Coverage, and Michigan No-Fault Coverages including all owned, non-owned, and hired vehicles. D. Otsego County will be named as Additional Insured on all insurance coverage, with the exception of Workers Compensation and Employers’ Liability insurance. Limits of Liability for General Liability, and Vehicle Liability shall be within the following guidelines based on contract amount:  Projects up to $750,000: Minimum of $1,000,000 per occurrence and aggregate.  Projects $750,001 to $1,750,000: Minimum of $2,000,000 per occurrence and aggregate.  Projects $1,750,001 to $2,750,000: Minimum of $3,000,000 per occurrence and aggregate.  The required amounts continue to escalate by adding $1,000,000 to the beginning and ending project range and to the minimum insurance requirement.  A Waiver of Subrogation is required on the certificate of liability insurance.  The certificate of liability insurance is required to have a 30-day notice of cancellation. 2.19 Professional Services Contracts Requirements: Professional Liability Coverage (Errors and Omissions) is required for all contracts for professional services such as architect, engineer, design firm or similar professions, and the medical professions, etc.  In the event that services delivered either directly or indirectly involve or require professional services (e.g. architectural, engineering, medical), Professional Liability Coverage (Errors and Omissions) insurance coverage must be provided with a limit of liability of not less than $1,000,000 per occurrence and aggregate generally, and must further be in an amount to be equal to or greater than the total project cost.  A Waiver of Subrogation is required on the certificate of liability insurance. ---PAGE BREAK--- COUNTY OF OTSEGO Administrative Policy Manual Page Number 8 of 9 Procedures  The certificate of liability insurance is required to have a 30-day notice of cancellation. 2.20 Other Contractor Insurance Requirements: For projects of over $250,000, all vendor insurance must be obtained through an insurance company that has a financial strength rating of A or better by a reputable insurance rating company such as A.M. Best. 2.21 Purchases on Behalf of Other Agencies: For purchases made by Otsego County while acting as a grant fiduciary on behalf of other agencies, Otsego County will allow Preferred Vendors at the written request of an authorized representative from the requesting agency. 2.22 Nepotism: A County employee or grant administrator may not hire a person related to him/her to do contractual work until approved by the County Administrator for compliance with the spirit of the County’s Purchasing Policy and Nepotism Policy. For the purposes of this policy, “related” shall cover the following relationships: 1. Parent (natural, step, or in-law) 2. Child (natural or step) 3. Brother/sister (natural, step, or in-law) 4. Spouse 5. Grandparent 6. Legal Guardian The County of Otsego will accept delivery of and authorize payment of only those services, supplies, merchandise or articles authorized for purchase, and acceptable under terms of the purchase agreement, in accordance with the procedures stated herein. Payment for any services, supplies, merchandise or articles not authorized for purchase by the County Administrator and/or the Otsego County Board of Commissioners in accordance with the policies and procedures stated herein becomes the responsibility of the person or persons requesting such service, supplies, merchandise or article and the County may deny payment of the claim. Any service being performed for the County that has not been authorized in accordance with the policies and procedures stated herein, shall be immediately discontinued and the original conditions restored at the expense of the person or persons requesting such service. Payment in full for any service, supplies, merchandise or articles not acceptable for delivery or the use required, as put forth in the bid specifications or purchase agreement for such service, supplies, merchandise or articles, will be held in abeyance until such time as a replacement or replacements meeting the specifications put forth in the purchase agreement and acceptable for the use required are received. ---PAGE BREAK--- COUNTY OF OTSEGO Administrative Policy Manual Page Number 9 of 9 Procedures TABLE 1 Dollar Amount Bidding Requirement Final Approval $0 - $500 None Management Team Member or Designee $501 - $5,000 Informal Bid County Administrator $5,001 - $10,000 Formal or Competitive Quote County Administrator $10,001 or more Competitive Bids Board of Commissioners Approvals (name and department) Board of Commissioners April 13, 2004